scholarly journals Characterization of pore and crystal structure of synthesized LiBOB with varying quality of raw materials as electrolyte for lithium-ion battery

2016 ◽  
Author(s):  
Titik Lestariningsih ◽  
Christin Rina Ratri ◽  
Etty Marty Wigayati ◽  
Qolby Sabrina
Keyword(s):  
Crystal Structure ◽  
Lithium Ion Battery ◽  
Raw Materials ◽  
Lithium Ion

The Synthesis and Characterization of Dispersant for LiFePO4 Lithium Ion Battery Slurry

2014 ◽  
Vol 997 ◽  
pp. 383-386
Author(s):  
Yun Ren ◽  
Bo Wang ◽  
Da Hai Zhang ◽  
Yu Hong Gao
Keyword(s):  
Acrylic Acid ◽  
Lithium Ion Battery ◽  
Orthogonal Experiment ◽  
Lithium Ion ◽  
Ethyl Acrylate ◽  
Graphitized Carbon Black ◽  
Optimum Amount ◽  
Coating Technology

The acrylic acid copolymerized with allyl polyethenoxy ether, to produce the dispersant for LiFePO4 lithium ion battery slurry. Taking the quality of acrylic acid as a benchmark, the orthogonal experiment was used to optimalize the burden: the acrylic acid (AA) is 100%, maleic anhydride (MA) is 10%,ethyl acrylate (EA) is 2%, sodium allylsulfonate (ALS) is 6%, allyl polyethenoxy ether (APEG1200) is 60%. The effect of dispersant concentration to slurry fluidity was studied,LiFePO4 content in pulp was 75%, graphitized carbon black was 0.75%,the optimum amount of the dispersant is 0.3wt% of the LiFePO4, the slurry initial viscosity is 1806 mPa.s and 2337 mPa.s after 90min which meet requirements for coating technology.

scholarly journals A Methodology Based on FT-IR Data Combined with Random Forest Model to Generate Spectralprints for the Characterization of High-Quality Vinegars

Foods ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 1411
Author(s):  
José Luis P. Calle ◽  
Marta Ferreiro-González ◽  
Ana Ruiz-Rodríguez ◽  
Gerardo F. Barbero ◽  
José Á. Álvarez ◽  
...  
Keyword(s):  
Random Forest ◽  
Raw Materials ◽  
Principal Component ◽  
Hierarchical Cluster ◽  
Raw Material ◽  
Support Vector ◽  
Protected Designation Of Origin ◽  
Ft Ir

Sherry wine vinegar is a Spanish gourmet product under Protected Designation of Origin (PDO). Before a vinegar can be labeled as Sherry vinegar, the product must meet certain requirements as established by its PDO, which, in this case, means that it has been produced following the traditional solera and criadera ageing system. The quality of the vinegar is determined by many factors such as the raw material, the acetification process or the aging system. For this reason, mainly producers, but also consumers, would benefit from the employment of effective analytical tools that allow precisely determining the origin and quality of vinegar. In the present study, a total of 48 Sherry vinegar samples manufactured from three different starting wines (Palomino Fino, Moscatel, and Pedro Ximénez wine) were analyzed by Fourier-transform infrared (FT-IR) spectroscopy. The spectroscopic data were combined with unsupervised exploratory techniques such as hierarchical cluster analysis (HCA) and principal component analysis (PCA), as well as other nonparametric supervised techniques, namely, support vector machine (SVM) and random forest (RF), for the characterization of the samples. The HCA and PCA results present a clear grouping trend of the vinegar samples according to their raw materials. SVM in combination with leave-one-out cross-validation (LOOCV) successfully classified 100% of the samples, according to the type of wine used for their production. The RF method allowed selecting the most important variables to develop the characteristic fingerprint (“spectralprint”) of the vinegar samples according to their starting wine. Furthermore, the RF model reached 100% accuracy for both LOOCV and out-of-bag (OOB) sets.

scholarly journals Fabrication and Characterization of Nylon 66/PAN Nanofibrous Film Used as Separator of Lithium-Ion Battery

Polymers ◽  
2021 ◽  
Vol 13 (12) ◽  
pp. 1984
Author(s):  
Yu-Hsun Nien ◽  
Chih-Ning Chang ◽  
Pao-Lin Chuang ◽  
Chun-Han Hsu ◽  
Jun-Lun Liao ◽  
...  
Keyword(s):  
Lithium Ion Battery ◽  
Lithium Batteries ◽  
Lithium Battery ◽  
Coulombic Efficiency ◽  
Electronic Devices ◽  
Lithium Ion ◽  
Nylon 66 ◽  
Excellent Electrochemical Performance ◽  
Fabrication And Characterization

In recent years, portable electronic devices have flourished, and the safety of lithium batteries has received increasing attention. In this study, nanofibers were prepared by electrospinning using different ratios of nylon 66/polyacrylonitrile (PAN), and their properties were studied and compared with commercial PP separators. The experimental results show that the addition of PAN in nylon 66/PAN nanofibrous film used as separator of lithium-ion battery can enhance the porosity up to 85%. There is also no significant shrinkage in the shrinkage test, and the thermal dimensional stability is good. When the Li/LiFePO4 lithium battery is prepared by nylon 66/PAN nanofibrous film used as separator, the capacitor can be maintained at 140 mAhg−1 after 20 cycles at 0.1 C, and the coulombic efficiency is still maintained at 99%, which has excellent electrochemical performance.

scholarly journals Making and Characterization of Limnpo4 Using Solid State Reaction Method for Lithium Ion Battery Cathodes

2019 ◽  
pp. 583-588
Author(s):  
Adelyna Oktavia ◽  
Kurnia Sembiring ◽  
Slamet Priyono
Keyword(s):  
Solid State ◽  
Lithium Ion Battery ◽  
Lithium Ion ◽  
Solid State Reaction Method ◽  
Raw Material ◽  
X Ray Diffraction ◽  
Solid State Method ◽  
X Ray ◽  
General Investigation

Hospho-material of olivine, LiMnPO4 identified as promising for cathode material generation next Lithium-ion battery and has been successfully synthesized by solid-state method with Li2Co3, 2MnO2, 2NH4H2PO4 as raw material. The influence of initial concentration of precursors at kalsinasi temperatures (400-800 ° C) flows with nitrogen. The purity and composition phase verified by x-ray diffraction analysis (XRD), scanning electron microscopy (SEM), spectroscopy, energy Dispersive x-ray Analysis (EDS), Raman spectra. General investigation shows that there is a correlation between the concentration of precursors, the temperature and the temperature of sintering kalsinasi that can be exploited to design lithium-ion next generation.

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