Facile template free approach for the large-scale solid phase synthesis of nanocrystalline XIn2S4 (X = Cd/Zn) and its photocatalytic performance for H2 evolution

2020 ◽  
Vol 44 (23) ◽  
pp. 9634-9646 ◽  
Author(s):  
Sonali D. Naik ◽  
Sanjay K. Apte ◽  
Sunil N. Garaje ◽  
Yogesh A. Sethi ◽  
Manish D. Shinde ◽  
...  
Keyword(s):  
Large Scale ◽  
Photocatalytic Performance ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
H2 Evolution ◽  
Phase Synthesis ◽  
Template Free

Nanostructured CdIn2S4 and ZnIn2S4 with unique morphologies can be synthesized using this method which is simple and easy to operate.

A Facile Template-Free Approach for the Large-Scale Solid-Phase Synthesis of CdS Nanostructures and Their Excellent Photocatalytic Performance

Small ◽  
2011 ◽  
Vol 7 (7) ◽  
pp. 957-964 ◽  
Author(s):  
Sanjay K. Apte ◽  
Sunil N. Garaje ◽  
Gurudas P. Mane ◽  
Ajayan Vinu ◽  
Sonali D. Naik ◽  
...  
Keyword(s):  
Large Scale ◽  
Photocatalytic Performance ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Phase Synthesis ◽  
Cds Nanostructures ◽  
Template Free

Criteria for the economic large scale solid-phase synthesis of oligonucleotides

Tetrahedron ◽  
1994 ◽  
Vol 50 (8) ◽  
pp. 2617-2622 ◽  
Author(s):  
F.Xavier Montserrat ◽  
Anna Grandas ◽  
Ramon Eritja ◽  
Enrique Pedroso
Keyword(s):  
Large Scale ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Phase Synthesis

scholarly journals Optimal Method for Disulfide Bond Closure in the Synthesis of Atosiban—Antagonist of Oxytocin Receptors

2021 ◽  
Vol 47 (6) ◽  
pp. 1241-1248
Author(s):  
D. V. Avdeev ◽  
M. V. Ovchinnikov ◽  
Y. S. Dudkina ◽  
A. S. Molokoedov ◽  
A. A. Azmuko ◽  
...  
Keyword(s):  
Disulfide Bond ◽  
Large Scale ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Comparative Assessment ◽  
Polymer Support ◽  
Optimal Method ◽  
Phase Synthesis ◽  
Oxytocin Receptors ◽  
By Products

Abstract This work is devoted to the large-scale solid-phase synthesis (SPS) of Atosiban, Mpa1-D-Tyr(OEt)-Ile-Thr-Asn-Cys6-Pro-Orn-Gly-NH2 cyclic 1,6 disulfide, the only clinically used oxytocin receptor antagonist. The conditions have been selected for the closure of the disulfide bond (S–S) in the Atosiban molecule both in the solution and solid phase with the minimal formation of by-products. A comparative assessment of the formation of the S–S bond was carried out under various conditions. The formation of by-products during the closure of the disulfide bond has been studied both in solution and on the polymer support. The developed technique allows for the synthesis of Atosiban on an enlarged scale (10–20 mmol) involving the cyclization of a protected intermediate with the formation of the S–S bond during solid-phase synthesis with the minimal formation of by-products.

A facile template-free approach for the solid-phase synthesis of CoS2 nanocrystals and their enhanced storage energy in supercapacitors

RSC Advances ◽  
2014 ◽  
Vol 4 (91) ◽  
pp. 50220-50225 ◽  
Author(s):  
Ying Ji ◽  
Xiaoyang Liu ◽  
Wei Liu ◽  
Ying Wang ◽  
Hongdan Zhang ◽  
...  
Keyword(s):  
Molten Salt ◽  
Specific Capacitance ◽  
Solid Phase Synthesis ◽  
Solid Phase ◽  
Molten Salt Synthesis ◽  
Phase Synthesis ◽  
Template Free ◽  
Synthesis Approach ◽  
Storage Energy

Porous CoS2 is synthesized by a modified molten-salt synthesis approach with a specific capacitance as high as 654 F g−1.

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