Improved Double‐Crystal Spectrometer for Small Angle Scattering Measurements

1950 ◽  
Vol 21 (4) ◽  
pp. 399-400 ◽  
Author(s):  
Leo Broussard
1993 ◽  
Vol 48 (12) ◽  
pp. 1203-1206
Author(s):  
R. M. Hagenmayer ◽  
C. M. E. Zeyen ◽  
P. Lamparter ◽  
S. Steeb

Abstract Using a neutron double crystal spectrometer, thin amorphous Ni-Pd-P-samples were investi-gated at very small Q-values (10-5 Å -1 ≦Q≦10 -3 Å -1). The immersion method shows that the small angle scattering effect is mainly caused by surface scattering.


1977 ◽  
Vol 10 (1) ◽  
pp. 37-44 ◽  
Author(s):  
C. Cabos ◽  
P. Delord ◽  
J. Rouviere

The structure of micellar solutions is determined from X-ray small-angle scattering measurements on an absolute scale. The most probable structure is chosen by comparison with spherical cylindrical and lamellar models. This method is applied to two-component micelles and it is possible to follow the variation of micellar dimensions when the concentration of each component is varying.


1967 ◽  
Vol 11 ◽  
pp. 332-338 ◽  
Author(s):  
Donald M. Koffman

AbstractAn X-ray small-angle scattering instrument is described which is used for recording X-ray diffraction patterns or small-angle X-ray scattering curves in an angular region very close to the direct beam. The measurement of X-ray intensity is accomplished with standard geiger or scintillation counter techniques. The instrument is designed for use with a spot-focus or vertical-line X-ray source, In essence, it is a multiple-reflection double-crystal diffractometer, based on a concept developed by Bonse and Hart, employing two grooved perfect germanium crystals arranged in the parallel position. Multiple diffraction from these crystals produces a monochromated X-ray beam which can be several millimeters wide while still exhibiting extremely high angular resolution. As a result, effective sample volumes can be employed with maximum volume-to-thickness ratios. The principal features of the instrument are discussed with emphasis on the advantages of this device over those employing complex slit systems and film-re cording techniques, Data are presented to illustrate the operation, intensity, and resolution of the unit.


2017 ◽  
Vol 73 (a1) ◽  
pp. a101-a101
Author(s):  
Andrew J. Allen ◽  
Fan Zhang ◽  
Jan Ilavsky ◽  
Pete R. Jemian

1989 ◽  
Vol 174 ◽  
Author(s):  
D. L. Worcester ◽  
T. J. Michalski ◽  
M. K. Bowman ◽  
J. J. Katz

AbstractNeutron small-angle scattering measurements of several different chlorophylls hydrated in deuterated octane-toluene mixtures show that long, hollow cylinders of aggregated chlorophyll are formed. Clear secondary maxima are present in the scattering, and the cylinder diameters are well determined, but depend on the type of chlorophyll. Chlorophyll-a and Bacteriochlorophyll-a were particularly studied, and several samples of each have been measured. Other chlorophylls have also been studied. The results provide strong evidence that chlorophyll cylinders are only certain sizes, with diameters very nearly in the ratio of small integers. Thus, the cylinder diameters appear to be quantized. Neutron scattering results that further test this quantization property are presented here, together with a proposal for the stereochemical features of chlorophyll aggregation which account for the diameter quantization.


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