Time-economical synthesis of selenofunctionalized heterocycles via I2O5-mediated selenylative heterocyclization

2021 ◽  
Author(s):  
Chen-Fan Zhou ◽  
Yun-Qian Zhang ◽  
Yong Ling ◽  
Liang Ming ◽  
Xia Xi ◽  
...  
Keyword(s):  
Robust Synthesis

A time-economical and robust synthesis of various selenofunctionalized heterocycles was accomplished via I2O5-mediated selenocyclizations of olefins with diselenides. Using this method, 116 selenomethyl-substituted heterocycles were synthesized with up to 97%...

Development of a Flexible and Robust Synthesis of Tetrahydrofuro[3,4-b]furan Nucleoside Analogues

2021 ◽  
Author(s):  
David A. Candito ◽  
Yingchun Ye ◽  
Ryan V. Quiroz ◽  
Michael H. Reutershan ◽  
David Witter ◽  
...  
Keyword(s):  
Nucleoside Analogues ◽  
Robust Synthesis

Path Tracking Design by Fractional Prefilter Extension to Square MIMO Systems

2009 ◽  
Author(s):  
P. Melchior ◽  
C. Inarn ◽  
A. Oustaloup
Keyword(s):  
Mimo Systems ◽  
Path Tracking ◽  
Multivariable Systems ◽  
Frequency Bandwidth ◽  
Control Loop ◽  
Physical Constraints ◽  
Performance Specifications ◽  
Fractional Derivation ◽  
Synthesis Methodology ◽  
Robust Synthesis

The aim of this paper concerns motion control and robust path tracking. An approach based on fractional prefilter synthesis was already developed. It allows tracking optimization according to the fractional derivation order, the actuators physical constraints and the control loop frequency bandwidth. The purpose of this paper is the extension of this approach to multivariable systems. A non integer prefilter synthesis methodology for square MIMO systems (Multi-Input, Multi-Output) is presented. It is based on the MIMO-QFT robust synthesis methodology, taking into account of the plant uncertainties. MIMO-QFT robust synthesis methodology is based on multiple SISO (MISO systems) synthesis by considering the loop couplings. The SISO-QFT synthesis methodology can be then used for each SISO synthesis. Then the prefilters are synthesized. The prefilter parameter optimization is founded on the prefilter output error integral minimization, taking into account of the actuators physical constraints and the tracking performance specifications. An application example is given.

Bayesian Analysis for Robust Synthesis of Nanostructures

2012 ◽  
Vol 1 ◽  
pp. 172-186 ◽  
Author(s):  
Nader Ebrahimi ◽  
Mahmoud Shehadeh ◽  
Kristin McCullough
Keyword(s):  
Bayesian Analysis ◽  
Synthesis Of Nanostructures ◽  
Robust Synthesis

scholarly journals Robust Synthesis of NIR-Emissive P-Rhodamine Fluorophores

2020 ◽  
Author(s):  
Maria Sauer ◽  
Veselin Nasufovic ◽  
Hans-Dieter Arndt ◽  
Ivan Vilotijevic
Keyword(s):  
Quantum Yields ◽  
Insight Into ◽  
Robust Synthesis

P-rhodamines were accessed by implementing a robust three step sequence consisting of (i) addition of m-metallated anilines to dichlorophosphine oxides, (ii) selective dibromination, and (iii) cyclization of the diaryllithium reagents derived from the dibromides to form the dihydroacridophosphine core of P-rhodamines. A modified route to produce non-symmetric P-rhodamines was additionally developed. A library of the prepared P-rhodamines provides first insight into dependence of fluorophore properties on the structure of P-rhodamines. A P-rhodamine with highest batochromic shifts and quantum yields in the class was identified.

Robust Synthesis of Highly Charged Superparamagnetic Fe3O4 Colloidal Nanocrystal Clusters for Magnetically Responsive Photonic Crystals

2021 ◽  
Author(s):  
Li-Ting Pan ◽  
Zhuo Pen ◽  
Hai-Rong Yu ◽  
Ting Liang ◽  
Chang-Jing Cheng
Keyword(s):  
Photonic Crystals ◽  
Structural Color ◽  
Robust Synthesis

Highly charged superparamagnetic Fe3O4 colloidal nanocrystal clusters (CNCs) with uniform and widely tunable sizes can be magnetically assembled into responsive photonic crystals to exhibit rapid and reversible brilliant structural color...

Cost-effective robust synthesis of methacrylic cellulosic sponge for organoid culture

Cellulose ◽  
2019 ◽  
Vol 27 (1) ◽  
pp. 171-184
Author(s):  
Zheng Liu ◽  
Farah Tasnim ◽  
Shujian Ong ◽  
Sabrina Shen ◽  
Xiao Zhong Huang ◽  
...  
Keyword(s):  
Cost Effective ◽  
Organoid Culture ◽  
Robust Synthesis

Robust synthesis of C-terminal cysteine-containing peptide acids through a peptide hydrazide-based strategy

2019 ◽  
Vol 17 (23) ◽  
pp. 5698-5702 ◽  
Author(s):  
Chao Zuo ◽  
Bing-Jia Yan ◽  
Han-Ying Zhu ◽  
Wei-Wei Shi ◽  
Tong-Kuai Xi ◽  
...  
Keyword(s):  
Efficient Strategy ◽  
Highly Efficient ◽  
Peptide Acids ◽  
Robust Synthesis

A simple-to-operate and highly efficient strategy for the epimerization-free synthesis of C-terminal Cys-containing peptide acids, which avoids the use of derivatization reagents for resin modification, is developed.

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