Monochromator crystal mounting stage

2002 ◽  
Vol 73 (3) ◽  
pp. 1571-1573 ◽  
Author(s):  
Wilfried Schildkamp
2001 ◽  
Vol 34 (3) ◽  
pp. 258-262 ◽  
Author(s):  
D. F. R Mildner ◽  
M. Arif ◽  
S. A. Werner

Thermal neutron transmission measurements have been made as a function of wavelength on a pyrolytic graphite monochromator crystal that has been set to diffract a horizontal beam at different take-off angles. The major dips in the transmission caused by the various reflections have been identified. These results can be used for the design of a beamline on which more than one instrument is placed. The transmission data show that it is best for the monochromator with the greatest (horizontal) take-off angle to be placed upstream, with monochromators with decreasing take-off angles progressively further downstream. The order of instruments for which the wavelength is greater than 0.43 nm is unimportant.


1996 ◽  
Author(s):  
Horst Schulte-Schrepping ◽  
Zhibi Wang ◽  
Joachim Heuer

2012 ◽  
Vol 20 (1) ◽  
pp. 80-88 ◽  
Author(s):  
Tadashi Matsushita ◽  
Etsuo Arakawa ◽  
Wolfgang Voegeli ◽  
Yohko F. Yano

An X-ray reflectometer has been developed, which can simultaneously measure the whole specular X-ray reflectivity curve with no need for rotation of the sample, detector or monochromator crystal during the measurement. A bent-twisted crystal polychromator is used to realise a convergent X-ray beam which has continuously varying energyE(wavelength λ) and glancing angle α to the sample surface as a function of horizontal direction. This convergent beam is reflected in the vertical direction by the sample placed horizontally at the focus and then diverges horizontally and vertically. The normalized intensity distribution of the reflected beam measured downstream of the specimen with a two-dimensional pixel array detector (PILATUS 100K) represents the reflectivity curve. Specular X-ray reflectivity curves were measured from a commercially available silicon (100) wafer, a thin gold film coated on a silicon single-crystal substrate and the surface of liquid ethylene glycol with data collection times of 0.01 to 1000 s using synchrotron radiation from a bending-magnet source of a 6.5 GeV electron storage ring. A typical value of the simultaneously covered range of the momentum transfer was 0.01–0.45 Å−1for the silicon wafer sample. The potential of this reflectometer for time-resolved X-ray studies of irreversible structural changes is discussed.


1996 ◽  
Vol 67 (9) ◽  
pp. 3352-3352
Author(s):  
Ivan Neschev Ivanov ◽  
Sorinel Cimpoes ◽  
John Chrzas

1995 ◽  
Vol 66 (2) ◽  
pp. 2092-2094 ◽  
Author(s):  
Hitoshi Yamaoka ◽  
Andreas K. Freund ◽  
Kiyotaka Ohtomo ◽  
Michael Krumrey

2014 ◽  
Vol 47 (4) ◽  
pp. 1329-1336 ◽  
Author(s):  
S. Stoupin ◽  
S. A. Terentyev ◽  
V. D. Blank ◽  
Yu. V. Shvyd'ko ◽  
K. Goetze ◽  
...  

A double-crystal diamond (111) monochromator recently implemented at the Linac Coherent Light Source (LCLS) enables splitting of the primary X-ray beam into a pink (transmitted) and a monochromatic (reflected) branch. The first monochromator crystal, with a thickness of ∼100 µm, provides sufficient X-ray transmittance to enable simultaneous operation of two beamlines. This article reports the design, fabrication and X-ray characterization of the first and second (300 µm-thick) crystals utilized in the monochromator and the optical assemblies holding these crystals. Each crystal plate has a region of about 5 × 2 mm with low defect concentration, sufficient for use in X-ray optics at the LCLS. The optical assemblies holding the crystals were designed to provide mounting on a rigid substrate and to minimize mounting-induced crystal strain. The induced strain was evaluated using double-crystal X-ray topography and was found to be small over the 5 × 2 mm working regions of the crystals.


2008 ◽  
Vol 41 (4) ◽  
pp. 798-799 ◽  
Author(s):  
Hiroshi Okuda ◽  
Kazuo Nakajima ◽  
Kozo Fujiwara ◽  
Kohei Morishita ◽  
Shojiro Ochiai

Pre-polished Ge(111) single-crystal wafers were deformed just below the melting temperature to prepare point-focusing Johansson monochromator crystals. The (111) lattice plane had curvature 2Rin the focusing plane andRperpendicular to it, with a hemispherical inner surface with a radius ofR= 600 mm. By using CuKα radiation, the diverging X-ray beam was focused onto a small spot.


1996 ◽  
Vol 29 (3) ◽  
pp. 230-235 ◽  
Author(s):  
C. Giannini ◽  
L. Tapfer

This work proposes a new four-crystal monochromator particularly indicated for applications in the field of high-resolution X-ray diffraction. The monochromator is made of two monolithic crystal elements. The first one is a channel-cut crystal consisting of two symmetrically cut components set in a parallel nondispersive geometry. The second monolithic crystal is composed of two crystal components in a parallel nondispersive geometry but the crystal surfaces are miscut with respect to the diffraction planes. The diffraction geometry for both components of the second monochromator crystal element is the glancing-incidence condition. The peculiar properties of this monochromator are investigated theoretically. An appropriate rotation of the second component of the second monolithic block with respect to the first components corrects the beam deviation caused by the refraction effect. This monochromator system may allow one to obtain highly monochromated and collimated beams with high angular resolution (about 0.01 mrad) and wavelength dispersion of about 4 × 10−5. The intensity reduction of the proposed crystal arrangement in comparison with other monochromators is discussed, including wavelength spread and beam size increase.


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