Formation of Bi2Ir Nanoparticles in a Microwave-Assisted Polyol Process Revealing the Suboxide Bi4Ir2O

2021 ◽  
Author(s):  
Matthias Smuda ◽  
Kati Finzel ◽  
Martin Hantusch ◽  
Jonas Ströh ◽  
Nicole Pienack ◽  
...  
Keyword(s):  
Intermetallic Phases ◽  
Polyol Process ◽  
Microwave Assisted ◽  
Boiling Points ◽  
Crystallization From The Melt

Intermetallic phases are usually obtained by crystallization from the melt. However, phases containing elements with widely different melting and boiling points, as well as nanoparticles, which provide a high specific...

Investigation on performance of Pd/Al2O3–C catalyst synthesized by microwave assisted polyol process for electrooxidation of formic acid

RSC Advances ◽  
2012 ◽  
Vol 2 (1) ◽  
pp. 344-350 ◽  
Author(s):  
Wei-Li Qu ◽  
Zhen-Bo Wang ◽  
Zheng-Zhi Jiang ◽  
Da-Ming Gu ◽  
Ge-Ping Yin
Keyword(s):  
Formic Acid ◽  
Polyol Process ◽  
Microwave Assisted

scholarly journals Mechanism of Bi−Ni Phase Formation in a Microwave‐Assisted Polyol Process

ChemistryOpen ◽  
2020 ◽  
Vol 9 (11) ◽  
pp. 1085-1094
Author(s):  
Matthias Smuda ◽  
Christine Damm ◽  
Michael Ruck ◽  
Thomas Doert
Keyword(s):  
Phase Formation ◽  
Polyol Process ◽  
Microwave Assisted

Performance of Pt/C catalysts prepared by microwave-assisted polyol process for methanol electrooxidation

2010 ◽  
Vol 195 (7) ◽  
pp. 1799-1804 ◽  
Author(s):  
Yuan-Yuan Chu ◽  
Zhen-Bo Wang ◽  
Da-Ming Gu ◽  
Ge-Ping Yin
Keyword(s):  
Polyol Process ◽  
Methanol Electrooxidation ◽  
Microwave Assisted

scholarly journals Parameters Affecting the Microwave-Assisted Polyol Synthesis of Silver Nanorods

2011 ◽  
Vol 2011 ◽  
pp. 1-7 ◽  
Author(s):  
Srichandana Nandikonda ◽  
Edward W. Davis
Keyword(s):  
Microwave Heating ◽  
Polyol Process ◽  
Polyol Synthesis ◽  
Copper Salts ◽  
Silver Nanorods ◽  
Microwave Assisted ◽  
Traditional Process ◽  
Stark Contrast ◽  
Container Shape

The effects of salt chemistry and concentration on the morphology and yield of silver nanorods produced by the microwave-assisted polyol synthesis are reported. Compared to NaCl, iron and copper salts reduced nanorod yield and length and increased diameter. This is in stark contrast to expectations based on the slower traditional polyol process. The role of the cation was further explored using MgCl2 and MnCl2 which showed different concentration dependent effects on nanorod diameter. In addition, the morphology and yield of nanomaterials was found to be significantly influenced by small variations in the procedure including container shape and the time between reactant mixing and microwave heating. These results highlight that, while the microwave-assisted process is very promising, results cannot be directly anticipated based on the traditional process, and the synthesis is very sensitive to procedural changes.

New insights into the structural analysis of maghemite and (MFe2O4, M = Co, Zn) ferrite nanoparticles synthesized by a microwave-assisted polyol process

2020 ◽  
Vol 4 (10) ◽  
pp. 3063-3073
Author(s):  
Álvaro Gallo-Cordova ◽  
Ana Espinosa ◽  
Aida Serrano ◽  
Lucía Gutiérrez ◽  
Nieves Menéndez ◽  
...  
Keyword(s):  
Structural Analysis ◽  
Microwave Heating ◽  
Ferrite Nanoparticles ◽  
Polyol Process ◽  
Microwave Assisted ◽  
Zn Ferrite ◽  
Zn Nanoparticles

A comprehensive structural analysis was presented on crystalline maghemite and ferrite (MFe2O4, M = Co, Zn) nanoparticles prepared by the well-known polyol process enhanced by fast, reproducible, easy and efficient microwave heating.

scholarly journals Front Cover: Mechanism of Bi−Ni Phase Formation in a Microwave‐Assisted Polyol Process (ChemistryOpen 11/2020)

ChemistryOpen ◽  
2020 ◽  
Vol 9 (11) ◽  
pp. 1082-1082
Author(s):  
Matthias Smuda ◽  
Christine Damm ◽  
Michael Ruck ◽  
Thomas Doert
Keyword(s):  
Phase Formation ◽  
Polyol Process ◽  
Front Cover ◽  
Microwave Assisted
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