Optimizing the magnetic properties of Fe-based amorphous powder by adjusting atomic structures from vitrification at different temperatures

2019 ◽  
Vol 126 (16) ◽  
pp. 165109
Author(s):  
Song-Yi Kim ◽  
Hye-Ryeong Oh ◽  
Hyeon-Ah Kim ◽  
A-Young Lee ◽  
Hwi-Jun Kim ◽  
...  
Nanomaterials ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 1097
Author(s):  
Luran Zhang ◽  
Xinchen Du ◽  
Hongjie Lu ◽  
Dandan Gao ◽  
Huan Liu ◽  
...  

L10 ordered FePt and FePtCu nanoparticles (NPs) with a good dispersion were successfully fabricated by a simple, green, one-step solid-phase reduction method. Fe (acac)3, Pt (acac)2, and CuO as the precursors were dispersed in NaCl and annealed at different temperatures with an H2-containing atmosphere. As the annealing temperature increased, the chemical order parameter (S), average particle size (D), coercivity (Hc), and saturation magnetization (Ms) of FePt and FePtCu NPs increased and the size distribution range of the particles became wider. The ordered degree, D, Hc, and Ms of FePt NPs were greatly improved by adding 5% Cu. The highest S, D, Hc, and Ms were obtained when FePtCu NPs annealed at 750 °C, which were 0.91, 4.87 nm, 12,200 Oe, and 23.38 emu/g, respectively. The structure and magnetic properties of FePt and FePtCu NPs at different annealing temperatures were investigated and the formation mechanism of FePt and FePtCu NPs were discussed in detail.


2005 ◽  
Vol 872 ◽  
Author(s):  
Yousong Gu ◽  
Dayong Zhang ◽  
Xiaoyuan Zhan ◽  
Zhen Ji ◽  
Xiaolan Zhen ◽  
...  

AbstractSeries of FePt/Fe multilayers with different layer thicknesses have been deposited on Si substrates by magnetron sputtering and post annealing at different temperatures and durations. The structure, surface morphology, composition, and magnetic properties of the deposited films have been characterized by XRD, SEM, EDX and VSM. It is found that after annealing at temperatures above 500°C, FePt phase undergoes a phase transition from disorder fcc into ordered fct structure, and become a hard magnetic phase. For [FePt/Fe]n multilayer with varying Fe layer thickness, lattice constants and grain sizes change with Fe layer thickness and annealing temperature. The coercivities of [FePt/Fe]n multilayers decrease with Fe layer deposition time, and the energy product (BH)max shows a maximum with Fe layer thickness. Optimization on layer thickness leads a high (BxH)max value of 15.2MGOe for [FePt(8min)/Fe(4min)]8. The effects of quick annealing and Ag underlayer on the structure and magnetic properties were also studied.


2012 ◽  
Vol 1471 ◽  
Author(s):  
Pierre-Emmanuel Berche ◽  
Saoussen Djedai ◽  
Etienne Talbot

ABSTRACTMonte Carlo simulations are used to perform an atomic scale modelling of the magnetic properties of epitaxial exchange-coupled DyFe2/YFe2 superlattices. These samples, extremely well-researched experimentally, are constituted by a hard ferrimagnet DyFe2 and a soft ferrimagnet YFe2 antiferromagnetically coupled. Depending on the layers and on the temperature, the field dependence of the magnetization depth profile is complex. In this work, we reproduce by Monte Carlo simulations hysteresis loops for the net and compound-specific magnetizations at different temperatures, and assess the quality of the results by a direct comparison to experimental hysteresis loops.


Rare Metals ◽  
2006 ◽  
Vol 25 (6) ◽  
pp. 458-461
Author(s):  
F GUO ◽  
S BA ◽  
D LI ◽  
Z LU ◽  
C LU ◽  
...  

2000 ◽  
Vol 215-216 ◽  
pp. 284-287 ◽  
Author(s):  
M Yagi ◽  
I Endo ◽  
I Otsuka ◽  
H Yamamoto ◽  
R Okuno ◽  
...  

2017 ◽  
Vol 89 (4) ◽  
pp. 545-552
Author(s):  
Alena Michalcová ◽  
Ivo Marek ◽  
Adél Len ◽  
Oleg Heczko ◽  
Jan Drahokoupil ◽  
...  

Abstract Nanocrystalline nickel is an interesting material for catalysis, and also, like all nanocrystalline metals, it has potential for structural application. Our aim was to develop a method for preparation of precursor materials for powder metallurgy. Because of this, selective leaching of binary alloy was chosen as it leads to production of nanocrystalline clustered (sub)micro particles. In this work, the preparation of Ni particles by selective leaching of Al matrix from Al-50 wt.% Ni in NaOH water solution is described. It was found that structure and magnetic properties were strongly dependent on leaching temperature, which was proven by characterization of Ni particles leached at −20, 0, 20, 40, 60 and 80°C. The microstructure of as-prepared particles was observed by HRTEM and also by small angle neutron scattering. Magnetic properties were characterized by measuring of saturation magnetization. It was proven that with increased leaching temperature the grain size of prepared nanocrystalline particles increased. Also the value of saturated magnetization follows the same trend. The amount of hydrogen stored in nickel particles is independent on leaching temperature.


2000 ◽  
Vol 36 (5) ◽  
pp. 3421-3423 ◽  
Author(s):  
I. Endo ◽  
H. Tatsumi ◽  
I. Otsuka ◽  
H. Yamamoto ◽  
A. Shintani ◽  
...  

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