From Ag2S to luminescent Ag–In–S nanocrystals via an ultrasonic method – an in situ synthesis study in an NMR tube

2020 ◽  
Vol 8 (26) ◽  
pp. 8942-8952
Author(s):  
Patrycja Kowalik ◽  
Mateusz Penkala ◽  
Piotr Bujak ◽  
Angelika Kmita ◽  
Marta Gajewska ◽  
...  
Keyword(s):  
Ultrasonic Method ◽  
In Situ Synthesis ◽  
Preparation Conditions ◽  
First Time

Taking advantage of “mild” preparation conditions we have been able for the first time to perform the synthesis of Ag2S and luminescent AgInS2 nanocrystals in an NMR tube.

scholarly journals Graphene spin-coated electrode for polyacrylonitrile acoustic nanogenerators

2021 ◽  
Author(s):  
Sedigheh Aghayari
Keyword(s):  
Nickel Nanoparticles ◽  
In Situ Synthesis ◽  
Coated Electrode ◽  
The Subject ◽  
First Time ◽  
Piezoelectric Nanogenerators ◽  
High Dust ◽  
Screen Ink

Abstract In recent years piezoelectric nanogenerators, due to their more durability in high dust or humidity are more attractive than triboelectric ones. So, increasing their outputs is the subject of much researches. I focused on electrodes of the acoustic nanofibers nanogenerators for the first time. Here, I introduced a new electrode that is cheaper and does not result in lower outputs. Here for the first time graphene spin-coated ink was used for polyacrylonitrile-based acoustic nanogenerator. The results of the tests compared with the in-situ synthesis of nickel nanoparticles on the layer and using graphene spin-coated screen ink and conductive tapes. Finally, producing sound by this graphene ink was done too.

In situ synthesis of novel ZIF-8 membranes on polymeric and inorganic supports

2015 ◽  
Vol 3 (14) ◽  
pp. 7469-7476 ◽  
Author(s):  
V. I. Isaeva ◽  
M. I. Barkova ◽  
L. M. Kustov ◽  
D. A. Syrtsova ◽  
E. A. Efimova ◽  
...  
Keyword(s):  
In Situ Synthesis ◽  
Inorganic Supports ◽  
First Time

The fabrication of integrated ZIF-8 membranes via a direct in situ crystallization on a porous polyacrylonitrile material and a composite aluminum zirconate based support was performed for the first time.

In situ synthesis of protein-loaded hydrogels via biocatalytic ATRP

2020 ◽  
Vol 11 (8) ◽  
pp. 1525-1532 ◽  
Author(s):  
Aotian Zhang ◽  
Xiancheng Meng ◽  
Chunyang Bao ◽  
Qiang Zhang
Keyword(s):  
In Situ Synthesis ◽  
One Pot ◽  
P Protein ◽  
First Time ◽  
Polymerization Conditions

Protein-loaded hydrogels were synthesized in one pot under mild polymerization conditions via biocatalytic ATRP for the first time.

In situ synthesis of Na2Ti7O15 nanotubes on a Ti net substrate as a high performance anode for Na-ion batteries

2015 ◽  
Vol 51 (45) ◽  
pp. 9298-9300 ◽  
Author(s):  
Huan Li ◽  
Hailong Fei ◽  
Xin Liu ◽  
Jie Yang ◽  
Mingdeng Wei
Keyword(s):  
High Performance ◽  
Cycling Performance ◽  
In Situ Synthesis ◽  
First Time

Na2Ti7O15 nanotubes on a Ti net substrate were fabricated for the first time and exhibited excellent cycling performance.

In situ synthesis of ultrathin metal–organic framework nanosheets: a new method for 2D metal-based nanoporous carbon electrocatalysts

2017 ◽  
Vol 5 (35) ◽  
pp. 18610-18617 ◽  
Author(s):  
Liang Huang ◽  
Xueping Zhang ◽  
Yujie Han ◽  
Qingqing Wang ◽  
Youxing Fang ◽  
...  
Keyword(s):  
Oxygen Reduction Reaction ◽  
Metal Organic Framework ◽  
Nanoporous Carbon ◽  
Reduction Reaction ◽  
In Situ Synthesis ◽  
Growth Strategy ◽  
Carbon Nanosheets ◽  
Metal Organic ◽  
First Time

Ultrathin ZIF-67 nanosheets are synthesized for the first time via a salt-template confined in situ growth strategy. And the directly carbonized Co,N-doped nanoporous carbon nanosheets greatly boost the oxygen reduction reaction (ORR) as well.

In situ synthesis of porous SnO2 nanospheres/graphene composite with enhanced electrochemical performance

RSC Advances ◽  
2016 ◽  
Vol 6 (71) ◽  
pp. 67011-67016 ◽  
Author(s):  
Youwen Yang ◽  
Yuanhao Gao ◽  
Ting Cheng ◽  
Dongming Ma ◽  
Jiguang Liu ◽  
...  
Keyword(s):  
Electrochemical Performance ◽  
Hydrothermal Method ◽  
Graphene Nanosheets ◽  
Large Diameter ◽  
In Situ Synthesis ◽  
Graphene Composite ◽  
First Time ◽  
Enhanced Electrochemical Performance

A large diameter porous SnO2 nanospheres/graphene composite was synthesized by an in situ hydrothermal method for the first time. TEM images indicate that the porous SnO2 nanospheres are distributed on the graphene nanosheets uniformly.

Probing the Dynamic Self-Assembly Behaviour of Photoswitchable Wormlike Micelles in Real Time

2018 ◽  
Author(s):  
Elaine A. Kelly ◽  
Judith E. Houston ◽  
Rachel Evans
Keyword(s):  
Real Time ◽  
Absorption Spectroscopy ◽  
Self Assembly ◽  
Uv Light ◽  
Wormlike Micelles ◽  
Tetraethylene Glycol ◽  
Light Illumination ◽  
First Time ◽  
Dependent Processes

Understanding the dynamic self-assembly behaviour of azobenzene photosurfactants (AzoPS) is crucial to advance their use in controlled release applications such as<i></i>drug delivery and micellar catalysis. Currently, their behaviour in the equilibrium <i>cis-</i>and <i>trans</i>-photostationary states is more widely understood than during the photoisomerisation process itself. Here, we investigate the time-dependent self-assembly of the different photoisomers of a model neutral AzoPS, <a>tetraethylene glycol mono(4′,4-octyloxy,octyl-azobenzene) </a>(C<sub>8</sub>AzoOC<sub>8</sub>E<sub>4</sub>) using small-angle neutron scattering (SANS). We show that the incorporation of <i>in-situ</i>UV-Vis absorption spectroscopy with SANS allows the scattering profile, and hence micelle shape, to be correlated with the extent of photoisomerisation in real-time. It was observed that C<sub>8</sub>AzoOC<sub>8</sub>E<sub>4</sub>could switch between wormlike micelles (<i>trans</i>native state) and fractal aggregates (under UV light), with changes in the self-assembled structure arising concurrently with changes in the absorption spectrum. Wormlike micelles could be recovered within 60 seconds of blue light illumination. To the best of our knowledge, this is the first time the degree of AzoPS photoisomerisation has been tracked <i>in</i><i>-situ</i>through combined UV-Vis absorption spectroscopy-SANS measurements. This technique could be widely used to gain mechanistic and kinetic insights into light-dependent processes that are reliant on self-assembly.

The Total Synthesis of Rhabdastrellic Acid A

2018 ◽  
Author(s):  
Yaroslav Boyko ◽  
Christopher Huck ◽  
David Sarlah
Keyword(s):  
Total Synthesis ◽  
Late Stage ◽  
Cross Coupling ◽  
Side Chains ◽  
General Strategy ◽  
Modular Approach ◽  
Linear Sequence ◽  
Generating Sequence ◽  
First Time

<div>The first total synthesis of rhabdastrellic acid A, a highly cytotoxic isomalabaricane triterpenoid, has been accomplished in a linear sequence of 14 steps from commercial geranylacetone. The prominently strained <i>trans-syn-trans</i>-perhydrobenz[<i>e</i>]indene core characteristic of the isomalabaricanes is efficiently accessed in a selective manner for the first time through a rapid, complexity-generating sequence incorporating a reductive radical polyene cyclization, an unprecedented oxidative Rautenstrauch cycloisomerization, and umpolung 𝛼-substitution of a <i>p</i>-toluenesulfonylhydrazone with in situ reductive transposition. A late-stage cross-coupling in concert with a modular approach to polyunsaturated side chains renders this a general strategy for the synthesis of numerous family members of these synthetically challenging and hitherto inaccessible marine triterpenoids.</div>

Hydrothermal In Situ Synthesis ZnO Nanoarrays and Their Photocatalytic Applications

2013 ◽  
Vol 30 (6) ◽  
pp. 667
Author(s):  
Zhenzhen WANG ◽  
Fangfang LI ◽  
Han GUO ◽  
Jiuju FENG ◽  
Aijun WANG
Keyword(s):  
In Situ Synthesis ◽  
Photocatalytic Applications
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