Development of an in situ high-temperature X-ray diffraction technique for lithium-ion battery materials

2021 ◽  
Vol 57 (76) ◽  
pp. 9752-9755
Author(s):  
Kazuhiko Mukai ◽  
Takeshi Uyama ◽  
Takamasa Nonaka
Keyword(s):  
High Temperature ◽  
Lithium Ion Battery ◽  
Lithium Ion ◽  
Thermal Runaway ◽  
X Ray Diffraction ◽  
Battery Materials ◽  
Detailed Mechanism ◽  
X Ray

The development of an in situ high-temperature X-ray diffraction technique for lithium-ion battery materials is crucial for understanding the detailed mechanism of thermal runaway.

High Temperature Compatible Conflat Cell with Adjustable Stack Pressure for In-Situ and Operando X-Ray Studies of Lithium-Ion Battery Materials

2021 ◽  
Vol MA2021-02 (1) ◽  
pp. 105-105
Author(s):  
Oles Sendetskyi ◽  
Mark Salomons ◽  
Patricio Mendez ◽  
Michael Fleischauer
Keyword(s):  
High Temperature ◽  
Lithium Ion Battery ◽  
Lithium Ion ◽  
Battery Materials ◽  
X Ray

Thermal structural stability of a multi-component olivine electrode for lithium ion batteries

CrystEngComm ◽  
2016 ◽  
Vol 18 (39) ◽  
pp. 7463-7470 ◽  
Author(s):  
Kyu-Young Park ◽  
Hyungsub Kim ◽  
Seongsu Lee ◽  
Jongsoon Kim ◽  
Jihyun Hong ◽  
...  
Keyword(s):  
High Temperature ◽  
Neutron Diffraction ◽  
Lithium Ion Batteries ◽  
Structural Stability ◽  
Cathode Materials ◽  
Structural Evolution ◽  
Lithium Ion ◽  
X Ray Diffraction ◽  
X Ray

In this paper, the structural evolution of Li(Mn1/3Fe1/3Co1/3)PO4, which is a promising multi-component olivine cathode materials, is investigated using combined in situ high-temperature X-ray diffraction and flux neutron diffraction analyses at various states of charge.

ChemInform Abstract: Structural Evolution of LixMn2O4 in Lithium-Ion Battery Cells Measured in situ Using Synchrotron X-Ray Diffraction Techniques.

ChemInform ◽  
2010 ◽  
Vol 29 (19) ◽  
pp. no-no
Author(s):  
S. MUKERJEE ◽  
T. R. THURSTON ◽  
N. M. JISRAWI ◽  
X. Q. YANG ◽  
J. MCBREEN ◽  
...  
Keyword(s):  
Lithium Ion Battery ◽  
Structural Evolution ◽  
Lithium Ion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Battery Cells

In situ high-energy X-ray diffraction to study overcharge abuse of 18650-size lithium-ion battery

2013 ◽  
Vol 230 ◽  
pp. 32-37 ◽  
Author(s):  
Chi-Kai Lin ◽  
Yang Ren ◽  
Khalil Amine ◽  
Yan Qin ◽  
Zonghai Chen
Keyword(s):  
Lithium Ion Battery ◽  
Lithium Ion ◽  
High Energy ◽  
X Ray Diffraction ◽  
X Ray

Structural Evolution of Li x Mn2 O 4 in Lithium‐Ion Battery Cells Measured In Situ Using Synchrotron X‐Ray Diffraction Techniques

1998 ◽  
Vol 145 (2) ◽  
pp. 466-472 ◽  
Author(s):  
S. Mukerjee ◽  
T. R. Thurston ◽  
N. M. Jisrawi ◽  
X. Q. Yang ◽  
J. McBreen ◽  
...  
Keyword(s):  
Lithium Ion Battery ◽  
Structural Evolution ◽  
Lithium Ion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Battery Cells

scholarly journals Using In-Situ Laboratory and Synchrotron-Based X-ray Diffraction for Lithium-Ion Batteries Characterization: A Review on Recent Developments

2020 ◽  
Vol 5 (4) ◽  
pp. 75
Author(s):  
Alice V. Llewellyn ◽  
Alessia Matruglio ◽  
Dan J. L. Brett ◽  
Rhodri Jervis ◽  
Paul R. Shearing
Keyword(s):  
Structural Evolution ◽  
Deep Understanding ◽  
Lithium Ion ◽  
Market Demand ◽  
X Ray Diffraction ◽  
Battery Materials ◽  
X Ray ◽  
Challenges And Opportunities ◽  
Materials Research

Renewable technologies, and in particular the electric vehicle revolution, have generated tremendous pressure for the improvement of lithium ion battery performance. To meet the increasingly high market demand, challenges include improving the energy density, extending cycle life and enhancing safety. In order to address these issues, a deep understanding of both the physical and chemical changes of battery materials under working conditions is crucial for linking degradation processes to their origins in material properties and their electrochemical signatures. In situ and operando synchrotron-based X-ray techniques provide powerful tools for battery materials research, allowing a deep understanding of structural evolution, redox processes and transport properties during cycling. In this review, in situ synchrotron-based X-ray diffraction methods are discussed in detail with an emphasis on recent advancements in improving the spatial and temporal resolution. The experimental approaches reviewed here include cell designs and materials, as well as beamline experimental setup details. Finally, future challenges and opportunities for battery technologies are discussed.

Thermodynamic study of lithium-ion battery materials

2012 ◽  
Vol 1388 ◽  
Author(s):  
Denis Y.W. Yu ◽  
Yvan Reynier ◽  
Joanna Dodd Cardema ◽  
Yasunori Ozawa ◽  
Rachid Yazami
Keyword(s):  
Raman Spectroscopy ◽  
Phase Transitions ◽  
Lithium Ion Battery ◽  
Lithium Ion ◽  
State Of Health ◽  
X Ray Diffraction ◽  
Characterization Methods ◽  
Battery Materials ◽  
X Ray ◽  
The Status

AbstractThe ability to monitor the status of a battery during charge and discharge is important for predicting its performance and life. This is typically done by measuring the voltage and resistance across the terminals, or by external characterization methods such as X-ray diffraction and Raman spectroscopy. Thermodynamics measurements based on entropy and enthalpy provide another mean to “look inside” a battery, giving us more information to determine the state of health of the battery. In particular, entropy undergoes drastic changes at boundaries of phase transitions taking place in each electrode material at defined states of charge (lithium stoichiometry). Recent work on thermodynamics study on lithium ion battery materials is summarized in this paper.

Ball-Milled Graphite-Tin Composite Anode Materials for Lithium-Ion Battery

2012 ◽  
Vol 736 ◽  
pp. 127-132
Author(s):  
Kuldeep Rana ◽  
Anjan Sil ◽  
Subrata Ray
Keyword(s):  
Lithium Ion Battery ◽  
Anode Materials ◽  
High Capacity ◽  
Lithium Ion ◽  
Composite Anode ◽  
X Ray Diffraction ◽  
Promising Alternative ◽  
X Ray ◽  
Initial Discharge ◽  
Lithium Ion Cell

Lithium alloying compounds as an anode materials have been a focused for high capacity lithium ion battery due to their highenergy capacity and safety characteristics. Here we report on the preparation of graphite-tin composite by using ball-milling in liquid media. The composite material has been characterized by scanning electron microscope, energy depressive X-ray spectroscopy, X-ray diffraction and Raman spectra. The lithium-ion cell made from graphite-tin composite presented initial discharge capacity of 1065 mAh/g and charge capacity 538 mAh/g, which becomes 528 mAh/g in the second cycle. The composite of graphite-tin with higher capacity compared to pristine graphite is a promising alternative anode material for lithium-ion battery.

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