Synthesis and catalytic activity studies of α-MnO2 nanorodes, rutile TiO2 and its composite prepared by hydrothermal method

Author(s):  
Rashed Taleb Rasheed ◽  
Hadeel S. Mansoor ◽  
Rasha R. Al-Shaikhly ◽  
Thamer Adnan Abdullah ◽  
Ali Dawood Salman ◽  
...  
Nanoscale ◽  
2021 ◽  
Author(s):  
Bing Fu ◽  
Zhijiao Wu ◽  
Kai Guo ◽  
Lingyu Piao

Owing to their scientific and technological importance, the development of highly efficient photocatalytic water oxidation systems with rapid photogenerated charge separation and high surface catalytic activity has highly desirable for...


CrystEngComm ◽  
2011 ◽  
Vol 13 (14) ◽  
pp. 4557 ◽  
Author(s):  
Weijia Zhou ◽  
Xiaoyan Liu ◽  
Jingjie Cui ◽  
Duo Liu ◽  
Jing Li ◽  
...  

2014 ◽  
Vol 4 (12) ◽  
pp. 4250-4257 ◽  
Author(s):  
Toru Murayama ◽  
Junli Chen ◽  
Jun Hirata ◽  
Keeko Matsumoto ◽  
Wataru Ueda

Layered-structure-type niobium oxides were synthesized by the hydrothermal method by using ammonium niobium oxalate as a precursor.


Nanomaterials ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 683 ◽  
Author(s):  
Cheng Gong ◽  
Jun Du ◽  
Xiuyun Li ◽  
Zhenjie Yu ◽  
Jiansong Ma ◽  
...  

Three-dimensional and dendritic rutile TiO2 nanorods were successfully fabricated on a Ti foil surface using a one-step acidic hydrothermal method. The TiO2 nanorods were characterized using X-ray diffraction (XRD), energy dispersive X-ray spectrometry (EDX), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and optical contact angle testing. The results showed that the nanorods with diameters of 100–500 nm and lengths of 100 nm to 1 μm were obtained on the Ti foil surface. The length and density of the TiO2 nanorods were perfect at the conditions of HCl concentration 0.5 mol/L, temperature 220 °C, and reaction time 12 h. The TiO2 nanorods formed parallel to the consumption of Ti and grew along the (110) direction having a tetragonal rutile crystal. The morphology of the nanorods possessed a three-dimensional structure. The contact angle of the nanorods was only 13 ± 3.1°. Meanwhile, the photocatalytic activities of the TiO2 nanorods were carried out using ultraviolet fluorescence spectrophotometry for the methyl orange detection, and the degradation was found to be about 71.00% ± 2.43%. Thus, TiO2 nanorods can be developed by a one-step acidic hydrothermal method using Ti foil simultaneously as the substrate with a TiO2 source; the TiO2 nanorods exhibited photocatalytic performance while being environment-friendly.


2013 ◽  
Vol 743-744 ◽  
pp. 843-848
Author(s):  
Ya Ping Zhang ◽  
Qian Qian Zhi ◽  
Lian Qing Yu ◽  
Kai Tuo Dong ◽  
Ri Shan Liu ◽  
...  

In order to improve the separation efficiency and the circular utilization ratio of the catalyst, the Fe-doped nanotitanium and nanotitanium supported on Fe2O3 carrier was prepared by hydrothermal method. The tetra-butyl titanate and ethanol were used as starting materials to prepare nanotitanium. The results of Fe-doped nanotitanium showed that the doping of iron changed the nanotitanium crystal and crystal morphology. No matter UV-light or mercury lamp 577 nm irradiation, the samples with 0.5 mM Fe addition showed the highest photo catalytic activity, with degradation rate of methyl blue above 95%. The structure, photo catalytic activity and magnetic properties analysis showed that the magnetic nanotitanium met the purpose of separation between the catalyst and reaction solution. The photo catalytic activity of nanotitanium supported on Fe2O3 carrier has respond to visible light. With mercury lamp 577 nm as irradiation source, degradation rate of methylene blue light could reach 63.40%.


RSC Advances ◽  
2016 ◽  
Vol 6 (29) ◽  
pp. 24361-24365 ◽  
Author(s):  
Weiming Wu ◽  
Xianyang Yue ◽  
Xiao-Yuan Wu ◽  
Can-Zhong Lu

Nanocrystalline Ni12P5 was synthesized by a simple hydrothermal method. It showed high catalytic activity (10 760 μmol h−1 g−1, TOF = 9.3 h−1) and good stability (15 h) for the hydrogen evolution from water under visible light irradiation.


2019 ◽  
Vol 40 ◽  
pp. 94
Author(s):  
Fabiele Schaefer Rodrigues ◽  
Marcela Trojahn Nunes ◽  
Jocenir Boita

The use of nanoparticles in the field of catalysis has been the object of study by the scientific community, due to the high catalytic activity that the nanoparticles have in front of some reactions of technological interest. The objective of this work is to obtain a nanostructured catalyst using iron oxide supported on red ceramic residue (RCV), through nanostructures synthesized by the hydrothermal method, measured through the absorption of lightning in the XANES region through the National Laboratory of Synchrotron Light LNLS).


CrystEngComm ◽  
2020 ◽  
Vol 22 (14) ◽  
pp. 2462-2471
Author(s):  
V. V. Burungale ◽  
Hyojung Bae ◽  
A. S. Kamble ◽  
J.-H. Kim ◽  
P. S. Patil ◽  
...  

The structural appearance of TiO2 nanostructures can be easily engineered by means of pH of the solvent solution.


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