Ionic liquid-based effervescence-enhanced magnetic solid-phase extraction for organophosphorus pesticide detection in water samples

2022 ◽  
Author(s):  
Ming Gao ◽  
Xiaofan Zhang ◽  
Sai Ma ◽  
Xia Wang ◽  
Liyang Du ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Solid Phase Extraction ◽  
High Stability ◽  
Solid Phase ◽  
Organophosphorus Pesticides ◽  
Organophosphorus Pesticide ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Magnetic Solid ◽  
Pre Treatment

Herein, an ionic liquid-based effervescence-enhanced magnetic solid-phase extraction (ILE-MSPE) approach for extraction/concentration of organophosphorus pesticides in waters, which with high stability and portability for rapid sample pre-treatment in field. The...

scholarly journals Magnetic solid-phase extraction of pyrethroid insecticides from tea infusions using ionic liquid-modified magnetic zeolitic imidazolate framework-8 as an adsorbent

RSC Advances ◽  
2019 ◽  
Vol 9 (67) ◽  
pp. 39272-39281 ◽  
Author(s):  
Xiaodong Huang ◽  
Yanan Liu ◽  
Huifang Liu ◽  
Guangyang Liu ◽  
Xiaomin Xu ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Solid Phase Extraction ◽  
Solid Phase ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Zeolitic Imidazolate Framework ◽  
Pyrethroid Insecticides ◽  
Tea Infusions ◽  
Magnetic Solid

A MSPE-GC-MS/MS method was developed for the analysis of pyrethroids from tea infusions using Fe3O4/ZIF-8/IL as an adsorbent.

Magnetic solid-phase extraction of proteins based on hydroxy functional ionic liquid-modified magnetic nanoparticles

2014 ◽  
Vol 6 (20) ◽  
pp. 8358-8367 ◽  
Author(s):  
Jing Chen ◽  
Yuzhi Wang ◽  
Xueqin Ding ◽  
Yanhua Huang ◽  
Kaijia Xu
Keyword(s):  
Ionic Liquid ◽  
Ionic Liquids ◽  
Magnetic Nanoparticles ◽  
Solid Phase Extraction ◽  
Solid Phase ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Magnetic Solid ◽  
Extraction Performance ◽  
Modified Magnetic Nanoparticles

Hydroxy functional ionic liquids have been first designed and modified on the surface of silica-coated magnetic Fe3O4 nanoparticles (MNPs) for the investigation of the extraction performance of proteins.

scholarly journals Magnetic Solid Phase Extraction using Magnetic Mesoporous Silica for Preconcentration of Organophosphorus Pesticides

2019 ◽  
Vol 8 (4) ◽  
pp. 6847-6852
Keyword(s):  
Mesoporous Silica ◽  
Solid Phase Extraction ◽  
Water Samples ◽  
High Performance ◽  
Solid Phase ◽  
Organophosphorus Pesticides ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Magnetic Solid ◽  
Mcm 41

The present study describes the synthesis, characterization and application of two mesoporous silica material based coated magnetic nanoparticles namely Fe3O4 -SBA-15 and Fe3O4 -MCM-41 for the simultaneous preconcentration of three selected organophosphorus pesticides (OPPs) namely chlorpyrifos, diazinon and parathion methyl from water samples. The resultant sorbent material was physicochemically and morphologically characterized by field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD) and N2 adsorption analysis. OPPs pesticides extraction efficiency of two sorbents were evaluated through magnetic solid phase extraction (MSPE) using high performance liquid chromatography with ultraviolet detector (HPLC/UV). The main parameters affecting the sorbent efficiency namely extraction time and desorption solvent were optimized. Comparatively, Fe3O4 -SBA-15 achieved excellent percent recovery (97.5%) compared to the Fe3O4 -MCM-41 (87.1%) under optimum condition respectively. The result appealed that the Fe3O4 -SBA-15 composite was efficient sorbent with good capability for the preconcentration of selected OPPs from water samples.AThe present study describes the synthesis, characterization and application of two mesoporous silica material based coated magnetic nanoparticles namely Fe3O4 -SBA-15 and Fe3O4 -MCM-41 for the simultaneous preconcentration of three selected organophosphorus pesticides (OPPs) namely chlorpyrifos, diazinon and parathion methyl from water samples. The resultant sorbent material was physicochemically and morphologically characterized by field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD) and N2 adsorption analysis. OPPs pesticides extraction efficiency of two sorbents were evaluated through magnetic solid phase extraction (MSPE) using high performance liquid chromatography with ultraviolet detector (HPLC/UV). The main parameters affecting the sorbent efficiency namely extraction time and desorption solvent were optimized. Comparatively, Fe3O4 -SBA-15 achieved excellent percent recovery (97.5%) compared to the Fe3O4 -MCM-41 (87.1%) under optimum condition respectively. The result appealed that the Fe3O4 -SBA-15 composite was efficient sorbent with good capability for the preconcentration of selected OPPs from water samples.

Determination of trace rhodamine B by spectrofluorometry and magnetic solid phase extraction based on a 3D reduced graphene oxide composite

2017 ◽  
Vol 9 (37) ◽  
pp. 5433-5440 ◽  
Author(s):  
Jun Yan ◽  
Jian-Mei Cen ◽  
Xue-Cai Tan ◽  
Shao-Fen Tan ◽  
Ye-Yu Wu ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Solid Phase Extraction ◽  
Reduced Graphene Oxide ◽  
Solid Phase ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Oxide Composite ◽  
Reduced Graphene ◽  
Magnetic Solid ◽  
Pre Treatment

Sample pre-treatment by magnetic solid phase extraction based on a 3D reduced graphene oxide composite.

Magnetic multiwall carbon nanotubes modified with dual hydroxy functional ionic liquid for the solid-phase extraction of protein

The Analyst ◽  
2015 ◽  
Vol 140 (10) ◽  
pp. 3474-3483 ◽  
Author(s):  
Jing Chen ◽  
Yuzhi Wang ◽  
Yanhua Huang ◽  
Kaijia Xu ◽  
Na Li ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Ionic Liquid ◽  
Solid Phase Extraction ◽  
Solid Phase ◽  
Multiwall Carbon Nanotubes ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Magnetic Solid ◽  
Surface Modified ◽  
Multiwall Carbon

A novel adsorbent based on silica-coated magnetic multiwall carbon nanotubes (MWCNTs) surface modified by dual hydroxy functional ionic liquid (FIL) ([OH]-FIL-m-MWCNTs@SiO2) has been designed and used for the purification of lysozyme (Lys) by magnetic solid-phase extraction (MSPE).

Sign in / Sign up

Export Citation Format

Share Document