scholarly journals The dance of the nanobubbles: detecting acoustic backscatter from sub-micron bubbles using ultra-high frequency acoustic microscopy

Nanoscale ◽  
2020 ◽  
Vol 12 (41) ◽  
pp. 21420-21428
Author(s):  
Michael J. Moore ◽  
Filip Bodera ◽  
Christopher Hernandez ◽  
Niloufar Shirazi ◽  
Eric Abenojar ◽  
...  

Detection of the motion of individual nanobubbles and microbubbles in an agarose gel using an ultra-high frequency acoustic microscope.

2018 ◽  
Vol 140 (4) ◽  
Author(s):  
Jeong Nyeon Kim ◽  
Richard L. Tutwiler ◽  
Judith A. Todd

In pressure vessel and pipe inspection, ultrasonic nondestructive evaluation plays a pivotal role in both in-situ and laboratory examinations. Scanning acoustic microscopy (SAM) has been a well-recognized laboratory tool for both visualization and quantitative evaluation of pressure vessel and piping materials at the microscale since its invention in 1974. While there have been multiple advances in SAM over the past four decades, some issues still remain to be addressed. First, the measurement speed is limited by the mechanical movement of the acoustic lens and the sample stage. Second, a single-element transducer with an acoustic lens forms a predetermined beam pattern for a fixed focal length and incident angle, thereby limiting control of the inspection beam. Here, we propose to develop a phased-array probe as an alternative to overcome these issues. Preliminary studies to design a practical high-frequency phased-array acoustic microscope probe were explored. A linear phased-array, comprising 32 elements and operating at 5 MHz, was modeled using PZFlex, a finite element method software. This phased-array system was characterized in terms of electrical input impedance response, pulse-echo and impulse response, surface displacement profiles, mode shapes, and beam profiles. Details of the construction of the model and the results are presented in this paper. Development of a phased-array acoustic microscope probe will significantly enhance scanning acoustic microscopy techniques for detecting surface and subsurface defects and microstructural changes in laboratory samples of pressure vessel and piping materials.


Author(s):  
Jeong Nyeon Kim ◽  
Richard L. Tutwiler ◽  
Judith A. Todd

Scanning acoustic microscopy (SAM) has been a well-recognized tool for both visualization and quantitative evaluation of materials at the microscale since its invention in 1974. While there have been multiple advances in SAM over the past four decades, some issues still remain to be addressed. First, the measurement speed is limited by the mechanical movement of the acoustic lens. Second, a single element transducer acoustic lens only delivers a predetermined beam pattern for a fixed focal length and incident angle, thereby limiting control of the inspection beam. Here, we propose to develop a phased-array probe as an alternative to overcome these issues. Preliminary studies to design a practical high frequency phased-array acoustic microscope probe were explored. A linear phased-array, comprising 32 elements and operating at 5 MHz, was modeled using PZFlex, a finite-element method software. This phased-array system was characterized in terms of electrical input impedance response, pulse-echo and impulse response, surface displacement profiles, mode shapes, and beam profiles. The results are presented in this paper.


Author(s):  
O. Diaz de Leon ◽  
M. Nassirian ◽  
C. Todd ◽  
R. Chowdhury

Abstract Integration of circuits on semiconductor devices with resulting increase in pin counts is driving the need for improvements in packaging for functionality and reliability. One solution to this demand is the Flip- Chip concept in Ultra Large Scale Integration (ULSI) applications [1]. The flip-chip technology is based on the direct attach principle of die to substrate interconnection.. The absence of bondwires clearly enables packages to become more slim and compact, and also provides higher pin counts and higher-speeds [2]. However, due to its construction, with inherent hidden structures the Flip-Chip technology presents a challenge for non-destructive Failure Analysis (F/A). The scanning acoustic microscope (SAM) has recently emerged as a valuable evaluation tool for this purpose [3]. C-mode scanning acoustic microscope (C-SAM), has the ability to demonstrate non-destructive package analysis while imaging the internal features of this package. Ultrasonic waves are very sensitive, particularly when they encounter density variations at surfaces, e.g. variations such as voids or delaminations similar to air gaps. These two anomalies are common to flip-chips. The primary issue with this package technology is the non-uniformity of the die attach through solder ball joints and epoxy underfill. The ball joints also present defects as open contacts, voids or cracks. In our acoustic microscopy study packages with known defects are considered. It includes C-SCAN analysis giving top views at a particular package interface and a B-SCAN analysis that provides cross-sectional views at a desired point of interest. The cross-section analysis capability gives confidence to the failure analyst in obtaining information from a failing area without physically sectioning the sample and destroying its electrical integrity. Our results presented here prove that appropriate selection of acoustic scanning modes and frequency parameters leads to good reliable correlation between the physical defects in the devices and the information given by the acoustic microscope.


Author(s):  
Li Na ◽  
Jawed Khan ◽  
Lonnie Adams

Abstract For stacked die package delamination inspection using C-mode acoustic microscope, traditional interface and thorough scan techniques cannot give enough of information when the delamination occurs in multi-interfaces, and echoes from adjacent interfaces are not sufficiently separated from each other. A thinner thickness in the stacked-die package could complicate C-mode scanning acoustic microscopy (CSAM) analysis and sometimes may lead to false interpretations. The first objective of this paper is to briefly explain the CSAM mechanism. Based on that, some of the drawbacks of current settings in detecting the delamination for stacked-die packages are presented. The last objective is to introduce quantitative B-scan analysis mode (Q-BAM) and Zip-Slice technologies in order to better understand and improve the reliability of detecting the delamination in stacked-die packages. Therefore, a large portion of this paper focuses on the Q-BAM and Zip-Slice data acquisition and image interpretation.


2014 ◽  
Author(s):  
Nicholas A. Bishop ◽  
Mohammod Ali ◽  
Jason Miller ◽  
David L. Zeppettella ◽  
William Baron ◽  
...  

2017 ◽  
Author(s):  
Thong Dao ◽  
Frank McGroarty ◽  
Andrew Urquhart

2020 ◽  
Vol 4 (41) ◽  
pp. 35-43
Author(s):  
ALEKSEY A. VASIL’EV ◽  
◽  
ALEKSEY N. VASIL’EV ◽  
DMITRIY BUDNIKOV ◽  
ANTON SHARKO

The use of electrophysical influences for pre-sowing treatment of seeds is an effective way to increase their sowing quality. The use of these methods is limited by the fact that their implementation requires new technological equipment in grain processing lines. This problem is solved more easily when pre-sowing processing is performed using installations for active ventilation and grain drying. (Research purpose) The research purpose is in determining the possibility of using active ventilation units and ultra-high-frequency convective grain dryers for pre-sowing grain processing and to evaluating the effectiveness of such processing using computer modeling. (Materials and methods) It is necessary to ensure the uniformity of processing with external influence the seeds placed in a dense layer. Authors carried out pre-sowing treatment of seeds on real installations. Treated seeds were sown in experimental plots and the results of treatment were evaluated. (Results and discussion) The article presents graphs of changes in grain temperature and humidity during processing. To check the feasibility of pre-sowing treatment, authors performed modeling of air-heat and ultra-high-frequency convective seed treatment processes. Based on the results of field experiments, air-heat treatment stimulates the development of secondary plant roots, contributes to an intensive increase in the green mass of plants; ultra-high-frequency convective seed treatment allows increasing the number of productive stems in plants, the number of ears in one plant. (Conclusions) Technological equipment designed for drying and active ventilation of grain can be effectively used for pre-sowing seed processing. In the course of field experiments, it was revealed the possibility of controlling the structure of the crop using different types of external influence on seeds during their pre-sowing processing.


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