Facile synthesis of four-membered ring platinalactam complexes and the single-crystal structure of [Pt{CH(CN)C(O)N(CO2Et)}(cod)](cod = cycloocta-1,5-diene)

1994 ◽  
pp. 1831 ◽  
Author(s):  
William Henderson ◽  
Brian K. Nicholson ◽  
Allen G. Oliver
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Membered Ring ◽  
Single Crystal Structure ◽  
Facile Synthesis

Synthese und Kristallstruktur von Cl3Ti[N(SiMe2Cl)(SiMe2NH2)] / Synthesis and Crystal Structure of Cl3Ti[N(SiMe2Cl)(SiMe2N H2)]

1996 ◽  
Vol 51 (8) ◽  
pp. 1141-1144 ◽  
Author(s):  
R. Buheitel ◽  
W. Milius ◽  
W. Schnick
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Structure Determination ◽  
Membered Ring ◽  
Single Crystal Structure ◽  
Crystal Structure Determination ◽  
Central Feature ◽  
Synthesis And Crystal Structure

Cl3Ti[N(SiMe2Cl)(SiMe2NH2)] is yielded by reaction of TiCl4 with two molecules ClMe2SiNHSiMe3. A single crystal structure determination (P 21/n, a = 747.12(2), b = 1294.1(3), c = 1496.7(3) pm, β = 90.30(3)°, Z = 4) shows a planar four-membered ring Ti-N-Si-N as the central feature of the monomers formed by a weak coordinative bond of the NH2 group to the Ti atoms. The monomers are connected to give dimers via two Cl bridges linked to the Ti atoms.

Facile Synthesis, Single-Crystal Structure, and Biological Evaluation of Novel Pyrazolo[5,1-d][1,2,5]triazepin-4-ones

2012 ◽  
Vol 95 (1) ◽  
pp. 134-143 ◽  
Author(s):  
Liang-Wen Zheng ◽  
Hong-Zhuan Xuan ◽  
Ying-Rui Liu ◽  
Bao-Xiang Zhao ◽  
Jin-Ting Liu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Biological Evaluation ◽  
Single Crystal Structure ◽  
Facile Synthesis

ChemInform Abstract: Facile Synthesis, Single-Crystal Structure, and Biological Evaluation of Novel Pyrazolo[5,1-d][1,2,5]triazepin-4-ones.

ChemInform ◽  
2012 ◽  
Vol 43 (23) ◽  
pp. no-no
Author(s):  
Liang-Wen Zheng ◽  
Hong-Zhuan Xuan ◽  
Ying-Rui Liu ◽  
Bao-Xiang Zhao ◽  
Jin-Ting Liu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Biological Evaluation ◽  
Single Crystal Structure ◽  
Facile Synthesis

scholarly journals Facile Synthesis of Stacked Ni(OH)2 Hexagonal Nanoplates in a Large Scale

Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1407
Author(s):  
Yunfei Du ◽  
Zhijie Xin ◽  
Guodong Li ◽  
Taotao Li
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Formation Mechanism ◽  
Large Scale ◽  
Raw Materials ◽  
Single Crystal Structure ◽  
Facile Synthesis ◽  
Hydrothermal Route ◽  
Hexagonal Nanoplates

Using NiCl2 and NaOH as raw materials, stacked Ni(OH)2 hexagonal nanoplates with different edge lengths were prepared in a large scale by a simple hydrothermal route. The stacked Ni(OH)2 structure was composed of a certain amount of parallel Ni(OH)2 hexagonal nanoplates along the (001) direction. Each parallel Ni(OH)2 nanoplate had a single-crystal structure, and the exposed planes were (001), (00−1), and (100). The formation mechanism of the stacked Ni(OH)2 structures was discussed on the basis of the Ni(OH)2 crystal structure.

Iron in kornerupine; a57Fe Moessbauer spectroscopic study and comparison with single-crystal structure refinement

1999 ◽  
Vol 84 (4) ◽  
pp. 536-549 ◽  
Author(s):  
Edward S. Grew ◽  
Guenther J. Redhammer ◽  
Georg Amthauer ◽  
Mark A. Cooper ◽  
Frank C. Hawthorne ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
Spectroscopic Study ◽  
Structure Refinement ◽  
Single Crystal Structure ◽  
Crystal Structure Refinement

High‐pressure single‐crystal structure determinations for ruby up to 90 kbar using an automatic diffractometer

1978 ◽  
Vol 49 (8) ◽  
pp. 4411-4416 ◽  
Author(s):  
H. d’Amour ◽  
D. Schiferl ◽  
W. Denner ◽  
Heinz Schulz ◽  
W. B. Holzapfel
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Single Crystal ◽  
Single Crystal Structure ◽  
Structure Determinations ◽  
Automatic Diffractometer

Crystal and powder XRD data of Mg3(PO4)2-III: High-temperature and high-pressure form

1995 ◽  
Vol 10 (4) ◽  
pp. 293-295 ◽  
Author(s):  
F. Brunet ◽  
C. Chopin ◽  
A. Elfakir ◽  
M. Quarton
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Single Crystal ◽  
Diffraction Pattern ◽  
Structure Refinement ◽  
Powder Xrd ◽  
Single Crystal Structure ◽  
Crystal Structure Refinement ◽  
Pressure Form

A new diffraction pattern of the high-temperature and high-pressure polymorph Mg3(PO4)2-III (PDF 43-500) is given and indexed on the basis of a single-crystal structure refinement. It allows diffractogram indexing of the isostructural high-temperature and high-pressure form of Co3(PO4)2 (PDF 43-499).

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