scholarly journals Accurate Heteronuclear Distance Measurement under All Magic-Angle Spinning Frequencies in Solid-State NMR Spectroscopy

2021 ◽  
Author(s):  
Lixin Liang ◽  
Yi Ji ◽  
Zhenchao Zhao ◽  
Caitlin Quinn ◽  
Xiuwen Han ◽  
...  
Keyword(s):  
Molecular Structure ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
Intermolecular Interactions ◽  
Solid State Nmr ◽  
Dipolar Coupling ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid Materials ◽  
Angle Spinning

Heteronuclear dipolar coupling is indispensable in revealing the vital information related to molecular structure, dynamics, as well as the intermolecular interactions in various solid materials. Although numerous approaches have been...

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

A unified heteronuclear decoupling strategy for magic-angle-spinning solid-state NMR spectroscopy

2015 ◽  
Vol 142 (18) ◽  
pp. 184201 ◽  
Author(s):  
Asif Equbal ◽  
Morten Bjerring ◽  
P. K. Madhu ◽  
Niels Chr. Nielsen
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning

scholarly journals Solid-state NMR measurements and DFT calculations of the magnetic shielding tensors of protons of water trapped in barium chlorate monohydrate

RSC Advances ◽  
2014 ◽  
Vol 4 (99) ◽  
pp. 56248-56258 ◽  
Author(s):  
Diego Carnevale ◽  
Sharon E. Ashbrook ◽  
Geoffrey Bodenhausen
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dft Calculations ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magnetic Shielding ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Shielding Tensors ◽  
Angle Spinning

The magnetic shielding tensors of protons of water in barium chlorate monohydrate are investigated by means of solid-state NMR spectroscopy, both for static powders and under magic-angle spinning conditions.

Intermolecular Protein−RNA Interactions Revealed by 2D31P−15N Magic Angle Spinning Solid-State NMR Spectroscopy

2010 ◽  
Vol 132 (11) ◽  
pp. 3842-3846 ◽  
Author(s):  
Stefan Jehle ◽  
Melanie Falb ◽  
John P. Kirkpatrick ◽  
Hartmut Oschkinat ◽  
Barth-Jan van Rossum ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning
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