Effect of calcination temperature on microstructure and magnetic properties of Ni0.5Zn0.25Cu0.25 Fe2O4 nanoparticles synthesized by sol-gel method

2014 ◽  
Author(s):  
Prengki Pransisco ◽  
Afza Shafie ◽  
Beh Hoe Guan
Keyword(s):  
Magnetic Properties ◽  
Calcination Temperature ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method ◽  
Fe2o4 Nanoparticles ◽  
Microstructure And Magnetic Properties

Structural and Magnetic Properties of Ni0.5Zn0.5Fe2O4 Synthesized through the Sol-Gel Method

2014 ◽  
Vol 664 ◽  
pp. 75-79
Author(s):  
Beh Hoe Guan ◽  
Muhammad Hanif Zahari ◽  
Lee Kean Chuan
Keyword(s):  
Magnetic Properties ◽  
Calcination Temperature ◽  
Sol Gel ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Calcination Temperatures ◽  
Zn Ferrite

This study investigates the influence of calcination temperatures on the magnetic properties of Ni0.5Zn0.5Fe2O4(Ni-Zn) ferrites.Ni-Zn ferrite with the chemical formula Ni0.5Zn0.5Fe2O4was prepared from their respective nitrate salts through the sol-gel method. The resulting ferrites were characterized using X-ray diffraction (XRD), field emission scanning electron microscope (FESEM) and vibrating sample magnetometer (VSM). Single phased Ni0.5Zn0.5Fe2O4 was obtained at all calcination temperatures.FESEM Micrographs reveals an increase in the grain size with the increase of the calcination temperature. Consequently, the magnetic saturation of the samples were found to increase with each increase in the calcination temperature where the highest value obtained is 70.58 emu/g for the samples calcined at 1000°C.

Investigation of Nanostructure and Magnetic Properties of Nanocrystalline NiZnCu Ferrites Synthesized by Sol-Gel Method

2015 ◽  
Vol 754-755 ◽  
pp. 1169-1174 ◽  
Author(s):  
Prengki Pransisco ◽  
Afza Shafie ◽  
Beh Hoe Guan
Keyword(s):  
Grain Size ◽  
Magnetic Properties ◽  
Crystallite Size ◽  
Calcination Temperature ◽  
Sol Gel ◽  
Thermo Gravimetric Analysis ◽  
Variable Pressure ◽  
Gravimetric Analysis ◽  
Gel Method ◽  
Sol Gel Method

Nanocrystalline material of ferrites with composition Ni0.5Zn0.35Cu0.15Fe2O4was successfully synthesized by sol-gel method. This paper investigates nanostructure and magnetic properties of nanocrystaline material Ni0.5Zn0.35Cu0.15Fe2O4.Crystallite size, intensity,d-spacing and lattice parameters of material were investigated by using X-Ray diffractometer (XRD). While nanostructure, size, shape, surface morphology and topography of Ni0.5Zn0.35Cu0.15Fe2O4were examined by variable pressure field emission scanning electron microscope (VP-FESEM) SUPRA 55VP. Magnetic properties was investigated using vibrating sample magnetometer (VSM). According to thermo gravimetric analysis (TGA) result, it was found that after temperature 600oC there is no more weight loss detected and it was considered as minimum calcination temperature. XRD result shows that the samples is in single-phase cubic spinel structure. Crystallite size of the material is in range of 42.3-163.7nm. Highest intensity was 88.89 arb.units at highest calcination temperature 900oC. The value of d-spacing and FWHM decrease with increasing calcination temperature. Lattice paramenters decrease in the range of 8.4040-8.2458oA. VP-FESEM analysis shows that grain size increase by increasing calcination temperature. Grain size of the material is in the range of 47.6-506.9nm with cubic structure of the Ni0.5Zn0.35Cu0.15Fe2O4.VSM result shows that the highest value of magnetic saturation was at 152.8emu/g. The best value of coercive force (Hc) was in 31.8Oe and magnetic remanence (Mr) was in 2.6emu/g.

Annealing Effects on the Physical and Magnetic Properties of Tb1.5Y1.5Fe5O12 Films Nanoparticles Prepared by Sol-Gel Method

2013 ◽  
Vol 756 ◽  
pp. 91-98 ◽  
Author(s):  
Ftema W. Aldbea ◽  
Noor Bahyah Ibrahim ◽  
Mustafa Hj. Abdullah
Keyword(s):  
Particle Size ◽  
Magnetic Properties ◽  
Annealing Temperature ◽  
Quartz Substrate ◽  
Sol Gel ◽  
Lattice Parameter ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Iron Garnet

Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900 °C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900°C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-raySpectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealingtemperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. Normal 0 21 false false false MS X-NONE X-NONE MicrosoftInternetExplorer4 Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900°C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900 °C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-ray Spectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealing temperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. st1\:*{behavior:url(#ieooui) } /* Style Definitions */ table.MsoNormalTable {mso-style-name:"Table Normal"; mso-tstyle-rowband-size:0; mso-tstyle-colband-size:0; mso-style-noshow:yes; mso-style-priority:99; mso-style-qformat:yes; mso-style-parent:""; mso-padding-alt:0cm 5.4pt 0cm 5.4pt; mso-para-margin:0cm; mso-para-margin-bottom:.0001pt; mso-pagination:widow-orphan; font-size:11.0pt; font-family:"Calibri","sans-serif"; mso-ascii-font-family:Calibri; mso-ascii-theme-font:minor-latin; mso-fareast-font-family:"Times New Roman"; mso-fareast-theme-font:minor-fareast; mso-hansi-font-family:Calibri; mso-hansi-theme-font:minor-latin; mso-bidi-font-family:"Times New Roman"; mso-bidi-theme-font:minor-bidi;}

Magnetic properties of Fe and Co codoped SnO2 prepared by sol-gel method

2011 ◽  
Vol 110 (8) ◽  
pp. 083901 ◽  
Author(s):  
K. Nomura ◽  
J. Okabayashi ◽  
K. Okamura ◽  
Y. Yamada
Keyword(s):  
Magnetic Properties ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method

Magnetic Properties of Bulk Zn0.95-XMnXFe0.05O2 Prepared by Sol-Gel Method and Subsequent Hot Pressing

2011 ◽  
Vol 268-270 ◽  
pp. 356-359 ◽  
Author(s):  
Wen Song Lin ◽  
C. H. Wen ◽  
Liang He
Keyword(s):  
Magnetic Properties ◽  
Photoelectron Spectroscopy ◽  
Raw Materials ◽  
Sol Gel ◽  
Secondary Phase ◽  
X Ray Diffraction ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Doped Zno

Mn, Fe doped ZnO powders (Zn0.95-xMnxFe0.05O2, x≤0.05) were synthesized by an ameliorated sol-gel method, using Zn(CH3COO)2, Mn(CH3COO)2and FeCl2as the raw materials, with the addition of vitamin C as a kind of chemical reducer. The resulting powder was subsequently compacted under pressure of 10 MPa at the temperature of 873K in vacuum. The crystal structure and magnetic properties of Zn0.95-xMnxFe0.05O2powder and bulk samples have been investigated by X-ray diffraction (XRD) and vibrating sample magnetometer (VSM). X-ray photoelectron spectroscopy (XPS) was used to study chemical valence of manganese, iron and zinc in the samples. The x-ray diffraction (XRD) results showed that Zn0.95-xMnxFe0.05O (x≤0.05) samples were single phase with the ZnO-like wurtzite structure. No secondary phase was found in the XRD spectrum. X-ray photoelectron spectroscopy (XPS) showed that Fe and Mn existed in Zn0.95-xMnxFe0.05O2samples in Fe2+and Mn2+states. The results of VSM experiment proved the room temperature ferromagnetic properties (RTFP) of Mn, Fe co-doped ZnO samples.

Structural and Magnetic Properties of CoAl0.1Fe1.9O4 Thin Films Prepared by a Sol-Gel Method

2002 ◽  
Vol 189 (3) ◽  
pp. 883-887
Author(s):  
Sam Jin Kim ◽  
Woo Chul Kim ◽  
In Bo Shim ◽  
Chul Sung Kim ◽  
Seung Wha Lee
Keyword(s):  
Thin Films ◽  
Magnetic Properties ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method ◽  
Structural And Magnetic Properties

Magnetic properties of NiCuZn ferrite thin films prepared by the sol-gel method

2007 ◽  
Vol 22 (3) ◽  
pp. 506-509 ◽  
Author(s):  
Feng Liu ◽  
Tianling Ren ◽  
Chen Yang ◽  
Litian Liu ◽  
Jun Yu
Keyword(s):  
Thin Films ◽  
Magnetic Properties ◽  
Sol Gel ◽  
Gel Method ◽  
Sol Gel Method ◽  
Nicuzn Ferrite ◽  
Ferrite Thin Films
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