Tuning uracil derivatives for the AIE-based detection of pyrene at a nano-molar level: single-crystal X-ray structure and DFT support

2020 ◽  
Vol 44 (36) ◽  
pp. 15376-15386
Author(s):  
Mahuya Banerjee ◽  
Milan Ghosh ◽  
Sabyasachi Ta ◽  
Subhasis Ghosh ◽  
Debasis Das

Single crystal X-ray structurally characterized azo-uracil derivative (L) is explored for the selective detection of pyrene via aggregation-induced emission (AIE) with 99-fold fluorescence enhancement.

2018 ◽  
Vol 47 (32) ◽  
pp. 11084-11090 ◽  
Author(s):  
Milan Ghosh ◽  
Sabyasachi Ta ◽  
Jesús Sanmartín Matalobos ◽  
Debasis Das

Single crystal X-ray structurally characterized azine derivative (L) was explored for selective detection of Molybdenum (Mo(vi)) cation through green emission. The L was very efficient for enrichment of Mo(vi) from aqueous solution.


2021 ◽  
Author(s):  
Kulwinder Kaur ◽  
Raghubir Singh ◽  
Varinder Kaur ◽  
Neena Capalash

Herein, synthesis, spectroscopic studies, single-crystal X-ray diffraction, aggregation-induced emission enhancement (AIEE) and sensing application of water-stable organotin(IV) compounds (4a-6a and 4b-6b) obtained from 3-hydroxy-4H-chromen-4-one ligands is reported. All the synthesized...


2020 ◽  
Vol 8 (47) ◽  
pp. 16974-16983
Author(s):  
Kun Wu ◽  
Ji Zheng ◽  
Yong-Liang Huang ◽  
Dong Luo ◽  
Yan Yan Li ◽  
...  

The (4,8)-connected Zr/Hf-MOFs exhibit excellent performances in the detection of Cr2O72− and the exact location and configuration of Cr2O72− inside the MOFs were revealed by single-crystal X-ray diffraction studies for the first time.


2020 ◽  
Vol 44 (20) ◽  
pp. 8477-8485 ◽  
Author(s):  
Somnath Khanra ◽  
Sabyasachi Ta ◽  
Milan Ghosh ◽  
Sudeshna Chatterjee ◽  
Pallabi Mukherjee ◽  
...  

Single crystal X-ray structurally characterized anthracene appended unsymmetrical azine derivative, viz. 4-(anthracen-9-ylmethylene-hydrazonomethyl)-2-methoxy-phenol (L5) shows Al3+ assisted aggregation induced emission in SDS medium.


2015 ◽  
Vol 39 (12) ◽  
pp. 9743-9751 ◽  
Author(s):  
Feifei Yu ◽  
Yunxu Yang ◽  
Aizhi Wang ◽  
Biwei Hu ◽  
Xiaofei Luo ◽  
...  

An α-cyanostilbene derivative was synthesized for the selective detection of sodium houttuyfonate via AIEE with an obvious fluorescence enhancement.


CrystEngComm ◽  
2021 ◽  
Author(s):  
Qingfang Lin ◽  
Zhihui Zong ◽  
Jing Tong ◽  
Wen Xie ◽  
Li-Li Liang

Two cluster-based metal-organic frameworks {[Cd5L4Br10]•2(CH3)2NH}n (1) and {[MnIII3OL(TA)3]F•sol}n (2) (L = 1,3,5-tris(benzimidazol-1-ylmethyl)-2,4,6-trimethylbenzene, TA = terephthalate anion) containing a semi-rigid tribenzimidazol-based ligand were synthesized and characterized. Single crystal X-ray analyses show...


Author(s):  
J. M. Galbraith ◽  
L. E. Murr ◽  
A. L. Stevens

Uniaxial compression tests and hydrostatic tests at pressures up to 27 kbars have been performed to determine operating slip systems in single crystal and polycrystal1ine beryllium. A recent study has been made of wave propagation in single crystal beryllium by shock loading to selectively activate various slip systems, and this has been followed by a study of wave propagation and spallation in textured, polycrystal1ine beryllium. An alteration in the X-ray diffraction pattern has been noted after shock loading, but this alteration has not yet been correlated with any structural change occurring during shock loading of polycrystal1ine beryllium.This study is being conducted in an effort to characterize the effects of shock loading on textured, polycrystal1ine beryllium. Samples were fabricated from a billet of Kawecki-Berylco hot pressed HP-10 beryllium.


Author(s):  
Süheyla Özbey ◽  
F. B. Kaynak ◽  
M. Toğrul ◽  
N. Demirel ◽  
H. Hoşgören

AbstractA new type of inclusion complex, S(–)-1 phenyl ethyl ammonium percholorate complex of R-(–)-2-ethyl - N - benzyl - 4, 7, 10, 13 - tetraoxa -1- azacyclopentadecane, has been prepared and studied by NMR, IR and single crystal X-ray diffraction techniques. The compound crystallizes in space group


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