scholarly journals A two-axis goniometer for low-temperature nuclear magnetic resonance measurements on single crystals

2012 ◽  
Vol 83 (9) ◽  
pp. 093901 ◽  
Author(s):  
T. Shiroka ◽  
F. Casola ◽  
J. Mesot ◽  
W. Bachmann ◽  
H.-R. Ott
1978 ◽  
Vol 56 (17) ◽  
pp. 2253-2258 ◽  
Author(s):  
Morley Brownstein ◽  
Ronald J Gillespie ◽  
John P. Krasznai

The reactions of IOF5 with SbF5 and with AsF5 have been investigated at low temperature by 19F nmr and Raman spectroscopy. It was found that SbF5 forms labile 1:1 and 2:1 complexes whereas AsF5 forms only a 1:1 complex. The IOF5 is bound through its oxygen atom to the Lewis acids AsF5, SbF5, or (SbF5)2.


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