Comparison of the OKα x-ray emission bands in micro- and mesoporous silica materials and in α-quartz

2008 ◽  
Vol 129 (8) ◽  
pp. 084711 ◽  
Author(s):  
O. Yu. Khyzhun ◽  
T. Strunskus ◽  
Ch. Wöll ◽  
H. Gies ◽  
V. Staemmler
Keyword(s):  
Mesoporous Silica ◽  
X Ray ◽  
Silica Materials ◽  
Mesoporous Silica Materials

scholarly journals Simple Synthesis and Characterization of Hexagonal and Ordered Al–MCM–41 from Natural Perlite

Minerals ◽  
2019 ◽  
Vol 9 (5) ◽  
pp. 264 ◽  
Author(s):  
Hongyun Chen ◽  
Siyao Fu ◽  
Liangjie Fu ◽  
Huaming Yang ◽  
Deliang Chen
Keyword(s):  
Mesoporous Silica ◽  
Bet Surface Area ◽  
Ammonium Bromide ◽  
X Ray Diffraction ◽  
X Ray ◽  
Chemical Structures ◽  
Ordered Mesoporous ◽  
Silica Materials ◽  
Mesoporous Silica Materials ◽  
Mcm 41

Silica reagents are expensive and toxic for use in the synthesis of mesoporous silica materials. It is imperative to take an interest in green silicon sources. In this paper, we report the synthesis of hexagonal and ordered aluminum-containing mesoporous silica materials (Al–MCM–41) from natural perlite mineral without addition of silica or aluminum reagents. A pretreatment process involving acid leaching, alkali leaching, and strongly acidic cation exchange resins treatment was critical to obtain silicon and aluminum sources from natural perlite mineral. The Al–MCM–41 material was synthesized via a hydrothermal reaction with hexadecyl trimethyl ammonium bromide (CTAB) as the template and subsequent calcination. The resulting mesophase had a hexagonal and ordered mesoporous structure, confirmed by small-angle X-ray diffraction (SAXRD) and transmission electron microscopy (TEM). Al–MCM–41 material had a high Brunauer–Emmet–Teller (BET) surface area of 1024 m2/g, pore volume of 0.72 cm3/g and an average pore diameter of 2.8 nm with a pore size distribution centered at 2.5 nm. The thermal behavior of the as-synthesized samples during calcination was investigated by thermogravimetry (TG) and differential thermogravimetry (DTG) analysis. The Al–MCM–41 material showed a negative surface charge in aqueous solution with the pH value ranging from 2 to 13. The variations of chemical structures from natural perlite to Al–MCM–41 were traced by wide-angle X-ray diffraction (WAXRD) and Fourier-transform infrared spectroscopy (FTIR). A proposed mechanism for the synthesis of hexagonal and ordered mesoporous silica materials from natural perlite is discussed.

Study of mesoporous silica materials by small angle x-ray scattering

2001 ◽  
Vol 10 (5) ◽  
pp. 429-432 ◽  
Author(s):  
Li Zhi-hong ◽  
Gong Yan-jun ◽  
Zhang Ye ◽  
Wu Dong ◽  
Sun Yu-han ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Silica Materials ◽  
Mesoporous Silica Materials ◽  
Ray Scattering

scholarly journals Mechanisms and Intermediates in the True Liquid Crystal Templating Synthesis of Mesoporous Silica Materials

2021 ◽  
Vol 125 (12) ◽  
pp. 3197-3207
Author(s):  
Johanna R. Bruckner ◽  
Jessica Bauhof ◽  
Jacqueline Gebhardt ◽  
Ann-Katrin Beurer ◽  
Yvonne Traa ◽  
...  
Keyword(s):  
Liquid Crystal ◽  
Mesoporous Silica ◽  
Silica Materials ◽  
Mesoporous Silica Materials ◽  
Liquid Crystal Templating ◽  
Templating Synthesis

Fl–DFO molecules@mesoporous silica materials: Highly sensitive and selective nanosensor for dosing with iron ions

2011 ◽  
Vol 358 (1) ◽  
pp. 136-145 ◽  
Author(s):  
Bao-Lian Su ◽  
Nicolas Moniotte ◽  
Noan Nivarlet ◽  
Li-Hua Chen ◽  
Zheng-Yi Fu ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Iron Ions ◽  
Highly Sensitive ◽  
Silica Materials ◽  
Mesoporous Silica Materials

Monolithic Macroporous-Mesoporous Carbon Using Ionic Liquids as Carbon Source

2014 ◽  
Vol 988 ◽  
pp. 23-26
Author(s):  
Ai Bing Chen ◽  
Yun Hong Yu ◽  
Yi Feng Yu ◽  
Hai Jun Lv ◽  
Ting Ting Xing ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Carbon Source ◽  
Mesoporous Silica ◽  
Mesoporous Carbon ◽  
Structure Directing Agent ◽  
Silica Source ◽  
Pu Foam ◽  
Silica Materials ◽  
Mesoporous Silica Materials ◽  
Ordered Macroporous

A facile approach is employed for the preparation of hierarchically porous structures monolithic ordered macroporous-mesoporous silica materials (OMS) using the commercially available and cheap polyurethane (PU) foam as monolithic template, triblock copolymer P123 (EO20PO70EO20) as structure-directing agent and tetraethyl orthosilicate (TEOS) as silica source, then monolithic ordered macro porous-mesoporous carbon materials (OMC) is synthesized by using monolithic ordered macroporous-mesoporous silica materials as hard template and ionic liquids as the carbon source. The silica and carbon monoliths possess uniform pore sizes (3.74-3.84 nm) and ordered mesostructure.

scholarly journals Synthesis of Gold Catalysts Supported on Mesoporous Silica Materials: Recent Developments

Catalysts ◽  
2011 ◽  
Vol 1 (1) ◽  
pp. 97-154 ◽  
Author(s):  
Luis-Felipe Gutiérrez ◽  
Safia Hamoudi ◽  
Khaled Belkacemi
Keyword(s):  
Mesoporous Silica ◽  
Gold Catalysts ◽  
Silica Materials ◽  
Recent Developments ◽  
Mesoporous Silica Materials
Sign in / Sign up

Export Citation Format

Share Document