A microscopic model of the Tian-Calvet microcalorimeter, cell design for a faster response, and measurement by a continuous procedure

2014 ◽  
Vol 85 (3) ◽  
pp. 034101 ◽  
Author(s):  
Y. Kobayashi ◽  
F. Wang ◽  
Q. X. Li ◽  
D. Z. Wang
Author(s):  
J. R. Sellar ◽  
J. M. Cowley

Current interest in high voltage electron microscopy, especially in the scanning mode, has prompted the development of a method for determining the contrast and resolution of images of specimens in controlled-atmosphere stages or open to the air, hydrated biological specimens being a good example. Such a method would be of use in the prediction of microscope performance and in the subsequent optimization of environmental cell design for given circumstances of accelerating voltage, cell gas pressure and constitution, and desired resolution.Fig. 1 depicts the alfresco cell of a focussed scanning transmission microscope with a layer of gas L (and possibly a thin window W) between the objective O and specimen T. Using the principle of reciprocity, it may be considered optically equivalent to a conventional transmission electron microscope, if the beams were reversed. The layer of gas or solid material after the specimen in the STEM or before the specimen in TEM has no great effect on resolution or contrast and so is ignored here.


1983 ◽  
Vol 44 (C3) ◽  
pp. C3-1195-C3-1199
Author(s):  
H. Anzai ◽  
T. Moriya ◽  
K. Nozaki ◽  
T. Ukachi ◽  
G. Saito

2014 ◽  
Vol 59 (11) ◽  
pp. 1065-1077 ◽  
Author(s):  
A.V. Nesterov ◽  
◽  
V.S. Vasilevsky ◽  
T.P. Kovalenko ◽  
◽  
...  

2019 ◽  
Vol 64 (12) ◽  
pp. 1274-1280
Author(s):  
L. P. Ogorodova ◽  
Yu. D. Gritsenko ◽  
M. F. Vigasina ◽  
A. Yu. Bychkov ◽  
D. A. Ksenofontov ◽  
...  

A thermochemical study of natural calcium and magnesium orthosilicate ─ monticellite (Ca1.00Mg0.95)[SiO4] (Khabarovsk Territory, Russia) was carried out on the Tian-Calvet microcalorimeter. The enthalpy of formation from the elements fHоel(298.15 K) = -2238.4 4.5 kJ / mol was determined by the method of high-temperature melt solution calorimetry. The enthalpy and Gibbs energy of formation of monticellite of the theoretical composition of CaMg[SiO4] are calculated: fH0el(298.15 K) = -2248.4 4.5 kJ/mol and fG0el(298.15 K) = -2130.5 4.5 kJ/mol.


2019 ◽  
Vol 31 (7) ◽  
pp. 541-544
Author(s):  
Ming Dong ◽  
Chuantao Zheng ◽  
Yu Zhang ◽  
Yiding Wang ◽  
Frank K. Tittel

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