scholarly journals Hard X-ray induced fast secondary electron cascading processes in solids

2018 ◽  
Vol 113 (11) ◽  
pp. 114102 ◽  
Author(s):  
K. Mecseki ◽  
H. Höppner ◽  
M. Büscher ◽  
V. Tkachenko ◽  
N. Medvedev ◽  
...  
Author(s):  
S.A. Wight

Measurements of electrons striking the sample in the Environmental Scanning Electron Microscope (ESEM) are needed to begin to understand the effect of the presence of the gas on analytical measurements. Accurate beam current is important to x-ray microanalysis and it is typically measured with a faraday cup. A faraday cup (Figure 1) was constructed from a carbon block embedded in non-conductive epoxy with a 45 micrometer bore platinum aperture over the hole. Currents were measured with an electrometer and recorded as instrument parameters were varied.Instrument parameters investigated included working distance, chamber pressure, condenser percentage, and accelerating voltage. The conditions studied were low vacuum with gaseous secondary electron detector (GSED) voltage on; low vacuum with GSED voltage off; and high vacuum (GSED off). The base conditions were 30 kV, 667 Pa (5 Torr) water vapor, 100,000x magnification with the beam centered inside aperture, GSED voltage at 370 VDC, condenser at 50%, and working distance at 19.5 mm. All modifications of instrument parameters were made from these conditions.


2013 ◽  
Vol 481 ◽  
pp. 133-136 ◽  
Author(s):  
T.N. Myasoedova ◽  
G.E. Yalovega ◽  
N.K. Plugotarenko ◽  
M. Brzhezinskaya ◽  
V.V. Petrov ◽  
...  

Copper oxides films as promising materials for gas sensors applications were studied. Copper oxide films were deposited onto Si/SiO2substrates using a citrate sol-gel method with the subsequent temperature treatment at 150-5000C. These films were characterized by means of secondary electron microscopy (SEM) and X-ray-absorption near-edge structure (XANES) spectroscopy. The prepared films were utilized in NO2sensors. The dependences of the NO2response on the operating temperature and NO2concentration (10-200 ppm) were investigated. The maximum NO2response was achieved for the film annealed at 2500C.


1975 ◽  
Vol 68 ◽  
pp. 45-64 ◽  
Author(s):  
John H. Parkinson

The last few years have seen great progress in our understanding of X-ray spectra of solar active regions. This paper demonstrates both the usefulness and the limitations of the techniques, both scientific and instrumental, that have recently become available. Improvements in spectral resolution led to the discovery of weak satellite lines to helium-like ions; the quantitative theory for these lines is also discussed. The observed intensities of the Fe XVII lines are also investigated and found to be in agreement with calculations that allow for cascading processes.


1989 ◽  
Vol 134 ◽  
pp. 201-202
Author(s):  
Wayne A. Stein

The observed spectral index as a function of frequency of QSO continua must be explained in models. It is generally increasing (F(ν) ∝ ν−α, α increasing) with higher frequency in the infrared (downward curvature). The visual to ultraviolet continuum has been shown to be a broken power law with F(ν) ∝ ν−0.5 at low frequency and a break to larger α at νo ∼ 3×1015 Hz. X-ray observations frequently exhibit a flat continuum with α < 1. One prominent example is 3C273 for which α1–3μm → 2, αvis ∼ 0.5 and αx ∼ 0.5. These spectral indices arise naturally in Secondary Electron Synchrotron Self-Compton (SESSC) models. Some accretion disk models approach these spectral indices for the visual-ultraviolet portion of the spectral distribution.


1989 ◽  
Vol 60 (7) ◽  
pp. 2219-2222 ◽  
Author(s):  
Y. Hirai ◽  
I. Waki ◽  
A. Momose ◽  
K. Hayakawa

2011 ◽  
Vol 88 (1-2) ◽  
pp. 164-170 ◽  
Author(s):  
Aimee L. McNamara ◽  
Susanna Guatelli ◽  
Dale A. Prokopovich ◽  
Mark I. Reinhard ◽  
Anatoly B. Rosenfeld

2019 ◽  
Vol 26 (6) ◽  
pp. 1936-1939 ◽  
Author(s):  
Noritake Isomura ◽  
Naoko Takahashi ◽  
Satoru Kosaka ◽  
Hiroyuki Kawaura

Hard X-ray photoelectron spectroscopy at multiple photon energies is used to investigate the surface structure of carbon coatings on silicon materials destined for use as negative electrodes in lithium-ion batteries. The photoelectron intensity from the carbon coatings decreases with an increase in the kinetic energy of the photoelectron. By fitting the photoelectron intensity versus energy to numerically derived curves, the thickness and coverage of the carbon coatings can be obtained. The results are in agreement with the values suggested by the cross-sectional secondary-electron microscopy images of the carbon coatings, although the thickness should be corrected by accounting for the rectangular parallelepiped structure of the silicon material.


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