Instrumental Characterization Of Coir PITH By XRD, FTIR and SEM After Radium Adsorption From Aqueous Solution Under The Presence Of Humic Acids

2010 ◽  
Author(s):  
Zalina Laili ◽  
Muhamat Omar ◽  
Muhamad Samudi Yasir ◽  
Mohd Zaidi Ibrahim ◽  
Mohd Yusri Yahaya ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Humic Acids ◽  
Coir Pith

scholarly journals Characterization of Soil Organic Matter Individual Fractions (Fulvic Acids, Humic Acids, and Humins) by Spectroscopic and Electrochemical Techniques in Agricultural Soils

Agronomy ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 1067
Author(s):  
Aleksandra Ukalska-Jaruga ◽  
Romualda Bejger ◽  
Guillaume Debaene ◽  
Bożena Smreczak
Keyword(s):  
Molecular Weight ◽  
Organic Matter ◽  
Soil Organic Matter ◽  
Humic Substances ◽  
Humic Acids ◽  
Agricultural Soils ◽  
Fulvic Acids ◽  
Sorption Properties ◽  
Aliphatic Chains

The objective of this paper was to investigate the molecular characterization of soil organic matter fractions (humic substances (HS): fulvic acids-FAs, humic acids-HAs, and humins-HNs), which are the most reactive soil components. A wide spectrum of spectroscopic (UV–VIS and VIS–nearIR), as well as electrochemical (zeta potential, particle size diameter, and polydispersity index), methods were applied to find the relevant differences in the behavior, formation, composition, and sorption properties of HS fractions derived from various soils. Soil material (n = 30) used for the study were sampled from the surface layer (0–30 cm) of agricultural soils. FAs and HAs were isolated by sequential extraction in alkaline and acidic solutions, according to the International Humic Substances Society method, while HNs was determined in the soil residue (after FAs and HAs extraction) by mineral fraction digestion using a 0.1M HCL/0.3M HF mixture and DMSO. Our study showed that significant differences in the molecular structures of FAs, Has, and HNs occurred. Optical analysis confirmed the lower molecular weight of FAs with high amount of lignin-like compounds and the higher weighted aliphatic–aromatic structure of HAs. The HNs were characterized by a very pronounced and strong condensed structure associated with the highest molecular weight. HAs and HNs molecules exhibited an abundance of acidic, phenolic, and amine functional groups at the aromatic ring and aliphatic chains, while FAs mainly showed the presence of methyl, methylene, ethenyl, and carboxyl reactive groups. HS was characterized by high polydispersity related with their structure. FAs were characterized by ellipsoidal shape as being associated to the long aliphatic chains, while HAs and HNs revealed a smaller particle diameter and a more spherical shape caused by the higher intermolecular forcing between the particles. The observed trends directly indicate that individual HS fractions differ in behavior, formation, composition, and sorption properties, which reflects their binding potential to other molecules depending on soil properties resulting from their type. The determined properties of individual HS fractions are presented as averaged characteristics over the examined soils with different physico-chemical properties.

Optical Absorption Spectroscopy of DNA-Wrapped HiPco Carbon Nanotubes

2019 ◽  
Vol 943 ◽  
pp. 95-99
Author(s):  
Li Jun Wang ◽  
Kazuo Umemura
Keyword(s):  
Carbon Nanotubes ◽  
Aqueous Solution ◽  
Optical Absorption ◽  
Absorption Spectroscopy ◽  
Near Infrared ◽  
Nir Spectroscopy ◽  
Optical Characterization ◽  
Optical Absorption Spectroscopy ◽  
Double Stranded Dna

Optical absorption spectroscopy provides evidence for individually dispersed carbon nanotubes. A common method to disperse SWCNTs into aqueous solution is to sonicate the mixture in the presence of a double-stranded DNA (dsDNA). In this paper, optical characterization of dsDNA-wrapped HiPco carbon nanotubes (dsDNA-SWCNT) was carried out using near infrared (NIR) spectroscopy and photoluminescence (PL) experiments. The findings suggest that SWCNT dispersion is very good in the environment of DNA existing. Additionally, its dispersion depends on dsDNA concentration.

Characterization of humic acids from antarctic soils by nuclear magnetic resonance

2015 ◽  
Vol 48 (11) ◽  
pp. 1207-1211 ◽  
Author(s):  
S. N. Chukov ◽  
E. V. Abakumov ◽  
V. M. Tomashunas
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Humic Acids ◽  
Antarctic Soils ◽  
Nuclear Magnetic

scholarly journals STABILITY OF CODEINE: CHARACTERIZATION OF OXIDATION PRODUCTS OF CODEINE FORMED IN AQUEOUS SOLUTION

2013 ◽  
Vol 4 (7) ◽  
pp. 49-54
Author(s):  
Elahaj Babiker Mohamed ◽  
Shehab Naglaa Ahmed ◽  
Ali Heyam Saad
Keyword(s):  
Aqueous Solution ◽  
Oxidation Products

Characterization of olive mill wastes composts and their humic acids: stability assessment within different particle size fractions

2013 ◽  
Vol 34 (6) ◽  
pp. 787-797 ◽  
Author(s):  
Saoussan Masmoudi ◽  
Raja Jarboui ◽  
Hafedh El Feki ◽  
Teresa Gea ◽  
Khaled Medhioub ◽  
...  
Keyword(s):  
Particle Size ◽  
Humic Acids ◽  
Stability Assessment ◽  
Size Fractions ◽  
Particle Size Fractions ◽  
Olive Mill Wastes ◽  
Olive Mill
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