Low-temperature synthesis of large-scale single-crystal molybdenum trioxide (MoO3) nanobelts

2002 ◽  
Vol 81 (25) ◽  
pp. 4832-4834 ◽  
Author(s):  
Xiao-Lin Li ◽  
Jun-Feng Liu ◽  
Ya-Dong Li
RSC Advances ◽  
2015 ◽  
Vol 5 (56) ◽  
pp. 45122-45128 ◽  
Author(s):  
Lijuan Bu ◽  
Wenjing Yang ◽  
Hai Ming

TiO2single crystal nanorods (TNRs) with dominant (002) facets and the derivative, Au/TNRs, were prepared and investigated in a photocatalytic reaction.


2014 ◽  
Vol 07 (01) ◽  
pp. 1450002 ◽  
Author(s):  
Hongtao Cui ◽  
Minmin Wang ◽  
Wanzhong Ren ◽  
Yunan Zhao

Nonaggregate and well-crystallized Co 3 O 4 nanoparticles with size of 5–15 nm were prepared on a large scale at low temperature by an epoxide precipitation route. The preparation of Co 3 O 4 nanoparticles followed the steps of α- Co ( OH )2 formation through epoxide precipitation reactions, conversion of α- Co ( OH )2 to CoOOH in ammonia regulated alkaline suspension, and transformation of CoOOH to Co 3 O 4 at 100°C. The small size and nonaggregate state of obtained Co 3 O 4 nanoparticles guaranteed the full contact of Co 3 O 4 nanoparticles with electrolyte and the complete penetration of electrolyte into the particles. Consequently, the Co 3 O 4 nanoparticles presented specific capacitance as high as 879.5 F g-1 at scan rate of 5 mV s-1 in 1 KOH . Their specific capacitance remain 82.8% of the initial specific capacitance after 5000 charge and discharge cycles. These results demonstrated that these Co 3 O 4 nanoparticles can be applied as a high performance electrode material for supercapacitor.


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