High‐Temperature Thermal Gravimetric Apparatus

1973 ◽  
Vol 44 (9) ◽  
pp. 1428-1429 ◽  
Author(s):  
Richard A. Gardner ◽  
William R. Swiss
Keyword(s):  
High Temperature ◽  
Thermal Gravimetric ◽  
Gravimetric Apparatus

Oxidation Behavior of Steel and Pure Copper at 500-700°C

2013 ◽  
Vol 421 ◽  
pp. 401-405
Author(s):  
Sang An Ha ◽  
Jei Pil Wang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Oxidation Behavior ◽  
Pure Copper ◽  
Thermal Gravimetric ◽  
X Ray Diffraction ◽  
X Ray ◽  
Composition And Structure ◽  
Gravimetric Apparatus ◽  
Scanning Electron

The oxidation behavior of steel and pure copper has been investigated in the temperature range of 500-700°C at various oxygen pressures. The rate of oxidation was measured using thermal gravimetric apparatus (TGA). The morphology, composition and structure of the oxide scale were determined by scanning electron microscopy (SEM) and X-ray diffraction (XRD).

Synthesis of Novel Carbon Spheres and Study on Graphitization Process

2013 ◽  
Vol 634-638 ◽  
pp. 2293-2296
Author(s):  
Ai Li Ma ◽  
Cheng Qian Li ◽  
Wu Qing Du ◽  
Jie Chang
Keyword(s):  
High Temperature ◽  
Microwave Plasma ◽  
Gravimetric Analysis ◽  
Thermal Gravimetric ◽  
Carbon Spheres ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cvd Method ◽  
Graphitization Degree ◽  
Scanning Electron

In this paper, carbon spheres were synthesized by CVD method. These carbon spheres exhibit diameters of about 200 nm. Thermal gravimetric analysis indicated the good stability in high temperature of the carbon spheres. The products were treated by microwave plasma and high temperature vacuum heat treatments respectively. The products were characterized by X-ray diffraction, Raman spectroscopy and Field Emission Scanning Electron Microscope. The study indicated that the original products, with perfect morphology and low graphitization degree, were converted to crystal. The different techniques were considered for the influence on the graphitization degree.

Evaluation on Microstructure Stability and Thermal Resistant Ability at High Temperature of Ternary-Blended Geopolymer

2021 ◽  
Vol 321 ◽  
pp. 73-79
Author(s):  
Hoc Thang Nguyen
Keyword(s):  
High Temperature ◽  
Rice Husk Ash ◽  
High Thermal Stability ◽  
Gravimetric Analysis ◽  
Thermal Gravimetric ◽  
X Ray Diffraction ◽  
X Ray ◽  
Microstructure Stability ◽  
Before And After ◽  
Materials Used

Stability of microstructure and heat resistant ability at high temperature is one of the important properties in ceramics or silicate materials which are normally exposed with fire such as refractories and insulation or other materials used in furnaces. This study used a ternary-blended geopolymer which was synthesized from an optimized mixture of red mud (RM), rice husk ash (RHA), diatomaceous earth (DE), and water glass solution (WGS) with silica modulus of 2.5. The geopolymer samples were tested thermal properties of heat resistance (%), volumetric shrinkage (%), mass loss (%) at 1000°C to evaluate thermal resistant ability. Changes of microstructure of the ternary-blended geopolymer samples were also characterized before and after exposed at high temperature using methods of X-ray diffraction (XRD), Thermogravimetric analysis or thermal gravimetric analysis (DTA-TGA), and Scanning electron microscope (SEM). The experimental results showed the ternary-blended geopolymer has high thermal stability and unchanged microstructure even at high temperatures. Hence, the geopolymer in this study is suggested to apply as an insolation with the upper limit of temperature to work at 1000°C.

High Temperature Oxidation Behaviour of DSS 2205 in Humid Air

2014 ◽  
Vol 900 ◽  
pp. 673-676 ◽  
Author(s):  
Jian Guo Peng ◽  
Mou Cheng Li
Keyword(s):  
High Temperature ◽  
High Temperature Oxidation ◽  
Oxidation Behaviour ◽  
Gravimetric Analysis ◽  
Oxide Scales ◽  
Thermal Gravimetric ◽  
Humid Air ◽  
Temperature Oxidation ◽  
Increasing Temperature ◽  
Kinetics Of

The oxidation kinetics of 2205 stainless steel in humid air at high temperature were studied by adopting thermal-gravimetric analysis (TGA). The morphology, composition and microstructure of the oxide scales were analyzed using SEM and XRD. The experiment showed that few scales form on the surface of DSS2205 at less than 800°C.With increasing temperature above 800°C, thickness of oxide scales increase and the inner oxides can be found. The nodules can be observed when the temperature reaches 1050°C.

Experimental Study on Polymer Pyrolysis in High-Temperature Air Diluted by H2O and CO2 Using Stagnation-Point Flow

2011 ◽  
Author(s):  
Yasuhiro Ogami ◽  
Makoto Mori ◽  
Kentaro Yoshinaga ◽  
Hideaki Kobayashi
Keyword(s):  
Experimental Data ◽  
High Temperature ◽  
Kinetic Parameters ◽  
Stagnation Point ◽  
Stagnation Point Flow ◽  
Gravimetric Analysis ◽  
Thermal Gravimetric ◽  
Regression Rate ◽  
Extinction Limit ◽  
Polymer Pyrolysis

Combustion experiments were performed for polyethylene (PE) in stagnation-point flow to investigate the fundamental characteristics of PE in high-temperature air combustion (HiTAC). Air diluted by nitrogen, water vapor, and carbon dioxide was tested as the oxidizer, and the oxidizer temperature was varied from 300 to 773 K, to investigate the effect of the dilution and temperature on the regression rate, the extinction limit, and the sooting limit of PE. The kinetic parameters of PE pyrolysis under the combustion conditions were estimated from the regression rate experimental data using a new method combining experiments and numerical simulations. It was found that the previously reported kinetic parameters obtained with thermal gravimetric analysis (TGA) were much smaller than those obtained in this study, and that the kinetic parameters of pyrolysis were affected by dilution.

Simple Thermal‐Gravimetric Apparatus

1967 ◽  
Vol 38 (11) ◽  
pp. 1675-1676 ◽  
Author(s):  
J. J. Byerley
Keyword(s):  
Thermal Gravimetric ◽  
Gravimetric Apparatus

High-temperature fast pyrolysis of coal: An applied basic research using thermal gravimetric analyzer and the downer reactor

Energy ◽  
2021 ◽  
Vol 223 ◽  
pp. 119977
Author(s):  
Yuan Jiang ◽  
Peijie Zong ◽  
Xue Ming ◽  
Haixin Wei ◽  
Xin Zhang ◽  
...  
Keyword(s):  
High Temperature ◽  
Fast Pyrolysis ◽  
Basic Research ◽  
Thermal Gravimetric ◽  
Thermal Gravimetric Analyzer ◽  
Downer Reactor

Influence of Thermo-Mechanical Processing on the Microstructure of Beryllia Dispersed Nickel Alloys

1973 ◽  
Vol 31 ◽  
pp. 184-185
Author(s):  
M.S. Grewal ◽  
S.A. Sastri ◽  
N.J. Grant
Keyword(s):  
High Temperature ◽  
Nickel Alloys ◽  
Thermomechanical Processing ◽  
Cold Work ◽  
High Temperature Strength ◽  
Strengthening Effect ◽  
Mechanical Processing ◽  
Uniform Dispersion ◽  
Oxide Particles ◽  
Nickel Base

Currently there is a great interest in developing nickel base alloys with fine and uniform dispersion of stable oxide particles, for high temperature applications. It is well known that the high temperature strength and stability of an oxide dispersed alloy can be greatly improved by appropriate thermomechanical processing, but the mechanism of this strengthening effect is not well understood. This investigation was undertaken to study the dislocation substructures formed in beryllia dispersed nickel alloys as a function of cold work both with and without intermediate anneals. Two alloys, one Ni-lv/oBeo and other Ni-4.5Mo-30Co-2v/oBeo were investigated. The influence of the substructures produced by Thermo-Mechanical Processing (TMP) on the high temperature creep properties of these alloys was also evaluated.

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