scholarly journals High-throughput morphology mapping of self-assembling ternary polymer blends

RSC Advances ◽  
2020 ◽  
Vol 10 (69) ◽  
pp. 42529-42541
Author(s):  
Kristof Toth ◽  
Chinedum O. Osuji ◽  
Kevin G. Yager ◽  
Gregory S. Doerk
Keyword(s):  
Block Copolymer ◽  
High Throughput ◽  
Grazing Incidence ◽  
Ternary Mixtures ◽  
Electrospray Deposition ◽  
X Ray ◽  
Copolymer Blends ◽  
Self Assembling ◽  
X Ray Scattering ◽  
Ternary Polymer

Compositionally graded electrospray deposition combined with grazing incidence small angle X-ray scattering forms a high-throughput approach for mapping phase behavior in ternary mixtures as demonstrated here using block copolymer blends.

Probing Self-Assembly of Cylindrical Morphology Block Copolymer Using in Situ and ex Situ Grazing Incidence Small-Angle X-ray Scattering: The Attractive Case of Graphoepitaxy

2014 ◽  
Vol 47 (20) ◽  
pp. 7221-7229 ◽  
Author(s):  
Mireille Maret ◽  
Raluca Tiron ◽  
Xavier Chevalier ◽  
Patrice Gergaud ◽  
Ahmed Gharbi ◽  
...  
Keyword(s):  
Block Copolymer ◽  
Small Angle ◽  
Self Assembly ◽  
Grazing Incidence ◽  
Ex Situ ◽  
X Ray ◽  
X Ray Scattering ◽  
Attractive Case ◽  
Ray Scattering

An In Situ Grazing Incidence X-Ray Scattering Study of Block Copolymer Thin Films During Solvent Vapor Annealing

2013 ◽  
Vol 26 (2) ◽  
pp. 273-281 ◽  
Author(s):  
Xiaodan Gu ◽  
Ilja Gunkel ◽  
Alexander Hexemer ◽  
Weiyin Gu ◽  
Thomas P. Russell
Keyword(s):  
Thin Films ◽  
Block Copolymer ◽  
Grazing Incidence ◽  
Solvent Vapor ◽  
X Ray ◽  
X Ray Scattering ◽  
Vapor Annealing ◽  
Scattering Study ◽  
Solvent Vapor Annealing

Structural Analysis of Block Copolymer Thin Films with Grazing Incidence Small-Angle X-ray Scattering

2005 ◽  
Vol 38 (10) ◽  
pp. 4311-4323 ◽  
Author(s):  
Byeongdu Lee ◽  
Insun Park ◽  
Jinhwan Yoon ◽  
Soojin Park ◽  
Jehan Kim ◽  
...  
Keyword(s):  
Thin Films ◽  
Structural Analysis ◽  
Block Copolymer ◽  
Small Angle ◽  
Grazing Incidence ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

scholarly journals Self-assembly of block copolymers under non-isothermal annealing conditions as revealed by grazing-incidence small-angle X-ray scattering

2020 ◽  
Vol 27 (5) ◽  
pp. 1278-1288 ◽  
Author(s):  
Marta Fernández-Regúlez ◽  
Eduardo Solano ◽  
Laura Evangelio ◽  
Steven Gottlieb ◽  
Christian Pinto-Gómez ◽  
...  
Keyword(s):  
Block Copolymer ◽  
Small Angle ◽  
Self Assembly ◽  
Isothermal Annealing ◽  
Grazing Incidence ◽  
The Self ◽  
X Ray ◽  
Annealing Conditions ◽  
X Ray Scattering ◽  
Kinetics Of

An accurate knowledge of the parameters governing the kinetics of block copolymer self-assembly is crucial to model the time- and temperature-dependent evolution of pattern formation during annealing as well as to predict the most efficient conditions for the formation of defect-free patterns. Here, the self-assembly kinetics of a lamellar PS-b-PMMA block copolymer under both isothermal and non-isothermal annealing conditions are investigated by combining grazing-incidence small-angle X-ray scattering (GISAXS) experiments with a novel modelling methodology that accounts for the annealing history of the block copolymer film before it reaches the isothermal regime. Such a model allows conventional studies in isothermal annealing conditions to be extended to the more realistic case of non-isothermal annealing and prediction of the accuracy in the determination of the relevant parameters, namely the correlation length and the growth exponent, which define the kinetics of the self-assembly.

In situ grazing-incidence small-angle X-ray scattering observation of block-copolymer templated formation of magnetic nanodot arrays and their magnetic properties

Nano Research ◽  
2016 ◽  
Vol 10 (2) ◽  
pp. 456-471 ◽  
Author(s):  
Andreas Meyer ◽  
Norbert Franz ◽  
Hans Peter Oepen ◽  
Jan Perlich ◽  
Gerardina Carbone ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Block Copolymer ◽  
Small Angle ◽  
Grazing Incidence ◽  
X Ray ◽  
X Ray Scattering ◽  
Nanodot Arrays ◽  
Ray Scattering

scholarly journals Micellar‐Mediated Block Copolymer Ordering Dynamics Revealed by In Situ Grazing Incidence Small‐Angle X‐Ray Scattering during Spin Coating

2019 ◽  
Vol 29 (10) ◽  
pp. 1806741 ◽  
Author(s):  
Guillaume Fleury ◽  
Daniel Hermida‐Merino ◽  
Dong Jingjin ◽  
Karim Aissou ◽  
Aleksei Bytchkov ◽  
...  
Keyword(s):  
Block Copolymer ◽  
Small Angle ◽  
Spin Coating ◽  
Grazing Incidence ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering
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