On-line isotope dilution and sample dilution by flow injection and inductively coupled plasma mass spectrometry

1990 ◽  
Vol 5 (2) ◽  
pp. 125-133 ◽  
Author(s):  
Miklós Viczián ◽  
Alexandra Lásztity ◽  
Xioaru Wang ◽  
Ramon M. Barnes
1994 ◽  
Vol 48 (11) ◽  
pp. 1331-1336 ◽  
Author(s):  
Shayessteh Dadfarnia ◽  
Cameron W. McLeod

A flow injection system incorporating a microcolumn of activated alumina was combined with inductively coupled plasma mass spectrometry for on-line trace enrichment and determination of uranium in surface waters and sea water. Deposition of uranium was effected with the use of a basic alumina microcolumn, and injection of nitric acid (250 μL, 2M) served to elute retained species to the ICP. A sample volume of 14 mL resulted in a preconcentration factor of 40, and precision at the 50-ng 1−1 level was 4.5% (RSD). The procedure was applied to mineral waters, river water, and sea water, and accuracy was assessed through either analysis of certified reference waters or recovery experiments.


2014 ◽  
Vol 851 ◽  
pp. 64-71 ◽  
Author(s):  
Beatriz Fernández ◽  
Pablo Rodríguez-González ◽  
J. Ignacio García Alonso ◽  
Julien Malherbe ◽  
Sergio García-Fonseca ◽  
...  

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