Multiple-oscillating-field techniques for accurate distance measurements by solid-state NMR

2009 ◽  
Vol 130 (22) ◽  
pp. 225103 ◽  
Author(s):  
Lasse Arnt Straasø ◽  
Morten Bjerring ◽  
Navin Khaneja ◽  
Niels Chr. Nielsen
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Distance Measurements ◽  
Field Techniques

scholarly journals Self-Assembly of E5/PDGFβR in Membranes Studied by Solid-State NMR Distance Measurements

2020 ◽  
Vol 118 (3) ◽  
pp. 210a
Author(s):  
Li Tian ◽  
Stephan L. Grage ◽  
Parvesh Wadhwani ◽  
Anne S. Ulrich
Keyword(s):  
Solid State ◽  
Self Assembly ◽  
Solid State Nmr ◽  
Distance Measurements

scholarly journals Distance Measurements in Multiply Labeled Crystalline Cytidines by Dipolar Recoupling Solid State NMR

1999 ◽  
Vol 103 (20) ◽  
pp. 3890-3903 ◽  
Author(s):  
S. R. Kiihne ◽  
K. B. Geahigan ◽  
N. A. Oyler ◽  
H. Zebroski ◽  
M. A. Mehta ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Distance Measurements ◽  
Dipolar Recoupling

Distance Measurements by Dipolar Recoupling Two-Dimensional Solid-State NMR

1998 ◽  
Vol 102 (13) ◽  
pp. 2274-2282 ◽  
Author(s):  
S. Kiihne ◽  
M. A. Mehta ◽  
J. A. Stringer ◽  
D. M. Gregory ◽  
J. C. Shiels ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Two Dimensional ◽  
Distance Measurements ◽  
Dipolar Recoupling

scholarly journals Dihedral Angle Measurements for Structure Determination by Biomolecular Solid-State NMR Spectroscopy

2021 ◽  
Vol 8 ◽  
Author(s):  
Patrick C. A. van der Wel
Keyword(s):  
Solid State ◽  
Structure Determination ◽  
Solid State Nmr ◽  
Structural Information ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Distance Measurements ◽  
Challenges And Opportunities ◽  
Molecule Interactions ◽  
Angle Spinning

In structural studies of immobilized, aggregated and self-assembled biomolecules, solid-state NMR (ssNMR) spectroscopy can provide valuable high-resolution structural information. Among the structural restraints provided by magic angle spinning (MAS) ssNMR the canonical focus is on inter-atomic distance measurements. In the current review, we examine the utility of ssNMR measurements of angular constraints, as a complement to distance-based structure determination. The focus is on direct measurements of angular restraints via the judicious recoupling of multiple anisotropic ssNMR parameters, such as dipolar couplings and chemical shift anisotropies. Recent applications are highlighted, with a focus on studies of nanocrystalline polypeptides, aggregated peptides and proteins, receptor-substrate interactions, and small molecule interactions with amyloid protein fibrils. The review also examines considerations of when and where ssNMR torsion angle experiments are (most) effective, and discusses challenges and opportunities for future applications.

Distance measurements in nucleic acids using windowless dipolar recoupling solid state NMR

1996 ◽  
Vol 7 (3) ◽  
pp. 211-228 ◽  
Author(s):  
M.A. Mehta ◽  
D.M. Gregory ◽  
S. Kiihne ◽  
D.J. Mitchell ◽  
M.E. Hatcher ◽  
...  
Keyword(s):  
Solid State ◽  
Nucleic Acids ◽  
Solid State Nmr ◽  
Distance Measurements ◽  
Dipolar Recoupling

Solid-State NMR Correlation Experiments and Distance Measurements in Paramagnetic Metalorganics Exemplified by Cu-Cyclam

ChemPhysChem ◽  
2013 ◽  
Vol 14 (9) ◽  
pp. 1864-1870 ◽  
Author(s):  
Shashi K. Kumara Swamy ◽  
Agnieszka Karczmarska ◽  
Malgorzata Makowska-Janusik ◽  
Abdelhadi Kassiba ◽  
Jens Dittmer
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Distance Measurements

Exploiting 13C/14N solid-state NMR distance measurements to assign dihedral angles and locate neighboring molecules

2018 ◽  
Vol 54 (49) ◽  
pp. 6376-6379 ◽  
Author(s):  
Giovanna M. Pope ◽  
Ivan Hung ◽  
Zhehong Gan ◽  
Hani Mobarak ◽  
Göran Widmalm ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Natural Abundance ◽  
Dihedral Angles ◽  
Distance Measurements ◽  
Nmr Method

The RESPDOR NMR method rapidly provides multiple 13C/14N distance measurements in natural abundance solids.

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