scholarly journals Nondestructive testing of thin films using surface acoustic waves and laser ultrasonics

Author(s):  
Frédéric Jenot ◽  
Sabrina Fourez ◽  
Mohammadi Ouaftouh ◽  
Marc Duquennoy
Author(s):  
Amgad R. Rezk ◽  
Ofer Manor ◽  
Leslie Y. Yeo ◽  
James R. Friend

Arising from an interplay between capillary, acoustic and intermolecular forces, surface acoustic waves (SAWs) are observed to drive a unique and curious double flow reversal in the spreading of thin films. With a thickness at or less than the submicrometre viscous penetration depth, the film is seen to advance along the SAW propagation direction, and self-similarly over time t 1/4 in the inertial limit. At intermediate film thicknesses, beyond one-fourth the sound wavelength λ ℓ in the liquid, the spreading direction reverses, and the film propagates against the direction of the SAW propagation. The film reverses yet again, once its depth is further increased beyond one SAW wavelength. An unstable thickness region, between λ ℓ /8 and λ ℓ /4, exists from which regions of the film either rapidly grow in thickness to exceed λ ℓ /4 and move against the SAW propagation, consistent with the intermediate thickness films, whereas other regions decrease in thickness below λ ℓ /8 to conserve mass and move along the SAW propagation direction, consistent with the thin submicrometre films.


2009 ◽  
Vol 105 (2) ◽  
pp. 024508 ◽  
Author(s):  
X. Y. Du ◽  
Y. Q. Fu ◽  
J. K. Luo ◽  
A. J. Flewitt ◽  
W. I. Milne

1999 ◽  
Vol 593 ◽  
Author(s):  
A.C. Ferrari ◽  
J. Robertson ◽  
R. Pastorelli ◽  
M.G. Beghi ◽  
C.E. Bottani

ABSTRACTThe elastic constants of thin Diamond-Like Carbon (DLC) films supply important information, but their measurement is difficult. Standard nanoindentation does not directly measure the elastic constants and has strong limitations particularly in the case of hard thin films on softer substrates, such as tetrahedral amorphous carbon on Si. Surface acoustic waves provide a better mean to investigate elastic properties. Surface Brillouin scattering (SBS) intrinsically probes acoustic waves of the wavelength which is appropriate to test the properties of films in the tens to hundreds of nanometers thickness range. SBS can be used to derive all the isotropic elastic constants of hard-on-soft and soft-on-hard amorphous carbon films of different kinds, with thickness down to less than 10 nm. The results help to resolve the previous uncertainties in mechanical data. The Young's modulus of tetrahedral amorphous carbon (ta-C) turns out to be lower than that of diamond, while the moduli of hydrogenated ta-C (ta-C:H) are considerably lower than those of ta-C because of the weakening effect of C-H bonding.


2020 ◽  
pp. 147592172091516
Author(s):  
Chen-Yin Ni ◽  
Jin-Chao LV ◽  
Yue-Ying Zhang ◽  
Hai-Yan He ◽  
Xi-Feng Xia ◽  
...  

We study the responses of laser-generated acoustic waves to localized reversible/irreversible modifications of microscopic asperities on crack surfaces during crack closure, which is an essential process in nonlinear photoacoustic/photothermal crack detection techniques. Our laser ultrasonics technique involves optical measurement of the transmission and mode conversion of the laser-generated surface acoustic waves caused by the crack. Reversible/irreversible modifications of asperities can be achieved via non-contact photothermal loading of the crack. Three photothermal loading cycles were realized in individual succession and were monitored using the laser ultrasonics technique at various experimental locations along the crack. In our experiments, each photothermal loading cycle includes multiple successive subcycles, in which the material is first heated and then cooled to its equilibrium temperature, thereby initiating local closing, followed by opening of the crack. Each subcycle is monitored twice using the laser ultrasonics technique, once each at the end of heating and cooling. Furthermore, each successive subcycle is accomplished at a higher power of heating laser than that of the previous subcycle. Significant differences in the peak-to-peak amplitude of the surface skimming longitudinal acoustic wave, which is excited by mode conversion of the Rayleigh wave by the crack, are revealed during the first cycle of photothermal loading. These differences clearly indicate a partial irreversibility of the mechanical processes occurring in the crack surfaces during subcycles of the first cycle. In a larger temporal scale, irreversible modification of crack surfaces is observed from the significant difference between the experimental results of the first photothermal loading cycle and the subsequent two cycles, whereas a reversible response of the crack surface to thermoelastic loading is observed from the similarity of the measurements accumulated during the two subsequent cycles.


2020 ◽  
Vol 27 ◽  
pp. 57-61
Author(s):  
Radim Kudělka ◽  
Lukáš Václavek ◽  
Jan Tomáštík ◽  
Sabina Malecová ◽  
Radim Čtvrtlík

Knowledge of mechanical properties of thin films is essential for most of their applications. However, their determination can be problematic for very thin films. LAW (Laser-induced acoustic waves) is a combined acousto-optic method capable of measuring films with thickness from few nanometers. It utilizes ultrasound surface waves which are excited via short laser pulses and detected by a PVDF foil. Properties such as Young’s modulus, Poisson’s ratio and density of both the film and the substrate as well as film thickness can be explored.Results from the LAW method are successfully compared with nanoindentation for Young’s modulus evaluation and with optical method for film thickness evaluation and also with literature data. Application of LAW for anisotropy mapping of materials with cubic crystallographic lattice is also demonstrated.


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