The photoelectron spectrum of HCl and DCl studied with ultraviolet excitation, high resolution x‐ray excitation, and synchrotron radiation excitation: Isotope effects on line profiles

1988 ◽  
Vol 89 (12) ◽  
pp. 7193-7200 ◽  
Author(s):  
S. Svensson ◽  
L. Karlsson ◽  
P. Baltzer ◽  
B. Wannberg ◽  
U. Gelius ◽  
...  
2007 ◽  
Vol 130 ◽  
pp. 7-14 ◽  
Author(s):  
Andrew N. Fitch

The highly-collimated, intense X-rays produced by a synchrotron radiation source can be harnessed to build high-resolution powder diffraction instruments with a wide variety of applications. The general advantages of using synchrotron radiation for powder diffraction are discussed and illustrated with reference to the structural characterisation of crystalline materials, atomic PDF analysis, in-situ and high-throughput studies where the structure is evolving between successive scans, and the measurement of residual strain in engineering components.


1989 ◽  
Vol 28 (Part 1, No. 2) ◽  
pp. 263-266 ◽  
Author(s):  
Tatsumi Hirano ◽  
Katsuhisa Usami

2006 ◽  
Vol 252 (15) ◽  
pp. 5602-5606 ◽  
Author(s):  
J.J. Kim ◽  
E. Ikenaga ◽  
M. Kobata ◽  
A. Takeuchi ◽  
M. Awaji ◽  
...  

1990 ◽  
Vol 23 (5) ◽  
pp. 351-354
Author(s):  
D. Hohlwein ◽  
J. D. Axe

A photographic Weissenberg camera has been constructed which can be mounted on the 2θ arm of a four-circle diffractometer. At a distance of 0.5 m from the sample the 2θ resolution for a 100 μm crystal is 0.2 mrad (0.01°), allowing a high-resolution mapping of reciprocal space at a synchrotron source in an efficient way. As sample experimental results, a study is presented of the streak system around the 111 reflection of a perfect germanium crystal and the detection of a minute phase transformation in a single-powder grain of a high-Tc superconductor.


2010 ◽  
Author(s):  
Jianqi Sun ◽  
Ping Liu ◽  
Xiaoxia Liu ◽  
Xiang Gu ◽  
Jun Zhao ◽  
...  

1957 ◽  
Vol 1 ◽  
pp. 193-206 ◽  
Author(s):  
William J. Campbell ◽  
Melvin Leon ◽  
John Thatcher

AbstractAn investigation was undertaken by the Bureau of Mines at College Park, Md., to determine the effect of various combinations of collimators, analyzing crystals and detectors on line intensities, line-to-backgrouhd ratios, and spectral resolution. The research showed that line broadening due to mosaic crystal surfaces was greatly reduced and line splitting from faults was eliminatedby the use of two fine collimators (0.005 inch, spacing, 4 inch length). Line intensities were reduced, but lineto- background ratios arid line profiles were substantially improved with double collimators. Pulse height discrimination resulted in marked improvement in the line-to-background ratio in the long-wave length region, 2 to 10 A, but was much less effective for shorter wave lengths.


2003 ◽  
Vol 17 (04n06) ◽  
pp. 836-841 ◽  
Author(s):  
G. CAMPI ◽  
D. DI CASTRO ◽  
C. DELL'OMO ◽  
S. AGRESTINI ◽  
N. L. SAINI ◽  
...  

We have investigated charge ordering in an oxygen doped La 2 CuO 4.1 crystal by high resolution x-ray diffraction using synchrotron radiation. Thanks to the high brilliance synchrotron radiation it has been possible to record a large number of weak superstructure spots due to charge ordering around the main peaks of the average structure. A study of the charge modulations with stage 3.5, and their behaviour as a function of the temperature and the intensity of the x-ray incident flux is reported. We are able to distinguish a microscopic decomposition in; 1) a stable domain, due to charges self trapped into a crystal of static ordered strings of finite length (~ 145 Å) and; 2) bubbles of 'superstripes' showing, as a function of photon dose, a decreasing coherence length at T = 220 K.


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