Effect of pressure on the phase transformations and mechanical properties of 10 mol% Mg-PSZ sintered by HPHT

CrystEngComm ◽  
2022 ◽  
Author(s):  
Jian Wang ◽  
Zhiwen Wang ◽  
Yongkui Wang ◽  
Hongan Ma ◽  
Shuai Fang ◽  
...  

MgO (10 mol%)-stabilized zirconia ceramics were obtained using high-pressure high-temperature (HPHT) sintering. The effects of the sintering pressure (2.5, 3.7, and 5.0 GPa) on the phase transformations and hardness were...

1996 ◽  
Vol 220 (1-3) ◽  
pp. 149-157 ◽  
Author(s):  
V.D. Blank ◽  
S.G. Buga ◽  
N.R. Serebryanaya ◽  
G.A. Dubitsky ◽  
S.N. Sulyanov ◽  
...  

2002 ◽  
Vol 75 (5) ◽  
pp. 955-968 ◽  
Author(s):  
Jeremy E. Morin ◽  
Drew E. Williams ◽  
Richard J. Farris

Abstract High-pressure high-temperature sintering (HPHTS) is a novel recycling technique that makes it possible to recycle vulcanized rubber powders made from waste rubber (namely scrap tires) through only the application of heat and pressure. A brief look into the mechanism of sintering will be presented along with information about the influence of molding variables, such as time, temperature, pressure and rubber particle size on the mechanical properties of the produced parts. One of the most interesting observations is that powders of every crosslinked elastomer attempted sintered together via this technique, including silicone rubber (SI), sulfur cured [natural rubber (NR), ethylene-propylene-diene rubber (EPDM), styrene-butadiene rubber (SBR)], peroxide cured butadiene rubber (BR), and fluoroelastomers (FKM). Early work on sintered rubber made from commercially available rubber powder had a modulus of 1 to 2 MPa, strength of 4 to 7 MPa and an elongation at break of 150–250%. Recently, in-house ground samples of SBR have had sintered values over 9.5 MPa strength and 275% elongation, or greater than 60% retention of the original properties. Many of these mechanical properties are comparable with industrially manufactured rubbers, and it is believed that recycled rubbers produced via HPHTS offer the potential to replace virgin rubber in numerous applications.


2010 ◽  
Vol 63 ◽  
pp. 396-401 ◽  
Author(s):  
Piotr Klimczyk

Three types: micro-, submicro- and nano-structured Si3N4-SiC composites have been obtained by High Pressure-High Temperature (HPHT) sintering. Density, Young modulus, hardness and fracture toughness have been measured. Composites obtained from sub-micron powders are characterized by better mechanical properties than composites obtained from nanopowders.


2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.


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