scholarly journals The influence of particle morphology on the dynamic densification of metal powders

Author(s):  
Daniel E. Eakins ◽  
David James Chapman
2021 ◽  
Vol 2021 (9) ◽  
pp. 3-7
Author(s):  
Dmitriy Kostin ◽  
Aleksandr Amosov ◽  
Anatoliy Samboruk ◽  
Bogdan Chernyshev ◽  
Anton Kamynin

A comparison is made of the characteristics of metal powders of a hard magnetic alloy produced by centrifugal spraying and gas atomization. Comparative studies of particle morphology and particle size distribution of powders are presented in order to determine them.


2007 ◽  
Vol 539-543 ◽  
pp. 2782-2786 ◽  
Author(s):  
Jong Gwan Ahn ◽  
Dong Jin Kim ◽  
Jae Ryeong Lee ◽  
H.S. Jung ◽  
Byoung Gyu Kim

The synthesis of spherical silver powders by chemical reduction method was investigated. Conductive metal pastes to have good properties in adhesion, stability, and conductivity, it is very important to control the purity, size, and shape of metal particles. In the present study, proper methods to control the properties of micron sized metal powders for conductive pastes are investigated. Chemical reduction method in aqueous solution was adapted to produce silver powder. The effects of reaction time, concentration of reductant and additives, and stirring speed were investigated, in experimental. Fine spherical silver powder of 0.5 to 3 ㎛ were synthesized from silver nitrate solution with hydroquinone as a reducing additive by liquid phase method, and some variables and reaction mechanism in conjunction with the particle morphology and size were studied.


Author(s):  
Dmitriy Kostin ◽  
Aleksandr Amosov ◽  
Anatoliy Samboruk ◽  
Bogdan Chernyshev ◽  
Anton Kamynin

A comparison is made of the characteristics of metal powders of a hard magnetic alloy produced by centrifugal spraying and gas atomization. Comparative studies of particle morphology and particle size distribution of powders are presented in order to determine them.


Author(s):  
O. L. Shaffer ◽  
M.S. El-Aasser ◽  
C. L. Zhao ◽  
M. A. Winnik ◽  
R. R. Shivers

Transmission electron microscopy is an important approach to the characterization of the morphology of multiphase latices. Various sample preparation techniques have been applied to multiphase latices such as OsO4, RuO4 and CsOH stains to distinguish the polymer phases or domains. Radiation damage by an electron beam of latices imbedded in ice has also been used as a technique to study particle morphology. Further studies have been developed in the use of freeze-fracture and the effect of differential radiation damage at liquid nitrogen temperatures of the latex particles embedded in ice and not embedded.Two different series of two-stage latices were prepared with (1) a poly(methyl methacrylate) (PMMA) seed and poly(styrene) (PS) second stage; (2) a PS seed and PMMA second stage. Both series have varying amounts of second-stage monomer which was added to the seed latex semicontinuously. A drop of diluted latex was placed on a 200-mesh Formvar-carbon coated copper grid.


TAPPI Journal ◽  
2015 ◽  
Vol 14 (9) ◽  
pp. 565-576 ◽  
Author(s):  
YUCHENG PENG ◽  
DOUGLAS J. GARDNER

Understanding the surface properties of cellulose materials is important for proper commercial applications. The effect of particle size, particle morphology, and hydroxyl number on the surface energy of three microcrystalline cellulose (MCC) preparations and one nanofibrillated cellulose (NFC) preparation were investigated using inverse gas chromatography at column temperatures ranging from 30ºC to 60ºC. The mean particle sizes for the three MCC samples and the NFC sample were 120.1, 62.3, 13.9, and 9.3 μm. The corresponding dispersion components of surface energy at 30°C were 55.7 ± 0.1, 59.7 ± 1.3, 71.7 ± 1.0, and 57.4 ± 0.3 mJ/m2. MCC samples are agglomerates of small individual cellulose particles. The different particle sizes and morphologies of the three MCC samples resulted in various hydroxyl numbers, which in turn affected their dispersion component of surface energy. Cellulose samples exhibiting a higher hydroxyl number have a higher dispersion component of surface energy. The dispersion component of surface energy of all the cellulose samples decreased linearly with increasing temperature. MCC samples with larger agglomerates had a lower temperature coefficient of dispersion component of surface energy.


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