Dried droplet calibration approach for the analysis of inorganic nonmetallic materials by laser ablation-inductively coupled plasma-mass spectrometry

2020 ◽  
Vol 35 (7) ◽  
pp. 1441-1449
Author(s):  
Linqian Guo ◽  
Qing Li ◽  
Yirui Chen ◽  
Guoxia Zhang ◽  
Yisheng Xu ◽  
...  

A simple and general dried droplet calibration approach was developed for the quantitative analysis of elements in inorganic nonmetallic materials using laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS).

2017 ◽  
Vol 32 (3) ◽  
pp. 587-596 ◽  
Author(s):  
Ángela Villaseñor ◽  
Caroline Greatti ◽  
Marina Boccongelli ◽  
José Luis Todolí

Liquid standards are deposited, dried and ablated from the solid sample surface for accurate analysis through laser ablation ICP-MS.


2015 ◽  
Vol 30 (2) ◽  
pp. 327-338 ◽  
Author(s):  
Natalia Miliszkiewicz ◽  
Stanisław Walas ◽  
Anna Tobiasz

For solid sample quantitative analysis by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) the main analytical problems are adequate standards preparation and signals standardization.


Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 345
Author(s):  
Ángela Villaseñor ◽  
Raquel Sánchez ◽  
Marina Boccongelli ◽  
José-Luis Todolí

The present work shows, for the first time, the application of laser ablation connected to inductively coupled plasma mass spectrometry (LA-ICP-MS) to the localized quantitative analysis of inclusions in polymeric industrial films. The multielemental mapping capabilities of LA-ICP-MS has allowed to chemically examine unique defects appeared during the plastic processing. This analytical tool is perfectly suited to detect elements such as Al, Mg, Zr, Ti, Cr, P, Pb, Sb, Zn, and Si in those inclusions. A method for multielemental quantitative analysis of these defects has been developed in the present work. The profiling for more than 100 different defects in three samples has demonstrated that more than 50% of these inclusions contain aggregates of some of the aforementioned elements. Therefore, the distribution of elements used as additives or present in catalysts must be carefully controlled during the production of polymeric films in order to avoid degradation in their performance.


2016 ◽  
Vol 31 (4) ◽  
pp. 1030-1033 ◽  
Author(s):  
J. S. Hamilton ◽  
E. L. Gorishek ◽  
P. M. Mach ◽  
D. Sturtevant ◽  
M. L. Ladage ◽  
...  

A new single Peltier element ablation cell is described and its applicability to biological sampling discussed to evaluate its performance.


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