Whisker Growth from Iodide Titanium Wire

1958 ◽  
Vol 29 (7) ◽  
pp. 1130-1131 ◽  
Author(s):  
Allan M. Russell ◽  
Robert C. Abbott
Author(s):  
E. U. Lee ◽  
P. A. Garner ◽  
J. S. Owens

Evidence for ordering (1-6) of interstitial impurities (O and C) has been obtained in b.c.c. metals, such as niobium and tantalum. In this paper we report the atomic and microstructural changes in an oxygenated c.p.h. metal (alpha titanium) as observed by transmission electron microscopy and diffraction.Oxygen was introduced into zone-refined iodide titanium sheets of 0.005 in. thickness in an atmosphere of oxygen and argon at 650°C, homogenized at 800°C and furnace-cooled in argon. Subsequently, thin foils were prepared by electrolytic polishing and examined in a JEM-7 electron microscope, operated at 100 KV.


Author(s):  
D.M. Vanderwalker

There is a fundamental interest in electrochemical fusion of deuterium in palladium and titanium since its supposed discovery by Fleischmann and Pons. Their calorimetric experiments reveal that a large quantity of heat is released by Pd after hours in a cell, suggesting fusion occurs. They cannot explain fusion by force arguments, nor can it be an exothermic reaction on the formation of deuterides because a smaller quantity of heat is released. This study examines reactions of deuterium in titanium.Both iodide titanium and 99% pure titanium samples were encapsulated in vacuum tubes, annealed for 2h at 800 °C. The Ti foils were charged with deuterium in a D2SO4 D2O solution at a potential of .45V with respect to a calomel reference junction. Samples were ion beam thinned for transmission electron microscopy. The TEM was performed on the JEOL 200CX.The structure of D charged titanium is α-Ti with hexagonal and fee deuterides.


2020 ◽  
Vol 634 ◽  
pp. 231-236 ◽  
Author(s):  
EA McHuron ◽  
T Williams ◽  
DP Costa ◽  
C Reichmuth

2018 ◽  
Author(s):  
D. Basak ◽  
L. H. Ponce

Abstract Two case-studies on uncommon metals whiskers, performed at the Reliability Analysis Laboratory (RAL) of Northrop Grumman Innovation Systems, are presented. The components analyzed are an Oven Controlled Crystal Oscillator (OCXO) and an Electromechanical Relay. Investigative techniques were used to determine the chemical and physical makeup of the metal whiskers and develop an understanding of the underlying effects and mechanisms that caused the conditions conducive to whisker growth.


2019 ◽  
pp. 175-181
Author(s):  
A. I. Kovtunov ◽  
T. V. Semistenova ◽  
A. M. Ostryanko

The paper offers technology of argon-arc surfacing with titanium wire in order to form heat and wear resistant coating based on the titanium cuprides. The influence of surfacing modes on the chemical compound and structure of formed coatings is determined. The wear resistance and heat resistance at 600°C and 800°C were researched for copper–titanium coating with 8–63% titanium.


2016 ◽  
Vol 46 (7) ◽  
pp. 4062-4075 ◽  
Author(s):  
S. Das Mahapatra ◽  
B. S. Majumdar ◽  
I. Dutta ◽  
S. Bhassyvasantha

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1243
Author(s):  
Claudio Puglia ◽  
Giorgio De Simoni ◽  
Francesco Giazotto

The possibility to tune, through the application of a control gate voltage, the superconducting properties of mesoscopic devices based on Bardeen–Cooper–Schrieffer metals was recently demonstrated. Despite the extensive experimental evidence obtained on different materials and geometries, a description of the microscopic mechanism at the basis of such an unconventional effect has not been provided yet. This work discusses the technological potential of gate control of superconductivity in metallic superconductors and revises the experimental results, which provide information regarding a possible thermal origin of the effect: first, we review experiments performed on high-critical-temperature elemental superconductors (niobium and vanadium) and show how devices based on these materials can be exploited to realize basic electronic tools, such as a half-wave rectifier. Second, we discuss the origin of the gating effect by showing gate-driven suppression of the supercurrent in a suspended titanium wire and by providing a comparison between thermal and electric switching current probability distributions. Furthermore, we discuss the cold field-emission of electrons from the gate employing finite element simulations and compare the results with experimental data. In our view, the presented data provide a strong indication regarding the unlikelihood of the thermal origin of the gating effect.


2021 ◽  
Vol 11 (2) ◽  
pp. 595
Author(s):  
Tatsuhiko Aizawa ◽  
Tomoaki Yoshino ◽  
Yohei Suzuki ◽  
Tomomi Shiratori

A bare AISI420J2 punch often suffers from severe adhesion of metallic titanium as well as titanium oxide debris particles in dry, cold forging of biomedical titanium alloys. This punch was plasma-carburized at 673 K for 14.4 ks to harden it up to 1200 HV on average and to achieve carbon supersaturation in the carburized layer. This plasma-carburized punch was employed in the cold, dry forging of a pure titanium wire into a flat plate while reducing the thickness by 70%. The contact interface width approached the forged workpiece width with increasing the reduction ratio. This smaller bulging deformation reveals that the workpiece is upset by homogeneous plastic flow with a lower friction coefficient. This low-friction and anti-galling forging process was sustained by an in situ solid lubrication mechanism. Unbound free carbon was isolated from the carbon-supersaturated AISI420J2 matrix and deposited as a thin tribofilm to protect the contact interface from mass transfer of metallic titanium.


2019 ◽  
Vol 35 (8) ◽  
pp. 1735-1739 ◽  
Author(s):  
Yushuang Liu ◽  
Peigen Zhang ◽  
Jin Yu ◽  
Jian Chen ◽  
Yamei Zhang ◽  
...  

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