Gated and non-gated silver detection using microwave-assisted laser induced breakdown spectroscopy

2021 ◽  
Author(s):  
M. A. Wakil ◽  
Zeyad T. Alwahabi
Keyword(s):  
Emission Line ◽  
Laser Induced Breakdown Spectroscopy ◽  
Breakdown Spectroscopy ◽  
Microwave Assisted ◽  
Liquid Samples ◽  
Laser Induced Breakdown ◽  
Line P

The detection of silver using microwave-assisted laser induced breakdown spectroscopy (MW-LIBS) is demonstrated in solid and liquid samples at a 338.28 nm emission line.

scholarly journals Quantitative Analysis of Cerium-Gallium Alloys Using a Hand-Held Laser Induced Breakdown Spectroscopy Device

Atoms ◽  
2019 ◽  
Vol 7 (3) ◽  
pp. 84 ◽  
Author(s):  
Ashwin P. Rao ◽  
Matthew T. Cook ◽  
Howard L. Hall ◽  
Michael B. Shattan
Keyword(s):  
Emission Line ◽  
Limit Of Detection ◽  
Weight Percent ◽  
Emission Lines ◽  
Resolving Power ◽  
Laser Induced Breakdown Spectroscopy ◽  
Significant Heterogeneity ◽  
Emission Data ◽  
Breakdown Spectroscopy ◽  
Laser Induced Breakdown

A hand-held laser-induced breakdown spectroscopy device was used to acquire spectral emission data from laser-induced plasmas created on the surface of cerium-gallium alloy samples with Ga concentrations ranging from 0–3 weight percent. Ionic and neutral emission lines of the two constituent elements were then extracted and used to generate calibration curves relating the emission line intensity ratios to the gallium concentration of the alloy. The Ga I 287.4-nm emission line was determined to be superior for the purposes of Ga detection and concentration determination. A limit of detection below 0.25% was achieved using a multivariate regression model of the Ga I 287.4-nm line ratio versus two separate Ce II emission lines. This LOD is considered a conservative estimation of the technique’s capability given the type of the calibration samples available and the low power (5 mJ per 1-ns pulse) and resolving power ( λ / Δ λ = 4000) of this hand-held device. Nonetheless, the utility of the technique is demonstrated via a detailed mapping analysis of the surface Ga distribution of a Ce-Ga sample, which reveals significant heterogeneity resulting from the sample production process.

Ultra-trace metallic element detection in liquid samples using laser induced breakdown spectroscopy based on matrix conversion and crosslinked PVA polymer membrane

2016 ◽  
Vol 31 (8) ◽  
pp. 1622-1630 ◽  
Author(s):  
Qingyu Lin ◽  
Xiaodan Han ◽  
Jie Wang ◽  
Zhimei Wei ◽  
Kunping Liu ◽  
...  
Keyword(s):  
Laser Induced Breakdown Spectroscopy ◽  
Metallic Elements ◽  
Breakdown Spectroscopy ◽  
Liquid Samples ◽  
Metallic Element ◽  
Laser Induced Breakdown ◽  
Ultra Trace ◽  
Trace Metallic Element ◽  
Matrix Conversion ◽  
Sensitive Method

A novel, sensitive method based on crosslinked polyvinyl alcohol (PVA) was developed for determining trace-amounts of metallic elements in liquid samples using laser induced breakdown spectroscopy (LIBS).

Microwave-assisted laser induced breakdown molecular spectroscopy: quantitative chlorine detection

2019 ◽  
Vol 34 (9) ◽  
pp. 1892-1899 ◽  
Author(s):  
M. A. Wakil ◽  
Zeyad T. Alwahabi
Keyword(s):  
Detection Limit ◽  
Molecular Spectroscopy ◽  
Laser Induced Breakdown Spectroscopy ◽  
Breakdown Spectroscopy ◽  
Microwave Assisted ◽  
Laser Induced Breakdown

A 47 ± 7 μg. g−1 detection limit of chlorine in cement has been recorded, using microwave-assisted laser induced breakdown spectroscopy.

Enhancement of intensity in microwave-assisted laser-induced breakdown spectroscopy for remote analysis of nuclear fuel recycling

2014 ◽  
Vol 29 (5) ◽  
pp. 886-892 ◽  
Author(s):  
Motonobu Tampo ◽  
Masabumi Miyabe ◽  
Katsuaki Akaoka ◽  
Masaki Oba ◽  
Hironori Ohba ◽  
...  
Keyword(s):  
Laser Ablation ◽  
Nuclear Fuel ◽  
Emission Intensity ◽  
Ablation Plume ◽  
Wire Antenna ◽  
Laser Induced Breakdown Spectroscopy ◽  
Breakdown Spectroscopy ◽  
Microwave Assisted ◽  
Laser Induced Breakdown ◽  
Remote Analysis

In this study, an enhancement of emission intensity from laser ablation plume was achieved by coupling a pulsed microwave using a simple wire antenna

Metal-chelate induced nanoparticle aggregation enhanced laser-induced breakdown spectroscopy for ultra-sensitive detection of trace metal ions in liquid samples

2020 ◽  
Vol 35 (1) ◽  
pp. 188-197 ◽  
Author(s):  
Xiaojiao Liu ◽  
Qingyu Lin ◽  
Yonghui Tian ◽  
Wenlong Liao ◽  
Tao Yang ◽  
...  
Keyword(s):  
Trace Metal ◽  
Metal Ions ◽  
Metal Chelate ◽  
Laser Induced Breakdown Spectroscopy ◽  
Nanoparticle Aggregation ◽  
Trace Metal Ions ◽  
Breakdown Spectroscopy ◽  
Liquid Samples ◽  
Laser Induced Breakdown ◽  
Matrix Conversion

A simple but efficient strategy based on a matrix conversion method has been developed for determining trace metal ions in liquid samples using laser-induced breakdown spectroscopy (LIBS).

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