Fabrication and characterization of Cd0.98Zn0.02O film by inventive sol-gel screen-printing technique

2019 ◽  
Author(s):  
Renu Kumari ◽  
Vipin Kumar
Nanomaterials ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 1055
Author(s):  
Lucía dos Santos-Gómez ◽  
Javier Zamudio-García ◽  
José M. Porras-Vázquez ◽  
Enrique R. Losilla ◽  
David Marrero-López

Lowering the operating temperature of solid oxide fuel cells (SOFCs) is crucial to make this technology commercially viable. In this context, the electrode efficiency at low temperatures could be greatly enhanced by microstructural design at the nanoscale. This work describes alternative microstructural approaches to improve the electrochemical efficiency of the BaCo0.4Fe0.4Zr0.1Y0.1O3-δ (BCFZY) cathode. Different electrodes architectures are prepared in a single step by a cost-effective and scalable spray-pyrolysis deposition method. The microstructure and electrochemical efficiency are compared with those fabricated from ceramic powders and screen-printing technique. A complete structural, morphological and electrochemical characterization of the electrodes is carried out. Reduced values of area specific resistance are achieved for the nanostructured cathodes, i.e., 0.067 Ω·cm2 at 600 °C, compared to 0.520 Ω·cm2 for the same cathode obtained by screen-printing. An anode supported cell with nanostructured BCFZY cathode generates a peak power density of 1 W·cm−2 at 600 °C.


2011 ◽  
Vol 43 (3) ◽  
pp. 335-341 ◽  
Author(s):  
V. Kumar ◽  
D.K. Sharma ◽  
M.K. Bansal ◽  
D.K. Dwivedi ◽  
T.P. Sharma

Cadmium sulphide films having energy band gap of 2.4 eV found applications in solar cells and electroluminescent devices. CdS polycrystalline films have been prepared on ultra-clean glass substrate by screen-printing technique and then sintered in air. Optimum conditions for preparing good quality screen-printed films have been found. The optical band gaps ?Eg? of the CdS films were determined from the UV transmission spectroscopy and were found to be 2.47eV. The Wurtzite structure of CdS films was confirmed by X-ray diffraction analysis. DC conductivity and activation energy of films was also measured in vacuum by two-probe technique.


2004 ◽  
Vol 822 ◽  
Author(s):  
A. Morata ◽  
A. Tarancón ◽  
G. Dezanneau ◽  
F. Peiró ◽  
J. R. Morante

AbstractIn the present work, the screen printing technique has been used to deposit thick films of Zr0.84Y016O1.92 (8YSZ). In order to control the final porosity in view of a specific application (SOFCs or gas sensor), an experimental design based on analysis of variances (ANOVA) has been carried out. From this, we were able to determine the influence of several technological parameters on films porosity and grain size. The films obtained have been analysed with both Scanning Electron Microscopy (SEM) and Focused Ion Beam (FIB) combined with SEM. We show that only the combination of experimental design and advanced observation technique such as Focused Ion Beam allowed us to extract significant information for the improvement of the deposition process.


2017 ◽  
Vol 9 (24) ◽  
pp. 3689-3695 ◽  
Author(s):  
C. Karuwan ◽  
A. Wisitsoraat ◽  
P. Chaisuwan ◽  
D. Nacapricha ◽  
A. Tuantranont

This work presents a new method for mass fabrication of a new microfluidic device with integrated graphene-based electrochemical electrodes by the screen printing technique for in-channel amperometric detection.


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