scholarly journals In situmeasurement of electromigration-induced transient stress in Pb-free Sn–Cu solder joints by synchrotron radiation based x-ray polychromatic microdiffraction

2009 ◽  
Vol 106 (2) ◽  
pp. 023502 ◽  
Author(s):  
Kai Chen ◽  
N. Tamura ◽  
M. Kunz ◽  
K. N. Tu ◽  
Yi-Shao Lai
Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Masato Hoshino ◽  
...  

The reliability of solder joints on printed circuit boards (PCBs) is significantly affected by thermal fatigue processes due to downsizing and high density packaging in electronic components. Accordingly, there is a strong desire in related industries for development of a new nondestructive inspection technology to detect fatigue cracks appearing in these joints. The authors have applied the SP-μCT, a synchrotron radiation X-ray microtomography system, to the nondestructive observation of such cracks. However, for planar objects such as PCB substrates, reconstruction of CT images is difficult due to insufficient X-ray transmission along the parallel axis of the substrate. In order to solve this problem, a synchrotron radiation X-ray laminography system was developed to overcome the size limits of such specimens. In this work, this system was applied to the three-dimensional, nondestructive observation of thermal fatigue cracks in solder joints, for which X-ray CT inspection has been extremely difficult. The observed specimens included two typical joint structures formed using Sn-3.0Ag-0.5Cu solder: (1) a fine pitch ball grid array (FBGA) joint specimen in which an LSI package is connected to a substrate by solder bumps 360 μm in diameter, and (2) a die-attached specimen in which a 3 mm square ceramic chip is mounted on a substrate. The optical system developed for use in X-ray laminography was constructed to provide a rotation axis with a 30° tilt from the right angle to the X-ray beam, and to obtain X-ray projection images via the beam monitor. The same solder joints were observed successively using the laminography system at beamline BL20XU at SPring-8, the largest synchrotron radiation facility in Japan. In the FBGA type specimen, fatigue cracks were clearly observed to appear at the periphery of the joint interface, and to propagate gradually to the inner regions of the solder bumps as thermal cycling proceeded. In contrast, in the die-attached joint specimen, micro-cracks were observed to appear and propagate through the thin solder layer. An important observation was that these micro-cracks become interconnected prior to propagation of the main fatigue crack. The fatigue crack propagation lifetime was also estimated in both specimens by measuring the crack surface area and calculating the average crack propagation rate through the three-dimensional images. Consequently, the sectional images obtained by the laminography system clearly show the process of crack propagation due to thermal cyclic loading.


Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Kentaro Uesugi ◽  
...  

The reliability or lifetime of micro-joints on printed circuit boards (PCBs) is significantly affected by fatigue processes, including fatigue crack initiation and propagation to failure. Accordingly, the industries producing electronic devices and components strongly desire a new nondestructive inspection technology, which detects micro-cracks appearing as thermal fatigue fractures in the joints. In this investigation, we applied a synchrotron radiation X-ray micro-tomography system called the SP-μCT to three-dimensionally and nondestructively evaluate the fatigue crack propagation process in complex-shaped solder joints. The observed specimens have a typical joint structure in which chip type resistors 1.0 mm in length and 0.5 mm in width are mounted on an FR-4 substrate by joining with Sn-3.0Ag-0.5Cu solder. A thermal cycle test was carried out, and specimens were collected at fixed cycle numbers. The same solder joints were observed successively using the SP-μCT at beamline BL20XU at SPring-8, the largest synchrotron radiation facility in Japan. An X-ray energy of 29.0 keV was selected to obtain computed tomography (CT) images with high contrast among some components, and a refraction-contrast imaging technique was also applied to the visualization of fatigue cracks in the solder joints. The following results were obtained. At the early stage in the fatigue process of normal joints, the main fatigue cracks were clearly observed to initiate from the region around the solder joint tip and the vicinity of the chip corner. Additionally, many micro-cracks roughly 5 to 10 μm in length also formed in the thin solder layer between the chip and substrate. The important observed fact is that these micro-cracks deform, grow, and connect to each other due to the thermal cyclic loading, prior to main crack propagation. On the other hand, in case of solder joints which included relatively larger initial voids, the voids deformed, and the fatigue cracks initiated and propagated from the surface of the voids. Furthermore, by employing the three-dimensional crack images, the crack dimensions were quantified straightforwardly by measuring the surface area of the fatigue crack, and the fatigue crack propagation process was also accurately evaluated via the average crack propagation rate. Consequently, the obtained CT images clearly illustrate the process of crack propagation due to the thermal cyclic loading of a solder joint. In contrast, such information has not been obtained in any form by industrially employed X-ray CT systems or finite element analyses.


Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Kentaro Uesugi ◽  
...  

The reliability and lifetime of micro-joints on printed circuit boards (PCBs) is significantly affected by fatigue processes, including fatigue crack initiation and propagation to failure. Accordingly, the industries producing electronic devices and components strongly desire the development of a new nondestructive inspection technology, which detects micro-cracks appearing as thermal fatigue fractures in these joints. Accordingly, the authors have demonstrated that the micro-cracks in the micro-solder joints can be observed using the SP-μCT synchrotron X-ray micro tomography system. However, in order for such solder joint micro-cracks to be observable by SP-μCT, the observation object must have a diameter of less than roughly 1 mm. In this investigation, we applied a synchrotron radiation X-ray laminography system to three-dimensionally and nondestructively evaluate the fatigue crack propagation process in flip chip solder micro-joints. X-ray laminography is a technique for nondestructively observing planar objects. The optical system developed for use in X-ray laminography was constructed to provide the rotation stage with a 20° tilt from the horizontally incident X-ray beam. For this reason, X-rays were sufficiently transmitted through the planar object, in all directions. The observed specimens had a flip chip structure, in which a 10.04 mm square LSI chip is connected to a 52.55 mm (length) × 30.0 mm (width) FR-4 substrate by 120 μm diameter Sn-3.0wt%Ag-0.5wt%Cu lead-free solder bumps. A thermal cycle test was carried out, and specimens were collected at fixed cycle numbers. The same solder joints were observed successively using the synchrotron radiation X-ray laminography system at beamline BL20XU at SPring-8, the largest synchrotron radiation facility in Japan. An X-ray beam energy of 29.0 keV was selected to obtain laminography images with high contrast among component. The obtained laminography images clearly show the evolution of cracks, voids, and the Ag3Sn phase due to the thermal cyclic loading of the solder joints. In addition, the surface area of the same fatigue cracks was also measured, to quantify the crack propagation process. However, the surface area change measured by laminography differed from the crack propagation results obtained by standard SP-μCT. This difference may be due to an inability to observe some micro-cracks, due to crack closure to beneath than the detection limit of synchrotron radiation X-ray laminography. Consequently, these results demonstrate the possibility that nondestructive observation of fatigue cracks in the solder bumps on a large size electronic substrate by synchrotron radiation X-ray laminography, although its detection ability for narrow cracks may be limited, compared to SP-μCT.


2017 ◽  
Vol 2017 (0) ◽  
pp. GS0703
Author(s):  
Hiroki HIGASHIKATA ◽  
Hiroyuki TSURITANI ◽  
Toshihiko SAYAMA ◽  
Yoshiyuki OKAMOTO ◽  
Takeshi TAKAYANAGI ◽  
...  

Author(s):  
B. Jouffrey ◽  
D. Dorignac ◽  
A. Bourret

Since the early works on GP zones and the model independently proposed by Preston and Guinier on the first steps of precipitation in supersaturated solid solution of aluminium containing a few percent of copper, many works have been performed to understand the structure of different stages in the sequence of precipitation.The scheme which is generally admitted can be drawn from a work by Phillips.In their original model Guinier and Preston analysed a GP zone as composed of a single (100) copperrich plane surrounded by aluminum atomic planes with a slightly shorter distance from the original plane than in the solid solution.From X-ray measurements it has also been shown that GP1 zones were not only copper monolayer zones. They could be up to a few atomic planes thick. Different models were proposed by Guinier, Gerold, Toman. Using synchrotron radiation, proposals have been recently made.


1987 ◽  
Vol 48 (C1) ◽  
pp. C1-175-C1-181
Author(s):  
S. AHMAD ◽  
M. OHTOMO ◽  
R. W. WHITWORTH

Sign in / Sign up

Export Citation Format

Share Document