scholarly journals Strength of polycrystalline niobium from high-pressure x-ray diffraction data: A comparison of results from line-width and line-shift analyses

2015 ◽  
Vol 118 (6) ◽  
pp. 065903 ◽  
Author(s):  
Anil K. Singh ◽  
Hanns-Peter Liermann
Keyword(s):  
High Pressure ◽  
Line Width ◽  
Diffraction Data ◽  
Line Shift ◽  
X Ray Diffraction ◽  
X Ray ◽  
Comparison Of Results

scholarly journals High-pressure synthesis and crystal structure of the mixed-cation borate Ga4In4B15O33(OH)3

2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Mixed Cation ◽  
High Pressure High Temperature ◽  
Pressure Synthesis

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.

Crystalline structure of the TiO2 II high-pressure phase at 293, 223, and 133 K according to single-crystal x-ray diffraction data

2007 ◽  
Vol 52 (4) ◽  
pp. 195-199 ◽  
Author(s):  
S. K. Filatov ◽  
N. A. Bendeliani ◽  
B. Albert ◽  
J. Kopf ◽  
T. I. Dyuzheva ◽  
...  
Keyword(s):  
High Pressure ◽  
Single Crystal ◽  
Crystalline Structure ◽  
Diffraction Data ◽  
High Pressure Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Pressure Phase

High-pressure syntheses and crystal structures of orthorhombic DyGaO3 and trigonal GaBO3

2015 ◽  
Vol 70 (4) ◽  
pp. 207-214 ◽  
Author(s):  
Daniela Vitzthum ◽  
Stefanie A. Hering ◽  
Lukas Perfler ◽  
Hubert Huppertz
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Single Crystal ◽  
Crystal Structures ◽  
Diffraction Data ◽  
Room Temperature ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
High Pressure High Temperature

AbstractOrthorhombic dysprosium orthogallate DyGaO3 and trigonal gallium orthoborate GaBO3 were synthesized in a Walker-type multianvil apparatus under high-pressure/high-temperature conditions of 8.5 GPa/1350 °C and 8 GPa/700 °C, respectively. Both crystal structures could be determined by single-crystal X-ray diffraction data collected at room temperature. The orthorhombic dysprosium orthogallate crystallizes in the space group Pnma (Z = 4) with the parameters a = 552.6(2), b = 754.5(2), c = 527.7(2) pm, V = 0.22002(8) nm3, R1 = 0.0309, and wR2 = 0.0662 (all data) and the trigonal compound GaBO3 in the space group R3̅c (Z = 6) with the parameters a = 457.10(6), c = 1419.2(3) pm, V = 0.25681(7) nm3, R1 = 0.0147, and wR2 = 0.0356 (all data).

scholarly journals Synthesis and Crystal Structure of the Praseodymium Orthoborate λ -PrBO3

2010 ◽  
Vol 65 (10) ◽  
pp. 1206-1212 ◽  
Author(s):  
Almut Haberer ◽  
Reinhard Kaindl ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
Title Compound ◽  
Room Temperature ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
High Pressure High Temperature

The praseodymium orthoborate λ -PrBO3 was synthesized from Pr6O11, B2O3, and PrF3 under high-pressure / high-temperature conditions of 3 GPa and 800 °C in a Walker-type multianvil apparatus. The crystal structure was determined on the basis of single-crystal X-ray diffraction data, collected at room temperature. The title compound crystallizes in the orthorhombic aragonite-type structure, space group Pnma, with the lattice parameters a = 577.1(2), b = 506.7(2), c = 813.3(2) pm, and V = 0.2378(2) nm3, with R1 = 0.0400 and wR2 = 0.0495 (all data). Within the trigonal-planar BO3 groups, the average B-O distance is 137.2 pm. The praseodymium atoms are ninefold coordinated by oxygen atoms.

Notizen: Zur Kristallstruktur von SrPbO3 / The Crystal Structure of SrPbO3

1975 ◽  
Vol 30 (3-4) ◽  
pp. 277-278 ◽  
Author(s):  
Hans-L. Keller ◽  
Karl-H. Meier ◽  
Hk. Müller-Buschbaum
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Single Crystal ◽  
Single Crystals ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
Pressure Synthesis ◽  
Group D

Single crystals of SrPbO3 could be prepared by oxygen-high-pressure-synthesis (PO2 > 3500 at, t = 450°C). Single crystal X-ray diffraction data confirm the space group D2h16-Pnma. SrPbO3 belongs to the orthorhombic distorted Perowskit type with a = 5.964, b = 8.320, c = 5.860 Å. The atomic positions were refined.

scholarly journals Strength of polycrystalline coarse-grained platinum to 330GPa and of nanocrystalline platinum to 70GPa from high-pressure x-ray diffraction data

2008 ◽  
Vol 103 (6) ◽  
pp. 063524 ◽  
Author(s):  
Anil K. Singh ◽  
Hanns-Peter Liermann ◽  
Yuichi Akahama ◽  
Surendra K. Saxena ◽  
Eduardo Menéndez-Proupin
Keyword(s):  
High Pressure ◽  
Diffraction Data ◽  
Coarse Grained ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals High-Pressure Syntheses, Crystal Structures, And Thermal Behaviour Of β-Re(Bo2)3 (Re = Nd, Sm, Gd)

2007 ◽  
Vol 62 (6) ◽  
pp. 765-770 ◽  
Author(s):  
Holger Emme ◽  
Gunter Heymann ◽  
Almut Haberer ◽  
Hubert Huppertz
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Single Crystal ◽  
Crystal Structures ◽  
Thermal Behaviour ◽  
Diffraction Data ◽  
Ambient Pressure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Temperature Conditions

The compounds β -RE(BO2)3 [RE = Nd (neodymium meta-borate), Sm (samarium meta-borate) and Gd (gadolinium meta-borate)] were synthesized under high-pressure and high-temperature conditions in a Walker-type multianvil apparatus at 3.5 GPa (Nd), 7.5 GPa (Sm, Gd) and 1050 °C. The crystal structures were determined by single crystal X-ray diffraction data collected at r. t. (Sm, Gd) and at−73°C (Nd), respectively. The structures are isotypic with the already known ambient-pressure phases β -RE(BO2)3 (RE = (Tb, Dy) and the high-pressure phases β -RE(BO2)3 (RE = Ho-Lu)

Powder X-ray diffraction data of a new polymorph of HfMo2O8

2003 ◽  
Vol 18 (2) ◽  
pp. 147-149 ◽  
Author(s):  
S. N. Achary ◽  
G. D. Mukherjee ◽  
A. K. Tyagi ◽  
B. K. Godwal
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
Unit Cell ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Lattice Space ◽  
Monoclinic Lattice

A new polymorph of HfMo2O8 (β-form) is synthesized under high pressure and high temperature conditions. The powder X-ray diffraction (XRD) data could be explained based on a monoclinic lattice (Space Group: C2/c No. 15) with the unit cell parameters as: a=11.415(3), b=7.906(2), c=7.438(2) Å and β=122.37(2)°, V=566.9(2) Å3. The detailed powder XRD data and analysis are reported herein.

Analysis of high-energy x-ray diffraction data at high pressure: the case of vitreous As2O3at 32 GPa

2007 ◽  
Vol 19 (41) ◽  
pp. 415103 ◽  
Author(s):  
Q Mei ◽  
C J Benmore ◽  
E Soignard ◽  
S Amin ◽  
J L Yarger
Keyword(s):  
High Pressure ◽  
Diffraction Data ◽  
High Energy ◽  
X Ray Diffraction ◽  
X Ray
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