Analysis of High‐Resolution NMR Spectra by Means of the Nuclear Overhauser Effect and by Transitory Selective Irradiation (TSI) Methods

1964 ◽  
Vol 40 (12) ◽  
pp. 3734-3735 ◽  
Author(s):  
Ragnar A. Hoffman ◽  
Bo Gestblom ◽  
Sture Forsén
1985 ◽  
Vol 63 (2) ◽  
pp. 483-490 ◽  
Author(s):  
Michael A. Bernstein ◽  
Laurance D. Hall

Using a combination of one-dimensional (1D) and two-dimensional (2D) high resolution nmr methods, the 1H nmr spectrum of brucine was fully assigned. The 2D J-resolved and homonuclear chemical shift correlated (COSY) experiments provided assignments without full structural information; this was obtained from nuclear Overhauser effect (nOe) enhancement experiments (1D and 2D). With the proton spectrum fully assigned, proton-bearing carbons in the 13C nmr spectrum were easily assigned using the 2D heteronuclear chemical shift correlation map (CSCM) experiment.


2006 ◽  
Vol 128 (21) ◽  
pp. 6782-6783 ◽  
Author(s):  
Sharon E. Ashbrook ◽  
Nicholas G. Dowell ◽  
Ivan Prokes ◽  
Stephen Wimperis

1985 ◽  
Vol 107 (3) ◽  
pp. 711-712 ◽  
Author(s):  
R. H. Griffey ◽  
M. A. Jarema ◽  
S. Kunz ◽  
P. R. Rosevear ◽  
A. G. Redfield

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