Electron-beam-induced deposition using a subnanometer-sized probe of high-energy electrons

2003 ◽  
Vol 83 (10) ◽  
pp. 2064-2066 ◽  
Author(s):  
K. Mitsuishi ◽  
M. Shimojo ◽  
M. Han ◽  
K. Furuya
1989 ◽  
Vol 163 ◽  
Author(s):  
Takao Wada ◽  
Akihiro Takeda ◽  
Masaya Ichimura ◽  
Michihiko Takeda

AbstractGe and Zn atoms were introduced into the unirradiated regions of Si at 150°C and GaAs wafers at 50°C, respectively by using the electron-beam doping method. The surfaces of Si and GaAs substrates were covered partially by the overlayers of Ge and Zn sheets, respectively. The only surfaces of the Ge and Zn sheets were irradiated locally. with high energy electrons at 7MeV with the fluences of 5×1017 – 1×1018 electrons cm-2 . Even at a distance of ~10mm from the irradiated overlayers in the Si and GaAs substrates, Ge and Zn atoms respectively, whose interstitials may migrate the unirradiated regions, were detected by SIMS measurements. PL signal due to band-to-acceptor (ZnGa ) transition at 1.48eV becomes observable after annealing at 800°C for 20mm in the unirradiated GaAs region, which is separated from Zn sheet by nearly 10mm.


Author(s):  
А.Э. Муслимов ◽  
М.Г. Исмаилов ◽  
В.М. Каневский

Processes of film formation (0001) BaFe12O19 on sapphire with ferromagnetic "easy axis" directed along normal to substrate are investigated. Propagation of the beam of high-energy electrons during interaction with the (0001) BaFe12O19 film was studied depending on the angle of incidence of the beam. Deflection of sliding electron beam by magnetic field of (0001) BaFe12O19 film is demonstrated. It is shown that the presence of (0001) BaFe12O19 film on sapphire leads to the redistribution of cathodoluminescence in it mainly to the "red" region. The radiation associated with the film itself was not detected in the experiment.


1969 ◽  
Vol 37 (286) ◽  
pp. 270-274 ◽  
Author(s):  
M. P. Jones ◽  
J. Gavrilovic

SummaryIt is possible with a standard Geoscan microanalyser to produce back-scattered electron pictures that resemble Kikuchi patterns but which are produced by a different mechanism. These effects have been called scanning electron beam anomalous transmission (SEBAT) patterns and they are produced by the interaction of a parallel scanning beam of high-energy electrons with a crystalline sample. The patterns are excellent indicators of the crystallographic perfection and orientation of samples and can provide information about the lattice dimensions of solid, bulk specimens. The same specimens can, if necessary, be chemically analysed in the same instrument.In order to produce the patterns the electron beam must be deflected through a minimum angle of approximately 20° and, on existing instruments, the beam covers an area of about 2 × 2 mm during such a deflection. Minor modification of the authors' microanalyser has reduced the scanned area to 0·5 × 0·5 mm and attempts are being made to reduce this even further.In favourable circumstances the technique enables the mineralogist to determine, rapidly and easily, the crystallographic structure and orientation of large, bulk specimens. Examples are given of patterns that have been produced from cleaved, as grown, and polished mineral faces. The degree and nature of the crystallographic damage produced during mechanical polishing of a galena crystal are illustrated.


2021 ◽  
Vol 119 (1) ◽  
pp. 014103
Author(s):  
Zoey Warecki ◽  
Andrew A. Allerman ◽  
Andrew M. Armstrong ◽  
A. Alec Talin ◽  
John Cumings

Author(s):  
Paul F. Hlava ◽  
William F. Chambers

In the electron microprobe, a beam of high energy electrons is focussed to a fine point on the surface of a fairly thick specimen and the x rays produced are analyzed to determine the chemistry of the "point". The spa- cial resolution of this instrument for chemical analysis, then, is defined by the volume of material from which the x ray signal originates. This, in turn, is related to factors such as the diameter of the electron beam, the spreading of the electron beam as it penetrates into the sample and interacts with the atoms of the sample to generate x rays, and the extent to which these primary x rays penetrate beyond the region of electron beam interaction and generate secondary x rays by the process of fluorescence. Beam voltage, current, and diameter can all be easily controlled by the analyst. Once the electrons enter the specimen, however, the analyst loses control of their density. Each individual electron follows a unique, erratic path as it passes near, passes through, or collides with parts of the atoms in the specimen. Monte Carlo calculations are a means by which many investigators have tried to model the paths of individual electrons and the interation volume that large numbers of such electrons define.3 “* It is well known that the size and shape of the region into which the electron beam penetrates and expends its energy is controlled primarily by the average atomic number, atomic weight, and density of the specimen in the region of interest and the beam voltage.


2017 ◽  
Vol 265 ◽  
pp. 237-244 ◽  
Author(s):  
V.V. Novokreschenov ◽  
R.V. Rodyakina ◽  
M.A. Karimbekov

In this paper, based on the gas-kinetic theory of plasma, a theoretical analysis of the possibility of forming a plasma state in melting channel as a result of the interaction of high-energy electrons of the electron beam with the atoms of the material, being processed in melting channel (in free state) is proposed. Also the assessment of a possible impact of this process on the quality of weld metal is given. It is shown that if we take the electron-beam welding of large thickness with formation of a knife-form melting zone, the occurring processes can develop both in the direction of self-organization (synergetic, evolution) and chaotically (it all depends on the set of after-effects, caused by them, and their duration), which is manifested either as autofocusing and melted depth increase (synergy, evolution) or as formation of defects in the center of the channel (in the central part of the weld) in the form of steam and gas cavities of quite considerable size.


2017 ◽  
Vol 8 ◽  
pp. 2376-2388 ◽  
Author(s):  
Ragesh Kumar T P ◽  
Sangeetha Hari ◽  
Krishna K Damodaran ◽  
Oddur Ingólfsson ◽  
Cornelis W Hagen

We present first experiments on electron beam induced deposition of silacyclohexane (SCH) and dichlorosilacyclohexane (DCSCH) under a focused high-energy electron beam (FEBID). We compare the deposition dynamics observed when growing pillars of high aspect ratio from these compounds and we compare the proximity effect observed for these compounds. The two precursors show similar behaviour with regards to fragmentation through dissociative ionization in the gas phase under single-collision conditions. However, while DCSCH shows appreciable cross sections with regards to dissociative electron attachment, SCH is inert with respect to this process. We discuss our deposition experiments in context of the efficiency of these different electron-induced fragmentation processes. With regards to the deposition dynamics, we observe a substantially faster growth from DCSCH and a higher saturation diameter when growing pillars with high aspect ratio. However, both compounds show similar behaviour with regards to the proximity effect. With regards to the composition of the deposits, we observe that the C/Si ratio is similar for both compounds and in both cases close to the initial molecular stoichiometry. The oxygen content in the DCSCH deposits is about double that of the SCH deposits. Only marginal chlorine is observed in the deposits of from DCSCH. We discuss these observations in context of potential approaches for Si deposition.


Author(s):  
Joseph J. Comer ◽  
Charles Bergeron ◽  
Lester F. Lowe

Using a Van De Graaff Accelerator thinned specimens were subjected to bombardment by 3 MeV N+ ions to fluences ranging from 4x1013 to 2x1016 ions/cm2. They were then examined by transmission electron microscopy and reflection electron diffraction using a 100 KV electron beam.At the lowest fluence of 4x1013 ions/cm2 diffraction patterns of the specimens contained Kikuchi lines which appeared somewhat broader and more diffuse than those obtained on unirradiated material. No damage could be detected by transmission electron microscopy in unannealed specimens. However, Dauphiné twinning was particularly pronounced after heating to 665°C for one hour and cooling to room temperature. The twins, seen in Fig. 1, were often less than .25 μm in size, smaller than those formed in unirradiated material and present in greater number. The results are in agreement with earlier observations on the effect of electron beam damage on Dauphiné twinning.


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