Ni/NiO/Ni-B/Graphene Heterostructure-Modified Electrodes and Their Electrochemical Activities Towards Acetaminophen

2021 ◽  
Author(s):  
Hasan Hüseyin İpekci ◽  
Merve Ozcan ◽  
Busra Gizem Turkyılmaz ◽  
Aytekin Uzunoglu
Keyword(s):  
Nickel Oxide ◽  
High Performance ◽  
Electrochemical Sensors ◽  
Reduction Method ◽  
Modified Electrodes ◽  
One Step ◽  
Boron Particles

The surface of graphene was flourished with nickel/nickel oxide/nickel-boron particles to develop high-performance electrochemical sensors. The nanohybrid structures were prepared via a one-step reduction method under oxygen-rich atmosphere to obtain...

A Robust strategy enabling addressable porous 3D carbon-based functional nanomaterials in miniaturized systems

Nanoscale ◽  
2019 ◽  
Vol 11 (8) ◽  
pp. 3674-3680 ◽  
Author(s):  
Nongnoot Wongkaew ◽  
Marcel Simsek ◽  
Palaniappan Arumugam ◽  
Arne Behrent ◽  
Sheela Berchmans ◽  
...  
Keyword(s):  
High Performance ◽  
Electrochemical Sensors ◽  
Carbon Nanofiber ◽  
Functional Nanomaterials ◽  
One Step ◽  
Carbon Based ◽  
Miniaturized Systems

Facile construction of high performance carbon nanofiber electrodes via electrospinning and one-step laser-induced carbonization for electrochemical sensors in miniaturized systems.

Hierarchically Porous Nickel Oxide Nanosheets Grown on Nickel Foam Prepared by One-Step In Situ Anodization for High-Performance Supercapacitors

2014 ◽  
Vol 9 (6) ◽  
pp. 1579-1585 ◽  
Author(s):  
Li Yang ◽  
Lei Qian ◽  
Xianqing Tian ◽  
Jing Li ◽  
Jianyuan Dai ◽  
...  
Keyword(s):  
Nickel Oxide ◽  
High Performance ◽  
Nickel Foam ◽  
Porous Nickel ◽  
Hierarchically Porous ◽  
One Step

Electroanalysis of Catecholamine Drugs using Graphene Modified Electrodes

2019 ◽  
Vol 15 (4) ◽  
pp. 443-466 ◽  
Author(s):  
Mahya Karami Mosammam ◽  
Mohammad Reza Ganjali ◽  
Mona Habibi-Kool-Gheshlaghi ◽  
Farnoush Faridbod
Keyword(s):  
Electrochemical Sensors ◽  
Modified Electrodes ◽  
Electrochemical Methods ◽  
High Signal ◽  
Signal To Noise ◽  
Low Level ◽  
Biological Studies

Background: Catecholamine drugs are a family of electroactive pharmaceutics, which are widely analyzed through electrochemical methods. However, for low level online determination and monitoring of these compounds, which is very important for clinical and biological studies, modified electrodes having high signal to noise ratios are needed. Numerous materials including nanomaterials have been widely used as electrode modifies for these families during the years. Among them, graphene and its family, due to their remarkable properties in electrochemistry, were extensively used in modification of electrochemical sensors. Objective: In this review, working electrodes which have been modified with graphene and its derivatives and applied for electroanalyses of some important catecholamine drugs are considered.

scholarly journals Influence of Cu on the Improvement of Magnetic Properties and Structure of L10 FePt Nanoparticles

Nanomaterials ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 1097
Author(s):  
Luran Zhang ◽  
Xinchen Du ◽  
Hongjie Lu ◽  
Dandan Gao ◽  
Huan Liu ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Annealing Temperature ◽  
Reduction Method ◽  
Solid Phase ◽  
Average Particle Size ◽  
Fept Nanoparticles ◽  
Average Particle ◽  
Phase Reduction ◽  
Different Temperatures ◽  
One Step

L10 ordered FePt and FePtCu nanoparticles (NPs) with a good dispersion were successfully fabricated by a simple, green, one-step solid-phase reduction method. Fe (acac)3, Pt (acac)2, and CuO as the precursors were dispersed in NaCl and annealed at different temperatures with an H2-containing atmosphere. As the annealing temperature increased, the chemical order parameter (S), average particle size (D), coercivity (Hc), and saturation magnetization (Ms) of FePt and FePtCu NPs increased and the size distribution range of the particles became wider. The ordered degree, D, Hc, and Ms of FePt NPs were greatly improved by adding 5% Cu. The highest S, D, Hc, and Ms were obtained when FePtCu NPs annealed at 750 °C, which were 0.91, 4.87 nm, 12,200 Oe, and 23.38 emu/g, respectively. The structure and magnetic properties of FePt and FePtCu NPs at different annealing temperatures were investigated and the formation mechanism of FePt and FePtCu NPs were discussed in detail.

scholarly journals N, S and Transition-Metal Co-Doped Graphene Nanocomposites as High-Performance Catalyst for Glucose Oxidation in a Direct Glucose Alkaline Fuel Cell

Nanomaterials ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 202
Author(s):  
Yexin Dai ◽  
Jie Ding ◽  
Jingyu Li ◽  
Yang Li ◽  
Yanping Zong ◽  
...  
Keyword(s):  
Fuel Cell ◽  
Active Sites ◽  
High Performance ◽  
Glucose Oxidation ◽  
Alkaline Fuel Cell ◽  
Blank Group ◽  
Graphene Nanocomposites ◽  
Doped Graphene ◽  
One Step ◽  
Hydrothermal Approach

In this work, reduced graphene oxide (rGO) nanocomposites doped with nitrogen (N), sulfur (S) and transitional metal (Ni, Co, Fe) were synthesized by using a simple one-step in-situ hydrothermal approach. Electrochemical characterization showed that rGO-NS-Ni was the most prominent catalyst for glucose oxidation. The current density of the direct glucose alkaline fuel cell (DGAFC) with rGO-NS-Ni as the anode catalyst reached 148.0 mA/cm2, which was 40.82% higher than the blank group. The DGAFC exhibited a maximum power density of 48 W/m2, which was more than 2.08 folds than that of blank group. The catalyst was further characterized by SEM, XPS and Raman. It was speculated that the boosted performance was due to the synergistic effect of N, S-doped rGO and the metallic redox couples, (Ni2+/Ni3+, Co2+/Co3+ and Fe2+/Fe3+), which created more active sites and accelerated electron transfer. This research can provide insights for the development of environmental benign catalysts and promote the application of the DGAFCs.

scholarly journals Facile Synthesis of Uniform Mesoporous Nb2O5 Micro-Flowers for Enhancing Photodegradation of Methyl Orange

Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 3783
Author(s):  
Jian-Qing Qiu ◽  
Huan-Qing Xie ◽  
Ya-Hao Wang ◽  
Lan Yu ◽  
Fang-Yuan Wang ◽  
...  
Keyword(s):  
Methyl Orange ◽  
Active Sites ◽  
High Performance ◽  
Diffuse Reflectance Spectroscopy ◽  
X Ray Diffraction ◽  
Flower Structure ◽  
Electron Microscopies ◽  
Bet Method ◽  
One Step ◽  
Catalytic Active Sites

The removal of organic pollutants using green environmental photocatalytic degradation techniques urgently need high-performance catalysts. In this work, a facile one-step hydrothermal technique has been successfully applied to synthesize a Nb2O5 photocatalyst with uniform micro-flower structure for the degradation of methyl orange (MO) under UV irradiation. These nanocatalysts are characterized by transmission and scanning electron microscopies (TEM and SEM), X-ray diffraction (XRD), Brunauer–Emmett–Teller (BET) method, and UV-Vis diffuse reflectance spectroscopy (DRS). It is found that the prepared Nb2O5 micro-flowers presents a good crystal phases and consist of 3D hierarchical nanosheets with 400–500 nm in diameter. The surface area is as large as 48.6 m2 g−1. Importantly, the Nb2O5 micro-flowers exhibit superior catalytic activity up to 99.9% for the photodegradation of MO within 20 mins, which is about 60-fold and 4-fold larger than that of without catalysts (W/O) and commercial TiO2 (P25) sample, respectively. This excellent performance may be attributed to 3D porous structure with abundant catalytic active sites.

scholarly journals Carbon nanomaterial hybrids via laser writing for high-performance non-enzymatic electrochemical sensors: a critical review

2021 ◽  
Author(s):  
Marcel Simsek ◽  
Nongnoot Wongkaew
Keyword(s):  
Noble Metal ◽  
Critical Review ◽  
High Performance ◽  
Carbon Nanomaterials ◽  
Electrochemical Sensors ◽  
Low Cost ◽  
Three Dimensional ◽  
Laser Writing ◽  
Enzyme Mimicking ◽  
Natural Enzyme

AbstractNon-enzymatic electrochemical sensors possess superior stability and affordability in comparison to natural enzyme-based counterparts. A large variety of nanomaterials have been introduced as enzyme mimicking with appreciable sensitivity and detection limit for various analytes of which glucose and H2O2 have been mostly investigated. The nanomaterials made from noble metal, non-noble metal, and metal composites, as well as carbon and their derivatives in various architectures, have been extensively proposed over the past years. Three-dimensional (3D) transducers especially realized from the hybrids of carbon nanomaterials either with metal-based nanocatalysts or heteroatom dopants are favorable owing to low cost, good electrical conductivity, and stability. In this critical review, we evaluate the current strategies to create such nanomaterials to serve as non-enzymatic transducers. Laser writing has emerged as a powerful tool for the next generation of devices owing to their low cost and resultant remarkable performance that are highly attractive to non-enzymatic transducers. So far, only few works have been reported, but in the coming years, more and more research on this topic is foreseeable. Graphical abstract

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