scholarly journals Development of a hard X-ray split-and-delay line and performance simulations for two-color pump-probe experiments at the European XFEL

2018 ◽  
Vol 89 (6) ◽  
pp. 063121 ◽  
Author(s):  
W. Lu ◽  
B. Friedrich ◽  
T. Noll ◽  
K. Zhou ◽  
J. Hallmann ◽  
...  
Keyword(s):  
X Ray ◽  
2012 ◽  
Author(s):  
Wojciech Roseker ◽  
Sooheyong Lee ◽  
Michael Walther ◽  
Horst Schulte-Schrepping ◽  
Hermann Franz ◽  
...  

Author(s):  
Zhen Zhang ◽  
Joseph Duris ◽  
James P. MacArthur ◽  
Zhirong Huang ◽  
Agostino Marinelli

2016 ◽  
Author(s):  
Maurice A. Leutenegger ◽  
Marc Audard ◽  
Kevin R. Boyce ◽  
Gregory V. Brown ◽  
Meng P. Chiao ◽  
...  
Keyword(s):  
X Ray ◽  

2009 ◽  
Vol 34 (12) ◽  
pp. 1768 ◽  
Author(s):  
Wojciech Roseker ◽  
Hermann Franz ◽  
Horst Schulte-Schrepping ◽  
Anita Ehnes ◽  
Olaf Leupold ◽  
...  
Keyword(s):  

Author(s):  
Ralf K. Heilmann ◽  
Alexander R. Bruccoleri ◽  
Jungki Song ◽  
Mark L. Schattenburg ◽  
Randall K. Smith ◽  
...  
Keyword(s):  
X Ray ◽  

2018 ◽  
Vol 25 (6) ◽  
pp. 1673-1682 ◽  
Author(s):  
Adam S. Hoffman ◽  
Joseph A. Singh ◽  
Stacey F. Bent ◽  
Simon R. Bare

In situ characterization of catalysts gives direct insight into the working state of the material. Here, the design and performance characteristics of a universal in situ synchrotron-compatible X-ray diffraction cell capable of operation at high temperature and high pressure, 1373 K, and 35 bar, respectively, are reported. Its performance is demonstrated by characterizing a cobalt-based catalyst used in a prototypical high-pressure catalytic reaction, the Fischer–Tropsch synthesis, using X-ray diffraction. Cobalt nanoparticles supported on silica were studied in situ during Fischer–Tropsch catalysis using syngas, H2 and CO, at 723 K and 20 bar. Post reaction, the Co nanoparticles were carburized at elevated pressure, demonstrating an increased rate of carburization compared with atmospheric studies.


2013 ◽  
Vol 46 (5) ◽  
pp. 1508-1512 ◽  
Author(s):  
Byron Freelon ◽  
Kamlesh Suthar ◽  
Jan Ilavsky

Coupling small-angle X-ray scattering (SAXS) and ultra-small-angle X-ray scattering (USAXS) provides a powerful system of techniques for determining the structural organization of nanostructured materials that exhibit a wide range of characteristic length scales. A new facility that combines high-energy (HE) SAXS and USAXS has been developed at the Advanced Photon Source (APS). The application of X-rays across a range of energies, from 10 to 50 keV, offers opportunities to probe structural behavior at the nano- and microscale. An X-ray setup that can characterize both soft matter or hard matter and high-Zsamples in the solid or solution forms is described. Recent upgrades to the Sector 15ID beamline allow an extension of the X-ray energy range and improved beam intensity. The function and performance of the dedicated USAXS/HE-SAXS ChemMatCARS-APS facility is described.


2017 ◽  
Vol 24 (6) ◽  
pp. 1113-1119 ◽  
Author(s):  
E. Nazaretski ◽  
H. Yan ◽  
K. Lauer ◽  
N. Bouet ◽  
X. Huang ◽  
...  

A hard X-ray scanning microscope installed at the Hard X-ray Nanoprobe beamline of the National Synchrotron Light Source II has been designed, constructed and commissioned. The microscope relies on a compact, high stiffness, low heat dissipation approach and utilizes two types of nanofocusing optics. It is capable of imaging with ∼15 nm × 15 nm spatial resolution using multilayer Laue lenses and 25 nm × 26 nm resolution using zone plates. Fluorescence, diffraction, absorption, differential phase contrast, ptychography and tomography are available as experimental techniques. The microscope is also equipped with a temperature regulation system which allows the temperature of a sample to be varied in the range between 90 K and 1000 K. The constructed instrument is open for general users and offers its capabilities to the material science, battery research and bioscience communities.


2008 ◽  
Vol 91 (2) ◽  
pp. 287-293 ◽  
Author(s):  
F.M. Böttcher ◽  
B. Manschwetus ◽  
H. Rottke ◽  
N. Zhavoronkov ◽  
Z. Ansari ◽  
...  

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