Experimental setup for lensless imaging via soft x-ray resonant scattering

2007 ◽  
Vol 78 (4) ◽  
pp. 043702 ◽  
Author(s):  
Maurizio Sacchi ◽  
Carlo Spezzani ◽  
Alessandro Carpentiero ◽  
Mauro Prasciolu ◽  
Renaud Delaunay ◽  
...  
2021 ◽  
Vol 126 (8) ◽  
Author(s):  
G. Pérez-Callejo ◽  
E. V. Marley ◽  
D. A. Liedahl ◽  
L. C. Jarrott ◽  
G. E. Kemp ◽  
...  

2013 ◽  
Vol 28 (S2) ◽  
pp. S481-S490
Author(s):  
Oriol Vallcorba ◽  
Anna Crespi ◽  
Jordi Rius ◽  
Carles Miravitlles

The viability of the direct-space strategy TALP (Vallcorba et al., 2012b) to solve crystal structures of molecular compounds from laboratory powder diffraction data is shown. The procedure exploits the accurate metric refined from a ‘Bragg-Brentano’ powder pattern to extract later the intensity data from a second ‘texture-free’ powder pattern with the DAJUST software (Vallcorba et al., 2012a). The experimental setup for collecting this second pattern consists of a circularly collimated X-ray beam and a 2D detector. The sample is placed between two thin Mylar® foils, which reduces or even eliminates preferred orientation. With the combination of the DAJUST and TALP software a preliminary but rigorous structural study of organic compounds can be carried out at the laboratory level. In addition, the time-consuming filling of capillaries with diameters thinner than 0.3mm is avoided.


2019 ◽  
Vol 90 (8) ◽  
pp. 083905 ◽  
Author(s):  
Prakhyat Hejmady ◽  
Lucien C. Cleven ◽  
Lambèrt C. A. van Breemen ◽  
Patrick D. Anderson ◽  
Ruth Cardinaels

2001 ◽  
Vol 40 (Part 2, No. 8B) ◽  
pp. L884-L887 ◽  
Author(s):  
Riichirou Negishi ◽  
Masami Yoshizawa ◽  
Shengming Zhou ◽  
Isao Matsumoto ◽  
Tomoe Fukamachi ◽  
...  

2014 ◽  
Vol 70 (a1) ◽  
pp. C1330-C1330
Author(s):  
Joerg Wiesmann ◽  
Andreas Kleine ◽  
Christopher Umland ◽  
André Beerlink ◽  
Juergen Graf ◽  
...  

Parasitic scattering caused by apertures is a well-known problem in X-ray analytics, which forces users and manufacturers to adapt their experimental setup to this unwanted phenomenon. Increased measurement times due to lower photon fluxes, a lower resolution caused by an enlarged beam stop, a larger beam defining pinhole-to-sample distance due to the integration of an antiscatter guard and generally a lower signal-to-noise ratio leads to a loss in data quality. In this presentation we will explain how the lately developed scatterless pinholes called SCATEX overcome the aforementioned problems. SCATEX pinholes are either made of Germanium or of Tantalum and momentarily have a minimum diameter of 30µm. Thus, these novel apertures are applicable to a wide range of different applications and X-ray energies. We will show measurements which were performed either at home-lab small angle X-ray scattering (SAXS) systems such as the NANOSTAR of Bruker AXS or at synchrotron beamlines. At the PTB four-crystal monochromator beamline at BESSY II data was collected for a comparison of conventional pinholes, scatterless Germanium slit systems and SCATEX pinholes. At the Nanofocus Endstation P03 beamline at PETRA III we compared the performance of our SCATEX apertures with conventional Tungsten slit systems under high flux density conditions.


2018 ◽  
Vol 74 (6) ◽  
pp. 673-680 ◽  
Author(s):  
V. G. Kohn

The article reports an accurate theory of X-ray coplanar multiple diffraction for an experimental setup that consists of a generic synchrotron radiation (SR) source, double-crystal monochromator (M) and slit (S). It is called for brevity the theory of X-ray coplanar multiple SRMS diffractometry. The theory takes into account the properties of synchrotron radiation as well as the features of diffraction of radiation in the monochromator crystals and the slit. It is shown that the angular and energy dependence (AED) of the sample reflectivity registered by a detector has the form of a convolution of the AED in the case of the monochromatic plane wave with the instrumental function which describes the angular and energy spectrum of radiation incident on the sample crystal. It is shown that such a scheme allows one to measure the rocking curves close to the case of the monochromatic incident plane wave, but only using the high-order reflections by monochromator crystals. The case of four-beam (220)(331)({\overline {11}}1) diffraction in Si is considered in detail.


2019 ◽  
Vol 622 ◽  
pp. A61 ◽  
Author(s):  
R. Staubert ◽  
J. Trümper ◽  
E. Kendziorra ◽  
D. Klochkov ◽  
K. Postnov ◽  
...  

Cyclotron lines, also called cyclotron resonant scattering features are spectral features, generally appearing in absorption, in the X-ray spectra of objects containing highly magnetized neutron stars, allowing the direct measurement of the magnetic field strength in these objects. Cyclotron features are thought to be due to resonant scattering of photons by electrons in the strong magnetic fields. The main content of this contribution focusses on electron cyclotron lines as found in accreting X-ray binary pulsars (XRBP) with magnetic fields on the order of several 1012Gauss. Also, possible proton cyclotron lines from single neutron stars with even stronger magnetic fields are briefly discussed. With regard to electron cyclotron lines, we present an updated list of XRBPs that show evidence of such absorption lines. The first such line was discovered in a 1976 balloon observation of the accreting binary pulsar Hercules X-1, it is considered to be the first direct measurement of the magnetic field of a neutron star. As of today (end 2018), we list 35 XRBPs showing evidence of one ore more electron cyclotron absorption line(s). A few have been measured only once and must be confirmed (several more objects are listed as candidates). In addition to the Tables of objects, we summarize the evidence of variability of the cyclotron line as a function of various parameters (especially pulse phase, luminosity and time), and add a discussion of the different observed phenomena and associated attempts of theoretical modeling. We also discuss our understanding of the underlying physics of accretion onto highly magnetized neutron stars. For proton cyclotron lines, we present tables with seven neutron stars and discuss their nature and the physics in these objects.


2020 ◽  
Vol 6 (40) ◽  
pp. eaba9351
Author(s):  
Paul G. Evans ◽  
Samuel D. Marks ◽  
Stephan Geprägs ◽  
Maxim Dietlein ◽  
Yves Joly ◽  
...  

Spin electronic devices based on crystalline oxide layers with nanoscale thicknesses involve complex structural and magnetic phenomena, including magnetic domains and the coupling of the magnetism to elastic and plastic crystallographic distortion. The magnetism of buried nanoscale layers has a substantial impact on spincaloritronic devices incorporating garnets and other oxides exhibiting the spin Seebeck effect (SSE). Synchrotron hard x-ray nanobeam diffraction techniques combine structural, elemental, and magnetic sensitivity and allow the magnetic domain configuration and structural distortion to be probed in buried layers simultaneously. Resonant scattering at the Gd L2 edge of Gd3Fe5O12 layers yields magnetic contrast with both linear and circular incident x-ray polarization. Domain patterns facet to form low-energy domain wall orientations but also are coupled to elastic features linked to epitaxial growth. Nanobeam magnetic diffraction images reveal diverse magnetic microstructure within emerging SSE materials and a strong coupling of the magnetism to crystallographic distortion.


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