Setup for in situ x-ray diffraction study of swift heavy ion irradiated materials

2007 ◽  
Vol 78 (11) ◽  
pp. 113901 ◽  
Author(s):  
P. K. Kulriya ◽  
F. Singh ◽  
A. Tripathi ◽  
R. Ahuja ◽  
A. Kothari ◽  
...  
2012 ◽  
Vol 83 (1) ◽  
pp. 013902 ◽  
Author(s):  
C. Grygiel ◽  
H. Lebius ◽  
S. Bouffard ◽  
A. Quentin ◽  
J. M. Ramillon ◽  
...  

2008 ◽  
Vol 104 (7) ◽  
pp. 073504 ◽  
Author(s):  
Jean-Marc Costantini ◽  
François Guillet ◽  
Sébastien Lambert ◽  
Dominique Grébille ◽  
François Beuneu ◽  
...  

2015 ◽  
Vol 48 (3) ◽  
pp. 711-717 ◽  
Author(s):  
Raul I. Palomares ◽  
Cameron L. Tracy ◽  
Fuxiang Zhang ◽  
Changyong Park ◽  
Dmitry Popov ◽  
...  

Hydrothermal diamond anvil cells (HDACs) provide facile means for coupling synchrotron X-ray techniques with pressure up to 10 GPa and temperature up to 1300 K. This manuscript reports on an application of the HDAC as an ambient-pressure sample environment for performingin situdefect annealing and thermal expansion studies of swift heavy ion irradiated CeO2and ThO2using synchrotron X-ray diffraction. The advantages of thein situHDAC technique over conventional annealing methods include rapid temperature ramping and quench times, high-resolution measurement capability, simultaneous annealing of multiple samples, and prolonged temperature and apparatus stability at high temperatures. Isochronal annealing between 300 and 1100 K revealed two-stage and one-stage defect recovery processes for irradiated CeO2and ThO2, respectively, indicating that the morphology of the defects produced by swift heavy ion irradiation of these two materials differs significantly. These results suggest that electronic configuration plays a major role in both the radiation-induced defect production and high-temperature defect recovery mechanisms of CeO2and ThO2.


Author(s):  
Eric O'Quinn ◽  
Cameron Tracy ◽  
William F. Cureton ◽  
Ritesh Sachan ◽  
Joerg C. Neuefeind ◽  
...  

Er2Sn2O7 pyrochlore was irradiated with swift heavy Au ions (2.2 GeV), and the induced structural modifications were systematically examined using complementary characterization techniques including transmission electron microscopy (TEM), X-ray diffraction...


Carbon ◽  
2015 ◽  
Vol 87 ◽  
pp. 246-256 ◽  
Author(s):  
Périne Landois ◽  
Mathieu Pinault ◽  
Stéphan Rouzière ◽  
Dominique Porterat ◽  
Cristian Mocuta ◽  
...  

2016 ◽  
Vol 4 (20) ◽  
pp. 7718-7726 ◽  
Author(s):  
Dorsasadat Safanama ◽  
Neeraj Sharma ◽  
Rayavarapu Prasada Rao ◽  
Helen E. A. Brand ◽  
Stefan Adams

In situ synchrotron X-ray diffraction study of the synthesis of solid-electrolyte Li1+xAlxGe2−x(PO4)3 (LAGP) from the precursor glass reveals that an initially crystallized dopant poor phase transforms into the Al-doped LAGP at 800 °C.


2021 ◽  
Vol 48 (10) ◽  
Author(s):  
Sergey V. Goryainov ◽  
John S. Tse ◽  
Serge Desgreniers ◽  
Saori I. Kawaguchi ◽  
Yuanming Pan ◽  
...  

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