Effect of grain size on structural and dielectric properties of barium titanate piezoceramics synthesized by high energy ball milling

2018 ◽  
Author(s):  
Narendra Kumar Verma ◽  
Sandeep Kumar Singh Patel ◽  
Dinesh Kumar ◽  
Chandra Bhal Singh ◽  
Akhilesh Kumar Singh
Keyword(s):  
Grain Size ◽  
Dielectric Properties ◽  
Barium Titanate ◽  
Ball Milling ◽  
High Energy ◽  
High Energy Ball Milling ◽  
Energy Ball

scholarly journals Impact Evaluation of High Energy Ball Milling Homogenization Process in the Phase Distribution of Hydroxyapatite-Barium Titanate Plasma Spray Biocoating

Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 728
Author(s):  
Roberto Gómez Batres ◽  
Zelma S. Guzmán Escobedo ◽  
Karime Carrera Gutiérrez ◽  
Irene Leal Berumen ◽  
Abel Hurtado Macias ◽  
...  
Keyword(s):  
Barium Titanate ◽  
Ball Milling ◽  
Plasma Spray ◽  
Bonding Strength ◽  
Phase Distribution ◽  
High Energy ◽  
High Energy Ball Milling ◽  
X Ray ◽  
Nanomechanical Properties ◽  
Energy Ball

Air plasma spray technique (APS) is widely used in the biomedical industry for the development of HA-based biocoatings. The present study focuses on the influence of powder homogenization treatment by high-energy ball milling (HEBM) in developing a novel hydroxyapatite-barium titanate (HA/BT) composite coating deposited by APS; in order to compare the impact of the milling process, powders were homogenized by mechanical stirring homogenization (MSH) too. For the two-homogenization process, three weight percent ratios were studied; 10%, 30%, and 50% w/w of BT in the HA matrix. The phase and crystallite size were analyzed by X-ray diffraction patterns (XRD); the BT-phase distribution in the coating was analyzed by backscattered electron image (BSE) with a scanning electron microscope (SEM); the energy-dispersive X-ray spectroscopy (EDS) analysis was used to determinate the Ca/P molar ratio of the coatings, the degree of adhesion (bonding strength) of coatings was determinate by pull-out test according to ASTM C633, and finally the nanomechanical properties was determinate by nanoindentation. In the results, the HEBM powder processing shows better efficiency in phase distribution, being the 30% (w/w) of BT in HA matrix that promotes the best bonding strength performance and failure type conduct (cohesive-type), on the other hand HEBM powder treatment promotes a slightly greater crystal phase stability and crystal shrank conduct against MSH; the HEBM promotes a better behavior in the nanomechanical properties of (i) adhesive strength, (ii) cohesive/adhesive failure-type, (iii) stiffness, (iv) elastic modulus, and (v) hardness properties.

Phase development during high-energy ball-milling of zinc oxide and iron – the impact of grain size on the source and the degree of contamination

2015 ◽  
Vol 44 (43) ◽  
pp. 18870-18881 ◽  
Author(s):  
G. Štefanić ◽  
S. Krehula ◽  
I. Štefanić
Keyword(s):  
Grain Size ◽  
Zinc Oxide ◽  
Ball Milling ◽  
High Energy ◽  
High Energy Ball Milling ◽  
Degree Of Contamination ◽  
Phase Development ◽  
Energy Ball ◽  
The Impact

The impact of grain size on the source and the degree of contamination.

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