Effect of the heat treatment time on microstructure and fracture toughness of laser-clad TiB2-TiC pseudoeutectic reinforced TiNi/Ti2Ni intermetallic matrix composite coating

2016 ◽  
Vol 113 (3) ◽  
pp. 304
Author(s):  
L. L. Bai ◽  
J. Li ◽  
J. L. Chen ◽  
R. Song ◽  
J. Z. Shao ◽  
...  
2020 ◽  
pp. 0734242X2095740
Author(s):  
Haijun Bi ◽  
Huabing Zhu ◽  
Lei Zu ◽  
Yong Gao ◽  
Song Gao ◽  
...  

Spent lithium iron phosphate (LFP) batteries contain abundant strategic lithium resources and are thus considered attractive secondary lithium sources. However, these batteries may contaminate the environment because they contain hazardous materials. In this work, a novel process involving low-temperature heat treatment is used as an alternative pretreatment method for recycling spent LFP batteries. When the temperature reaches 300°C, the dissociation effect of the anode material gradually improves with heat treatment time. At the heat treatment time of 120 minutes, an electrode material can be dissociated. The extension of heat treatment time has a minimal effect on quality loss. The physicochemical changes in thermally treated solid cathode and anode materials are examined through scanning electron microscopy with energy-dispersive X-ray spectroscopy. The heat treatment results in the complete separation of the materials from aluminium foil without contamination. The change in heat treatment temperature has a small effect on the quality of LFP material shedding. When the heat treatment temperature reaches 300°C and the time reaches 120 minutes, heat treatment time increases, and the yield of each particle size is stable and basically unchanged. The method can be scaled up and may reduce environmental pollution due to waste LFP batteries.


2018 ◽  
Vol 917 ◽  
pp. 64-68
Author(s):  
Wiendartun ◽  
Jaenudin Kamal ◽  
Dadi Rusdiana ◽  
Andhy Setiawan ◽  
Dani Gustaman Syarief

A study on the effect of heat treatment condition on the characteristics of MnO2 added-Fe2TiO5 ceramics for NTC thermistor has been carried out. The ceramics were produced by pressing an homogenous mixture of Fe2O3 (local/ yarosite), TiO2 and MnO2 (2.0 mole %) powders in appropriate proportions to produce Fe2TiO5 based ceramics and sintering the pressed powder at 1050 °C for 3 hours in oxygen gas. Some sintered pellets were heat treated by heating them at 300 °C for 5, 15 and 25 minutes in Ar + 7% H2 gas. The XRD analyses showed that the Fe2TiO5 ceramics with and without heat treatment time had orthorhombic structure. No peak from second phase was observed from the XRD profiles. From the electrical characteristics data, it was known that the heat treatment could change the electrical characteristics of the Fe2TiO5 based-thermistor. The thermistor constant (B) and room temperature resistivity (ρRT) decreased with the increasing of heat treatment time. All ceramics made had thermistor characteristics namely B = 3459-7596 K and ρRT = 1.056-6936.062 MΩcm. Thermistor constant of the ceramics was relatively big, indicated that ceramics made from local iron oxide in this work fit the market requirement for NTC thermistor.


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