3D-printing for forensic chemistry: Voltammetric determination of cocaine on additively manufactured graphene-polylactic acid electrodes

2021 ◽  
Author(s):  
Raquel G. Rocha ◽  
Julia R. Santos ◽  
Mário Henrique Santana ◽  
Eduardo Mathias Richter ◽  
Rodrigo Alejandro Abarza Munoz
Keyword(s):  
3D Printing ◽  
Polylactic Acid ◽  
Illicit Drugs ◽  
Voltammetric Determination ◽  
Forensic Chemistry ◽  
The World ◽  
Cocaine Detection ◽  
Police Forces ◽  
Crime Scenes

Cocaine is probably one of the most trafficked illicit drugs in the world. For this reason, police forces require fast, selective, and sensitive methods for cocaine detection at crime scenes....

scholarly journals Promising Applications of Additive-Manufactured (3D-printed) Electrochemical Sensors for Forensic Chemistry

2021 ◽  
Author(s):  
Sílvia Castro ◽  
Raquel Rocha ◽  
Afonso João ◽  
Eduardo Richter ◽  
Rodrigo Munoz
Keyword(s):  
3D Printing ◽  
Illicit Drugs ◽  
Industrial Revolution ◽  
Electrochemical Sensors ◽  
Forensic Chemistry ◽  
Recent Contribution ◽  
Printing Technology ◽  
3D Printing Technology ◽  
Wide Range ◽  
3D Printed

Additive-manufacturing is one of the major pillars of the new industrial revolution and the three-dimensional (3D) printing technology has been highlighted in this scenario. Among the many areas benefited by 3D-printing, the development of electrochemical sensors has appeared in evidence in the last years. One potential application of 3D-printed electrochemical sensors is devoted to forensic chemistry, which demands for portable analytical methods that can provide on-site measurements and thus bring a relevant information in loco. In this context, this review highlights the recent contribution of 3D-printing technology on the development of electrochemical sensors with great promises for on-site analysis in “real-world” forensic scenarios. From the detection of trace explosives, gunshot residues, illicit drugs and chemical threats, to the measurement of adulterants in food and fuels, we show the wide range of applications that 3D-printed electrochemical sensors have been proposed and future demands that can be addressed by such a powerful, affordable, and accessible tool.

Voltammetric determination of carbaryl in some cereals on an impregnated graphite electrode modified with carbon ink

2019 ◽  
Vol 94 (2) ◽  
pp. 45-50
Author(s):  
A.S. Gashevskaya ◽  
◽  
A.O. Gusar ◽  
Ye.V. Dorozhko ◽  
K.V. Dyorina ◽  
...  
Keyword(s):  
Graphite Electrode ◽  
Voltammetric Determination

Actual issues of valuation of businesses of the economic entity

2017 ◽  
Vol 31 (2) ◽  
pp. 156-162 ◽  
Author(s):  
O. V. Schneider
Keyword(s):  
Discount Rate ◽  
Accurate Prediction ◽  
Economic Activities ◽  
Business Valuation ◽  
Economic Entity ◽  
The World ◽  
Definition Of

The article summarizes the main approaches in the definition of business valuation the economic entity. In the process of business valuation, taking into account the risks of financial and economic activities necessary to obtain information on what stage the owner implements the business will receive income. The most difficult task is the impossibility of accurate prediction in determining the level of income and the determination of a discount rate capitalization of future incomes due to the instability of the economy, both in the country and around the world.

On-line Voltammetric Determination of Traces of Zn2+in 105Excess of Ni2+

2016 ◽  
Vol 12 (4) ◽  
pp. 378-383
Author(s):  
Roumen Zlatev ◽  
Margarita Stoytcheva
Keyword(s):  
Voltammetric Determination ◽  
On Line

Simple, Direct and Simultaneous Stripping Voltammetric Determination of Lead and Copper in Gasoline Using an In Situ Mercury Film Electrode

2013 ◽  
Vol 10 (4) ◽  
pp. 498-504 ◽  
Author(s):  
Lorena Martiniano ◽  
Joseany Almeida ◽  
Glene Cavalcante ◽  
Edmar Marques ◽  
Teresa Fonseca ◽  
...  
Keyword(s):  
Voltammetric Determination ◽  
Film Electrode ◽  
Mercury Film Electrode ◽  
Mercury Film

Differential Pulse Voltammetric Determination of Piroxicam on Lanthanide Ferric Oxide Nanoparticles-Carbon Paste Modified Electrode

2018 ◽  
Vol 14 (3) ◽  
pp. 271-276 ◽  
Author(s):  
Isaac Yves Lopes de Macedo ◽  
Morgana Fernandes Alecrim ◽  
Luane Ferreira Garcia ◽  
Aparecido Ribeiro de Souza ◽  
Wallans Torres Pio dos Santos ◽  
...  
Keyword(s):  
Modified Electrode ◽  
Ferric Oxide ◽  
Differential Pulse ◽  
Voltammetric Determination ◽  
Oxide Nanoparticles ◽  
Carbon Paste ◽  
Carbon Paste Modified Electrode

Polarographic and voltammetric determination of 6-mercaptopurine and 6-thioguanine

1986 ◽  
Vol 51 (11) ◽  
pp. 2466-2472 ◽  
Author(s):  
Jiří Barek ◽  
Antonín Berka ◽  
Ludmila Dempírová ◽  
Jiří Zima
Keyword(s):  
Detection Limit ◽  
Differential Pulse Voltammetry ◽  
Detection Limits ◽  
Differential Pulse ◽  
Voltammetric Determination ◽  
Differential Pulse Polarography ◽  
Hanging Mercury Drop Electrode ◽  
Pulse Polarography ◽  
Pulse Voltammetry

Conditions were found for the determination of 6-mercaptopurine (I) and 6-thioguanine (II) by TAST polarography, differential pulse polarography and fast-scan differential pulse voltammetry at a hanging mercury drop electrode. The detection limits were 10-6, 8 . 10-8, and 6 . 10-8 mol l-1, respectively. A further lowering of the detection limit to 2 . 10-8 mol l-1 was attained by preliminary accumulation of the determined substances at the surface of a hanging mercury drop.

The voltammetric determination of 4-nitrobiphenyl

1991 ◽  
Vol 56 (3) ◽  
pp. 595-601 ◽  
Author(s):  
Jiří Barek ◽  
Gulamustafa Malik ◽  
Jiří Zima
Keyword(s):  
Differential Pulse Voltammetry ◽  
Differential Pulse ◽  
Voltammetric Determination ◽  
Hanging Mercury Drop Electrode ◽  
Optimum Conditions ◽  
Mercury Drop Electrode ◽  
Working Electrode ◽  
Pulse Voltammetry ◽  
Unstirred Solution

Optimum conditions were found for the determination of 4-nitrobiphenyl by fast scan differential pulse voltammetry at a hanging mercury drop electrode in the concentration range 1 . 10-5 to 2 . 10-7 mol l-1. A further increase in sensitivity was attained by adsorptive accumulation of this substance on the surface of the working electrode, permitting determination in the concentration range (2 – 10) . 10-8 mol l-1 with one minute accumulation of the substance in unstirred solution or (2 – 10) . 10-9 mol l-1 with three-minute accumulation in stirred solution. Linear scan voltammetry can be used to determine 4-nitrobiphenyl in the concentration range (2 – 10) . 10-9 mol l-1 with five-minute accumulation in stirred solution, with the advantage of a smoother baseline and smaller interference from substances that yield only tensametric peaks.

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