scholarly journals Bolometric technique for high-resolution broadband microwave spectroscopy of ultra-low-loss samples

2004 ◽  
Vol 75 (1) ◽  
pp. 124-135 ◽  
Author(s):  
P. J. Turner ◽  
D. M. Broun ◽  
Saeid Kamal ◽  
M. E. Hayden ◽  
J. S. Bobowski ◽  
...  
Author(s):  
David C. Joy ◽  
Dennis M. Maher

High-resolution images of the surface topography of solid specimens can be obtained using the low-loss technique of Wells. If the specimen is placed inside a lens of the condenser/objective type, then it has been shown that the lens itself can be used to collect and filter the low-loss electrons. Since the probeforming lenses in TEM instruments fitted with scanning attachments are of this type, low-loss imaging should be possible.High-resolution, low-loss images have been obtained in a JEOL JEM 100B fitted with a scanning attachment and a thermal, fieldemission gun. No modifications were made to the instrument, but a wedge-shaped, specimen holder was made to fit the side-entry, goniometer stage. Thus the specimen is oriented initially at a glancing angle of about 30° to the beam direction. The instrument is set up in the conventional manner for STEM operation with all the lenses, including the projector, excited.


Author(s):  
William Krakow ◽  
Alec N. Broers

Low-loss scanning electron microscopy can be used to investigate the surface topography of solid specimens and provides enhanced image contrast over secondary electron images. A high resolution-condenser objective lens has allowed the low-loss technique to resolve separations of Au nucleii of 50Å and smaller dimensions of 25Å in samples coated with a fine grained carbon-Au-palladium layer. An estimate of the surface topography of fine grained vapor deposited materials (20 - 100Å) and the surface topography of underlying single crystal Si in the 1000 - 2000Å range has also been investigated. Surface imaging has also been performed on single crystals using diffracted electrons scattered through 10−2 rad in a conventional TEM. However, severe tilting of the specimen is required which degrades the resolution 15 to 100 fold due to image forshortening.


2012 ◽  
Vol 37 (16) ◽  
pp. 3384 ◽  
Author(s):  
Brandon Redding ◽  
Hui Cao

2013 ◽  
Vol 111 (12-13) ◽  
pp. 1923-1930 ◽  
Author(s):  
Paul Jansen ◽  
Isabelle Kleiner ◽  
Congsen Meng ◽  
Ronald M. Lees ◽  
Maurice H.M. Janssen ◽  
...  

2018 ◽  
Vol 20 (23) ◽  
pp. 15635-15640 ◽  
Author(s):  
P. Pinacho ◽  
A. Krin ◽  
C. Pérez ◽  
S. Zinn ◽  
J. C. López ◽  
...  

Four conformers of microsolvated ibuprofen have been characterized using high-resolution microwave spectroscopy.


2017 ◽  
Vol 35 (24) ◽  
pp. 5381-5384 ◽  
Author(s):  
Sergio Celaschi ◽  
Gilliard N. Malheiros-Silveira

2013 ◽  
Vol 24 (12) ◽  
pp. 51
Author(s):  
Brandon Redding ◽  
Sebastien Popoff ◽  
Hui Cao

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