HIGH-TEMPERATURE INTERNAL-FRICTION PEAK IN 99.999 wt % SINGLE-CRYSTAL ALUMINIUM

1985 ◽  
Vol 46 (C10) ◽  
pp. C10-359-C10-362 ◽  
Author(s):  
C. M. SU ◽  
T. S. KÊ
2012 ◽  
Vol 535-537 ◽  
pp. 1027-1030
Author(s):  
Xiao Hui Cao ◽  
Yu Wang

By using a low frequency inverted torsion pendulum, the high temperature internal friction spectra of Al-0.02wt%Zr and Al-0.1wt%Zr alloys were investigated respectively. In Al-0.02wt%Zr alloy, the conventional grain boundary internal friction peak (Pg) is observed with some small unstable peaks. In Al-0.1wt%Zr alloy, the bamboo peak is observed to appear at the high temperature side of the conventional grain boundary internal friction peak. The conventional grain boundary internal friction peak decreased and moved to higher temperature. The bamboo peak owns an activation energy of 1.75eV. When average grain size exceeded the diameter of samples, Pb strength was reduced and its position was shifted to a lower temperature. Based on the grain boundary sliding model, Pg and Pb peaks were explained. Their dependence on annealing temperature and time was determined by considering the effects of contained Ce atoms and other impurities on the relaxation across grain boundary.


2015 ◽  
Vol 60 (4) ◽  
pp. 3069-3072
Author(s):  
M.L. Nó ◽  
L. Dirand ◽  
A. Denquin ◽  
J. San Juan

In the present work we have studied the high-temperature shape memory alloys based on the Ru-Nb system by using two mechanical spectrometers working in temperature ranges from 200 to 1450ºC and -150 to 900ºC. We have studied internal friction peaks linked to the martensitic transformations in the range from 300 to 1200ºC. In addition, we have evidenced another internal friction peak at lower temperature than the transformations peaks, which apparently exhibits the behaviour of a thermally activated relaxation peak, but in fact is a strongly time-dependent peak. We have carefully studied this peak and discussed its microscopic origin, concluding that it is related to the interaction of some structural defects with martensite interfaces. Finally, we perform a complete analysis of the whole internal friction spectrum, taking into account the possible relationship between the time-dependent peak and the martensitic transformation behaviour.


1998 ◽  
Vol 24 (12) ◽  
pp. 904-907 ◽  
Author(s):  
S. N. Smirnov ◽  
V. D. Natsik ◽  
P. P. Pal’-Val’

2012 ◽  
Vol 184 ◽  
pp. 122-127 ◽  
Author(s):  
Mykola Ivanchenko ◽  
Yuriy Yagodzinskyy ◽  
H. Hänninen

Two oxygen-free copper grades with purity of 99.99 % were studied by means of free decay inverted torsion pendulum at the temperature range of 90 – 300 K and frequencies of 0.5 – 2 Hz. One copper grade was oxygen free electrolytically refined copper with oxygen content of 1.2 wt. ppm. The other one was oxygen-free phosphorous-alloyed grade with oxygen content less than 5 wt. ppm and phosphorous content of 30 – 70 wt. ppm. Electrochemical hydrogen charging induces a complex internal friction peak in the studied copper grades. The observed internal friction peak has a relaxation origin with apparent activation enthalpy and pre-exponential factor for the oxygen-free grade of 0.276 ± 0.002 eV and 10-11.59 ± 0.08 s, respectively. The internal friction peak can be fitted by three broadened Debye peaks (P1, P2 and P3) with activation enthalpies and pre-exponential factors of 0.248 ± 0.003 eV and 10-11.4 ± 0.4 s; 0.297 ± 0.004 eV and 10-11.8 ± 0.2 s; 0.36 ± 0.04 eV and 10-12.7 ± 1.4 s, respectively. Phosphorous doping markedly reduces the height of the observed peak. It was also shown that prior deformation by tension suppresses high-temperature components of the complex internal friction peak. Mechanism of relaxation is presumably caused by interaction of H – H pairs (low-temperature component, peak P1), interaction of hydrogen atoms with dislocations (P2) and interaction of hydrogen with impurities (high-temperature component, peak P3). Absorption of hydrogen in the studied copper grades during electrochemical hydrogen charging was confirmed by the thermal desorption method.


1990 ◽  
Vol 121 (2) ◽  
pp. 475-481 ◽  
Author(s):  
G. Y. Tian ◽  
J. Z. Lu ◽  
S. P. Wu ◽  
L. D. Zhang

1995 ◽  
Vol 14 (16) ◽  
pp. 1126-1128 ◽  
Author(s):  
T. Sakai ◽  
K. Takizawa ◽  
T. Eguchi ◽  
J. Horie

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