Thermodynamics of the actinide elements. Part I. Heats of formation of crystalline neptunium tetrachloride, neptunium oxide dichloride, and neptunium trioxide monohydrate, and a new determination of the heat of formation of the Np III and Np IV ions in M-hydrochloric acid

1969 ◽  
pp. 2995 ◽  
Author(s):  
J. Fuger ◽  
D. Brown ◽  
J. F. Easey
Keyword(s):  
Hydrochloric Acid ◽  
Heat Of Formation ◽  
Heats Of Formation ◽  
Actinide Elements

Determination of Chitosan Oligosaccharide Content by Acetylacetone Spectrophotometry Method

2012 ◽  
Vol 503-504 ◽  
pp. 543-547 ◽  
Author(s):  
Ze Ping Xu ◽  
Chuan Lun Yang ◽  
Xin Qing Zhang ◽  
Xiu Zhi Wang ◽  
Bao Sheng Huang
Keyword(s):  
Hydrochloric Acid ◽  
Linear Relationship ◽  
Regression Equation ◽  
Common Method ◽  
Chitosan Oligosaccharide ◽  
Average Recovery ◽  
Good Linear ◽  
Good Linear Relationship

Objective: To establish a common method to detect the content of chitosan oligosaccharide. Methods: Chitosan oligosaccharide was hydrolyzed completely by concentrated hydrochloric acid, and the solution was regulated into neutral with NaOH. Then, determined the absorbance in 525nm, and substituted into the regression equation to determine the results. Results: The results showed there was a good linear relationship when the concentration of chitosan oligosaccharide ranged from 0.02 mg/mL to 0.12 mg/mL, r2 = 0.999. The average recovery of chitosan oligosaccharide samples was 99.25%. Conclusion: The method is sensitive, accurate and simple. It is applied to determine of the content of chitosan oligosaccharide.

DETERMINATION OF TRACE AMOUNTS OF SILVER IN GALENA ORES

1960 ◽  
Vol 38 (9) ◽  
pp. 1488-1494 ◽  
Author(s):  
E. J. Bounsall ◽  
W. A. E. McBryde
Keyword(s):  
Aqueous Solution ◽  
Nitric Acid ◽  
Sodium Chloride ◽  
Hydrochloric Acid ◽  
Chloride Solution ◽  
Sodium Chloride Solution ◽  
Silver Content ◽  
Aqueous Sodium Chloride Solution ◽  
Aqueous Sodium

An analytical method is described for the determination of microgram amounts of silver in galena ores, based on the "reversion" of silver dithizonate. Silver is separated from relatively large amounts of lead by extraction as dithizonate into chloroform from an aqueous 1:99 nitric acid solution. Separation from mercury, which is also extracted under these conditions and would, if present, interfere in the analysis, is achieved by reverting the dithizonate solution with a 5% aqueous sodium chloride solution which is also 0.015 molar in hydrochloric acid. Following dilution of this aqueous solution and adjustment of pH, silver is again extracted into chloroform as the dithizonate, and determined absorptiometrically. Analyses of a number of galena ore samples showed a precision of within 3% for a silver content ranging from 0.03 to 0.4%.Some other methods for isolating silver from these samples, which were tried but found unsatisfactory, are discussed.

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