scholarly journals Grain orientation mapping of passivated aluminum interconnect lines by x-ray micro-diffraction

Author(s):  
C. H. Chang ◽  
A. A. MacDowell ◽  
A. C. Thompson ◽  
H. A. Padmore ◽  
J. R. Patel
1998 ◽  
Vol 524 ◽  
Author(s):  
A. A. MacDowell ◽  
C. H. Chang ◽  
H. A. Padmore ◽  
J. R. Patel ◽  
A. C. Thompson

ABSTRACTA micro x-ray diffraction facility is under development at the Advanced Light Source. Spot sizes are typically about 1-μm size generated by means of grazing incidence Kirkpatrick-Baez focusing mirrors. Photon energy is either white of energy range 6-14 keV or monochromatic generated from a pair of channel cut crystals. A Laue diffraction pattern from a single grain in a passivated 2-μm wide bamboo structured Aluminum interconnect line has been recorded. Acquisition times are of the order of a few seconds. The Laue pattern has allowed the determination of the crystallographic orientation of individual grains along the line length. The experimental and analysis procedures used are described, as is a grain orientation result. The future direction of this program is discussed in the context of strain measurements in the area of electromigration.


1995 ◽  
Vol 403 ◽  
Author(s):  
P.-C. Wang ◽  
G. S. Cargill ◽  
I. C. Noyan ◽  
E. G. Liniger

AbstractWe describe spatially resolved grain orientation mapping of polycrystalline films using a synchrotron-based x-ray microdiffraction system. The system consists of a tapered glass capillary as a white x-ray concentrator, an energy-dispersive solid state detector and an x-y-z sample stage. Two mapping modes are discussed: reciprocal-space mapping and real-space mapping. Information about the orientations of grains within the irradiated volume is determined by reciprocal-space mapping. The locations of grains having a specified orientation are determined by real-space mapping. Examples are shown for blanket films of AI(4 wt.% Cu) 4μm-thick and 0.5μm thick. Results are also shown for 10μm-wide and μm-wide pure lines. X-ray beams of 10inm diameter were used for these measurements. Spatially resolved thermal strain measurements were made for a single 10μm-wide, 200μm-long passivated Al line, and they were found to be consistent with calculations based on equi-biaxial thermal stress within the line.


1998 ◽  
Author(s):  
A.A. MacDowell ◽  
H.A. Padmore ◽  
A.C. Thompson ◽  
C.H. Chang ◽  
J.R. Patel

2003 ◽  
Vol 795 ◽  
Author(s):  
L. E. Moyer ◽  
G. S. Cargill ◽  
W. Yang ◽  
B. C. Larson ◽  
G. E. Ice

ABSTRACTThermally induced residual strains in polycrystalline Cu and Al films on single crystal Si and glass substrates, respectively, have been examined on a grain-by-grain basis by x-ray microbeam diffraction. The crystallographic orientation and the deviatoric strain tensor, εij*, are determined for each grain by white beam Laue diffraction. From grain orientation mapping and strain tensor measurements, information is obtained about the distributions of strains for similarly oriented grains, about strain variations within single grains, and about grain-to-grain correlations of strains. This type of information may be useful in developing and testing theories for intergrain effects in strain evolution in polycrystals.


2009 ◽  
Author(s):  
N. Tamura ◽  
K. Chen ◽  
M. Kunz ◽  
Paul S. Ho ◽  
Ehrenfried Zschech ◽  
...  

1990 ◽  
Vol 202 ◽  
Author(s):  
L. H. Chou ◽  
M. C. Kuo

ABSTRACTThin Sb films have been prepared on glass substrates by rapid thermal evaporation. Films with thicknesses varied from 260 Å to 1300Å were used for the study. X-ray diffraction data showed that for films deposited at room substrate temperature, an almost random grain orientation was observed for films of 1300 Å thick and a tendency for preferred grain orientation was observed as films got thinner. For films of 260 Å thick, only two x-ray diffraction peaks--(003) and (006) were observed. After thermal annealing, secondary grains grew to show preferred orientation in all the films. This phenomenon was explained by surface-energy-driven secondary grain growth. This paper reports the effects of annealing time and film thickness on the secondary grain growth and the evolution of thin Sb film microstmctures. Transmission electron microscopy (TEM) and x-ray diffraction were used to characterize the films.


Author(s):  
A. Whitaker

SummaryThe subaerial decomposition of struvite has been investigated at room temperature (21±2° C), from which it has been concluded that the decomposition product is newberyite. X-ray power patterns of newberyite, both from a diffractometer and Debye-Scherrer cameras, are given. Comparison of these patterns with other newberyite patterns suggest that the camera pattern is more reproducible; this may be due to grain orientation in the diffraetometer mounts.


2005 ◽  
Vol 105 ◽  
pp. 309-314 ◽  
Author(s):  
M. Ostafin ◽  
Jan Pospiech ◽  
Robert A. Schwarzer

The objectives of this investigation are structural effects in electrolytic copper sheets which are caused by the change of the direction of rolling. Unidirectional, reverse as well as cross-rolling at 90° respectively at 45° to the precedent rolling direction have been applied down to final deformations as low as 80% reduction in thickness. Texture has been determined by ACOM (Automated Crystal Orientation Measurement, “Automated EBSD”) in the SEM and by X-ray pole figure measurement. The main benefits of ACOM are a high spatial resolution which enables the investigation of texture gradients from the mid plane to the surface of the sheet, and the visualization of the microstructure by crystal orientation mapping. In addition to local texture, statistical distributions of misorientations across grain boundaries and of S grain boundaries have been derived from the individual grain orientation data. The change of the path of plastic deformation induces a destabilization of the substructure which is formed during the primary step of unidirectional rolling. A distinct change of texture is found depending on the deformation process. In cross rolling, the b fiber changes into the unstable b90 fiber which almost disappears with progressive deformation along the new rolling direction.


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