scholarly journals Non destructive neutron diffraction measurements of cavities, inhomogeneities, and residual strain in bronzes of Ghiberti’s relief from the Gates of Paradise

2011 ◽  
Vol 109 (6) ◽  
pp. 064908 ◽  
Author(s):  
G. Festa ◽  
R. Senesi ◽  
M. Alessandroni ◽  
C. Andreani ◽  
G. Vitali ◽  
...  
1988 ◽  
Vol 142 ◽  
Author(s):  
John H. Root ◽  
James D. Sullivan

AbstractNeutron diffraction is a powerful probe of the properties of condensed matter. In recent years neutron diffraction has been applied to the non-destructive evaluation of mechanical characteristics of engineering components. This paper presents examples of applications to ceramic composites including the measurement of position dependence of residual strain, grain size and minority phase concentration. In addition, an example of volume-averaged crystallographic texture is presented.


2018 ◽  
Vol 144 ◽  
pp. 387-392 ◽  
Author(s):  
Francesco Grazzi ◽  
Antonio Brunetti ◽  
Antonella Scherillo ◽  
Marco E. Minoja ◽  
Gianfranca Salis ◽  
...  

2018 ◽  
Author(s):  
Tomohiro Ikeda ◽  
Jeffrey Bunn ◽  
Chris Fancher ◽  
Alan Seid ◽  
Ryuta Motani ◽  
...  

2020 ◽  
Vol 10 (11) ◽  
pp. 3781 ◽  
Author(s):  
Rodica Mariana Ion ◽  
Bulat A. Bakirov ◽  
Sergey E. Kichanov ◽  
Denis P. Kozlenko ◽  
Alexander V. Belushkin ◽  
...  

The color characteristics, vibration spectra, phase and mineral composition, internal structural organization of several fragments of the ancient Roman mosaics from the Roman Mosaic Museum, Constanta, Romania were studied by non-destructive (Chromatic analysis, Neutron Diffraction, Neutron Tomography) and micro-invasive techniques (Optical Microscopy, X-ray Diffraction, Field Emission Scanning Electron Microscopy–Energy Dispersive X-ray Spectroscopy, Raman Spectroscopy, Wavelength Dispersion X-ray Fluorescence). These investigations were performed in order to characterize the original Roman mosaic fragments. The major and minor phase components of the studied mosaic fragments were determined, the crystal structure of the main phases was analyzed, and their three-dimension spatial arrangement was reconstructed. The similar composition of the major phases of all mosaic fragments can indicate a generic recipe for making mosaic elements, but minor phases were presumably added for coloring of mosaic pieces. Some degradation areas inside the volume of the mosaic fragments were found by means of neutron diffraction and neutron tomography methods. These degradation areas are probably related to the formation of iron hydroxides during chemical interactions of mosaic fragments with the sea and urban polluted atmosphere.


2010 ◽  
Vol 638-642 ◽  
pp. 748-753
Author(s):  
Abdelilah Benmarouane ◽  
Helene Citterio-Bigot ◽  
Guillaume Geandier ◽  
T. Hansen ◽  
Pierre Millet ◽  
...  

The quantitative evaluation of the preferential orientation of crystallites by the synchrotron and neutron diffraction techniques during regeneration at the interface with implant gives a good prediction of the mechanical properties of the bone. During the process of bone healing after implantation, the speed and quality of regeneration is affected by the nature of the implant surface. Titanium alloy (Ti-Al-4V) is currently coating with the hydroxyapatite (HAp), Ca10(PO4)6 (OH)2, in order to obtain a stable and functional direct connection between bone and implant. At the interface implant-bone, the new bone reconstituted after implantation must have the same mechanical properties of bone in order to accept the implant. Therefore, it is necessary to study by means of two non destructive techniques: neutron diffraction and synchrotron radiation, the crystal growth and texture of this new bone crystals reconstituted at the interface.


Author(s):  
Masaru Ogawa

In order to assure structural integrity for operating welded structures, it is necessary to evaluate crack growth rate and crack propagation direction for each observed crack non-destructively. Here, three dimensional (3D) welding residual stresses must be evaluated to predict crack propagation. Today, X-ray diffraction is used and the ultrasonic method has been proposed as non-destructive method to measure residual stresses. However, it is impossible to determine residual stress distributions in the thickness direction. Although residual stresses through a depth of several tens of millimeters can be evaluated non-destructively by neutron diffraction, it cannot be used as an on-site measurement technique. This is because neutron diffraction is only available in special irradiation facilities. Author pays attention to the bead flush method based on the eigenstrain methodology. In this method, 3D welding residual stresses are calculated by an elastic Finite Element Method (FEM) analysis from eigenstrains which are evaluated by an inverse analysis from released strains by strain gauges in the removal of the reinforcement of the weld. Here, the removal of the excess metal can be regarded as non-destructive treatment because toe of weld which may become crack starters can be eliminated. The effectiveness of the method has been proven for welded plates and pipes even with relatively lower bead height. In actual measurements, stress evaluation accuracy becomes poorer because measured values of strain gauges are affected by processing strains on the machined surface. In the previous studies, the author has developed the bead flush method that is free from the influence of the affecting strains by using residual strains on surface by X-ray diffraction. However, stress evaluation accuracy is not good enough because of relatively poor measurement accuracy of X-ray diffraction. In this study, a method to improve the estimation accuracy of residual stresses in this method is formulated, and it is shown numerically that inner welding residual stresses can be estimated accurately from the residual strains measured by X-ray diffraction.


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